SIGNIFICANCE AND USE
4.1 This test method is intended to be used for compliance with compositional specifications for manganese dioxide content in manganese ores. It is assumed that all who use these procedures will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices shall be followed, such as those described in Guide E882.
SCOPE
1.1 These test methods cover the determination of manganese dioxide in amounts commonly found in manganese ore. The determination measures the amount of manganese (IV) present in the sample. The result may be expressed as available oxygen or as manganese dioxide. The following test methods are included and may be used interchangeably:    
Sections  
Test Method A (Ferrous Ammonium Sulfate)  
9 – 13  
Test Method B (Periodate (Sodium Oxalate)  
14 – 18  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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This document specifies a potentiometric method for the determination of the manganese content of manganese ores and concentrates with manganese content equal to or greater than a mass fraction of 15 %.

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SIGNIFICANCE AND USE
5.1 This test method is intended to be used for compliance with compositional specifications for silica content. It is assumed that all who use these procedures will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices must be followed such as those described in Guide E882.
SCOPE
1.1 This test method covers the determination of silica in iron ores, iron ore concentrates and agglomerates, and manganese ore in the range from 0.5 % to 15 %.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
5.1 This test method is intended to be used as a referee method for compliance with compositional specifications for manganese content. It is assumed that all who use these procedures will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices must be followed such as those described in Guide E882.
SCOPE
1.1 This test method covers the determination of manganese in manganese ore in the range from 15 % to 60 %.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
5.1 This test method is intended to be used for compliance with compositional specifications for iron content in manganese ores. It is assumed that all who use these procedures will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices must be followed such as those described in Guide E882.
SCOPE
1.1 This test method covers the determination of iron in manganese ore in the range from 2 % to 20 %.  
Note 1: As used in this test method (except as related to the term relative standard deviation), “percent” or “%” refers to mass fraction (wt/wt) of the form 1g/100g.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Method I is applicable to manganese ores having chromium contents less than 0.1 % (m/m), method II is applicable to manganese ores having chromium contents greater than 0.1 % (m/m). This second edition cancels and replaces the first edition (i.e. ISO 619-1975). Should be read in conjunction with ISO 4297.

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The method is applicable to products having an arsenic content of 0,001 to 0.2 % (m/m). Should be read in conjunction with ISO 4297. Specifies principle, reactions, reagents, apparatus, sample, procedure and expression of results. A figure illustrates the apparatus for the distillation of arsenic.

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The method is applicable to products having sodium contents from 0,02 to 1,0 % (m/m), and potassium contents from 0,08 to 3,0 % (m/m). ISO 7969 should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, sampling, procedure and expression of results.

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The method is applicable to a concentration range of 0,1 to 4,0 % (m/m) of aluminium, 0,005 to 1,0 % (m/m) of copper, 0,005 to 1,0 % (m/m) of lead and 0,005 to 0,25 (m/m) of zinc. ISO 5889 should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, sampling, procedure and expression of results.

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The method is applicable to products having a silicon content greater than 0,5 % (m/m) and a fluorine content not more than 0,1 % (m/m). Should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, procedure and expression of results.

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The photometric method (A) is applicable to products having aluminium contents from 0,1 to 1,5 % (m/m), the oxine gravimetric method (B) is applicable to products having aluminium contents over 1,5 % (m/m). Cancels and replaces the first edition (ISO 4295:1978), of which it constitutes a technical revision. Should be read in conjunction with ISO 4297.

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The method is applicable to products having phosphorus contents from 0,02 to 0,5 % (m/m). ISO 4293 should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, sample, procedure and expression of results.

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The method is applicable to products having an iron content between 0,2 % (m/m) and 10 % (m/m). ISO 9681 should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, sampling and samples, procedure, and expression of results.

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Two methods are specified. Method A is applicable to products having a nickel content of 0.01 to 1.0 % (m/m), method B is applicable to products having a nickel content of 0.005 to 1.0 % (m/m). Both methods specify principle, reactions (method A only), reagents, apparatus, sample, procedure and expression of results.

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Describes three methods: methods I and II are gravimetric methods which are applicable to maganese ores having sulphur contents greater than 0.01 % (m/m), and method III is a titrimetric method. Should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, sample, procedure and expression of results. A figure illustrates the apparatus for determination of sulphur content in accordance with method III.

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The method is intended to be applied at the places of dispatch and/or acceptance of the ore. Annex A specifies a method to be used in the case of adhesive or wet manganese ores. Annex B specifies methods of correction for sprinkled water and/or rain-water. Cancels and replaces the first edition (ISO 4299:1980) of which it constitutes a minor revision.

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The method is applicable to products having calcium contents from 0,01 to 15 % (m/m) and magnesium contents from 0,01 to 4 % (m/m). ISO 7953 should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, sampling and samples, procedure and expression of results.

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The method is applicable to a concentration range of 0,08 to 3 % (m/m) of potassium and 0,02 to 1 % (m/m) of sodium. ISO 4571 should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, procedure and expression of results.

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This third edition cancels and replaces the second edition (ISO 312-1980), of which it constitutes a minor revision. Specifies principle, reagents, apparatus, sample, procedure and expression of results. A figure gives an example of apparatus.

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Method A is applicable to products having a total iron content from 1 to 25 % (m/m), and method B is applicable to products having a total iron content from 0.2 to 2 % (m/m). ISO 7990 should be read in conjunction with ISO 4297. Specifies principle, reactions (method A only), reagents, apparatus, sampling and samples, procedure and expression of results.

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Specifies general instructions concerning reagents, apparatus, sample, procedure, calibration graphs and test report.

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The method is applicable to products having calcium and magnesium contents greater than 0,3 % (m/m). Should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, sample, procedure and expression of results.

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The checking applies to manganese and chromium ores, whether natural or processed, being carried out in accordance with the methods specified in the relevant International Standards. Includes general conditions for division of experimental samples and experimental methods of division a) in three or more stages or b) in one or two stages.

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Specifies methods of preparing samples of manganese ores for determining the chemical composition and moisture content of a consignment. The methods are applicable to natural or processed manganese ores. Details of the riffle divider to be used are given in the annex.

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The method is based on drying of an air-dried test portion to constant mass in a laboratory oven at 105 °C to 110 °C, and measurement of the loss in mass. The determination is intended to be carried out simultaneously with that of other constituents of the same analytical sample, so that the contents of the other constituents can be calculated on the basis of the absolutely dry ore. Should be read in conjunction with ISO 4297.

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The checking applies to manganese and chromium ores, whether natural or processed, being carried out in accordance with the methods specified in the relevant International Standards. Includes conditions for sampling, preparation of experimental samples and of final moisture samples and moisture testing, gives a data sheet and analyses the experimental data and results.

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Specifies experimental methods for the evaluation of quality variation of manganese and chromium ores, whether natural or processed, for the purpose of defining sampling procedure by the mass-basis systematic method and the two-stage method as specified in the relevant International Standards. It also specifies methods for checking the precision of sampling by the mass-basis systematic method and the two-stage method.

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The checking applies to manganese and chromium ores, whether natural or processed, being carried out in accordance with the methods specified in the relevant International Standards. Includes general conditions for sampling and preparation of samples and experiments for bias of sampling and of sample preparation, gives a data analysis and reviews results.

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Specifies methods for taking samples of manganese ores to be used at the places of dispatch and acceptance of ores for determining the chemical composition and moisture content of a consignment.The methods are applicable to both the manual and mechanical sampling of natural or processed ores. Details of the hammer and shovel method are given in the annex.

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Applies to natural or processed manganese ores. The methods are applicable to size determination utilizing one or more sieves. ISO 6230 is intended to provide a basis for testing and for use of this material. When it is used for comparative purposes, agreements should be reached between the producer and the consumer in respect of the detailed method in order to eliminate sources of controversy.

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The method is based on drying of an air-dried test portion to constant mass in a laboratory oven at 105 °C to 110 °C, and measurement of the loss in mass. The determination is intended to be carried out simultaneously with that of other constituents of the same analytical sample, so that the contents of the other constituents can be calculated on the basis of the absolutely dry ore. Should be read in conjunction with ISO 4297.

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The method is applicable to products having an iron content between 0,2 % (m/m) and 10 % (m/m). ISO 9681 should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, sampling and samples, procedure, and expression of results.

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Applies to natural or processed manganese ores. The methods are applicable to size determination utilizing one or more sieves. ISO 6230 is intended to provide a basis for testing and for use of this material. When it is used for comparative purposes, agreements should be reached between the producer and the consumer in respect of the detailed method in order to eliminate sources of controversy.

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The method is intended to be applied at the places of dispatch and/or acceptance of the ore. Annex A specifies a method to be used in the case of adhesive or wet manganese ores. Annex B specifies methods of correction for sprinkled water and/or rain-water. Cancels and replaces the first edition (ISO 4299:1980) of which it constitutes a minor revision.

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The method is applicable to products having a total iron content from 0.1 % (m/m) to 15 % (m/m). ISO 9292 should be read in conjunction with ISO 4297. Specifies principle, reactions, reagents, apparatus, sampling and samples, procedure and expression of results.

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The photometric method (A) is applicable to products having aluminium contents from 0,1 to 1,5 % (m/m), the oxine gravimetric method (B) is applicable to products having aluminium contents over 1,5 % (m/m). Cancels and replaces the first edition (ISO 4295:1978), of which it constitutes a technical revision. Should be read in conjunction with ISO 4297.

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Specifies experimental methods for the evaluation of quality variation of manganese and chromium ores, whether natural or processed, for the purpose of defining sampling procedure by the mass-basis systematic method and the two-stage method as specified in the relevant International Standards. It also specifies methods for checking the precision of sampling by the mass-basis systematic method and the two-stage method.

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The checking applies to manganese and chromium ores, whether natural or processed, being carried out in accordance with the methods specified in the relevant International Standards. Includes conditions for sampling, preparation of experimental samples and of final moisture samples and moisture testing, gives a data sheet and analyses the experimental data and results.

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The checking applies to manganese and chromium ores, whether natural or processed, being carried out in accordance with the methods specified in the relevant International Standards. Includes general conditions for division of experimental samples and experimental methods of division a) in three or more stages or b) in one or two stages.

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The checking applies to manganese and chromium ores, whether natural or processed, being carried out in accordance with the methods specified in the relevant International Standards. Includes general conditions for sampling and preparation of samples and experiments for bias of sampling and of sample preparation, gives a data analysis and reviews results.

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This third edition cancels and replaces the second edition (ISO 312-1980), of which it constitutes a minor revision. Specifies principle, reagents, apparatus, sample, procedure and expression of results. A figure gives an example of apparatus.

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Method A is applicable to products having a total iron content from 1 to 25 % (m/m), and method B is applicable to products having a total iron content from 0.2 to 2 % (m/m). ISO 7990 should be read in conjunction with ISO 4297. Specifies principle, reactions (method A only), reagents, apparatus, sampling and samples, procedure and expression of results.

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The method is applicable to products having calcium contents from 0,01 to 15 % (m/m) and magnesium contents from 0,01 to 4 % (m/m). ISO 7953 should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, sampling and samples, procedure and expression of results.

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The method is applicable to products having sodium contents from 0,02 to 1,0 % (m/m), and potassium contents from 0,08 to 3,0 % (m/m). ISO 7969 should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, sampling, procedure and expression of results.

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Specifies methods for taking samples of manganese ores to be used at the places of dispatch and acceptance of ores for determining the chemical composition and moisture content of a consignment.The methods are applicable to both the manual and mechanical sampling of natural or processed ores. Details of the hammer and shovel method are given in the annex.

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Two methods are specified. Method A is applicable to products having a nickel content of 0.01 to 1.0 % (m/m), method B is applicable to products having a nickel content of 0.005 to 1.0 % (m/m). Both methods specify principle, reactions (method A only), reagents, apparatus, sample, procedure and expression of results.

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The method is applicable to products having a titanium content of 0,01 to 0,5 % (m/m). ISO 7723 should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, sample, procedure and expression of results.

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The method is applicable to products having an arsenic content of 0,001 to 0.2 % (m/m). Should be read in conjunction with ISO 4297. Specifies principle, reactions, reagents, apparatus, sample, procedure and expression of results. A figure illustrates the apparatus for the distillation of arsenic.

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Specifies methods of preparing samples of manganese ores for determining the chemical composition and moisture content of a consignment. The methods are applicable to natural or processed manganese ores. Details of the riffle divider to be used are given in the annex.

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The method is applicable to a concentration range of 0,1 to 4,0 % (m/m) of aluminium, 0,005 to 1,0 % (m/m) of copper, 0,005 to 1,0 % (m/m) of lead and 0,005 to 0,25 (m/m) of zinc. ISO 5889 should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, sampling, procedure and expression of results.

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