17.200 - Thermodynamics and temperature measurements
ICS 17.200 Details
Thermodynamics and temperature measurements
Thermodynamik. Temperaturmessungen
Thermodynamique et mesurage de temperature
Termodinamika in merjenje temperature
General Information
Frequently Asked Questions
ICS 17.200 is a classification code in the International Classification for Standards (ICS) system. It covers "Thermodynamics and temperature measurements". The ICS is a hierarchical classification system used to organize international, regional, and national standards, facilitating the search and identification of standards across different fields.
There are 1065 standards classified under ICS 17.200 (Thermodynamics and temperature measurements). These standards are published by international and regional standardization bodies including ISO, IEC, CEN, CENELEC, and ETSI.
The International Classification for Standards (ICS) is a hierarchical classification system maintained by ISO to organize standards and related documents. It uses a three-level structure with field (2 digits), group (3 digits), and sub-group (2 digits) codes. The ICS helps users find standards by subject area and enables statistical analysis of standards development activities.
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This document provides general methods for measurement and calculation of quantities associated with human exposure to electromagnetic fields in the frequency range from 0 Hz to 300 GHz. It is intended specifically to be used for the assessment of emissions from products and comparison of these with the exposure limits for the general public given in Council Recommendation 1999/519/EC, and those given for workers in Directive 2013/35/EU, as appropriate. It also is intended to be used for assessment of human exposure to electromagnetic fields in the workplace to determine compliance with the requirements of Directive 2013/35/EU.
This standard deals with quantities that can be measured or calculated external to the body, notably electric and magnetic field strength or power density, and includes the measurement and calculation of quantities inside the body that form the basis for protection guidelines. In particular the standard provides information on:
- definitions and terminology,
- characteristics of electromagnetic fields,
- measurement of exposure quantities,
- instrumentation requirements,
- methods of calibration,
- measurement techniques and procedures for evaluating exposure,
- calculation methods for exposure assessment.
Where an applicable electromagnetic field standard specific to a product or technology exists it is expected to be used rather than this document. EN 62311:-, Table 1 gives a list of relevant standards.
- Amendment9 pagesEnglish languagee-Library read for1 day
This document provides general methods for measurement and calculation of quantities associated with human exposure to electromagnetic fields in the frequency range from 0 Hz to 300 GHz. It is intended specifically to be used for the assessment of emissions from products and comparison of these with the exposure limits for the general public given in Council Recommendation 1999/519/EC, and those given for workers in Directive 2013/35/EU, as appropriate. It also is intended to be used for assessment of human exposure to electromagnetic fields in the workplace to determine compliance with the requirements of Directive 2013/35/EU. This standard deals with quantities that can be measured or calculated external to the body, notably electric and magnetic field strength or power density, and includes the measurement and calculation of quantities inside the body that form the basis for protection guidelines. In particular the standard provides information on: - definitions and terminology, - characteristics of electromagnetic fields, - measurement of exposure quantities, - instrumentation requirements, - methods of calibration, - measurement techniques and procedures for evaluating exposure, - calculation methods for exposure assessment. Where an applicable electromagnetic field standard specific to a product or technology exists it is expected to be used rather than this document. EN 62311:-, Table 1 gives a list of relevant standards.
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This part of IEC 61340 provides test methods and procedures for evaluating and selecting air ionization equipment and systems (ionizers).
This document establishes measurement techniques, under specified conditions, to determine offset voltage (ion balance) and decay (charge neutralization) time for ionizers.
This document does not include measurements of electromagnetic interference (EMI), or the use of ionizers in connection with ordnance, flammables, explosive items or electrically initiated explosive devices.
As contained in this document, the test methods and test conditions can be used by manufacturers of ionizers to provide performance data describing their products. Users of ionizers are urged to modify the test methods and test conditions for their specific application in order to qualify ionizers for use, or to make periodic verifications of ionizer performance. The user will decide the extent of the data required for each application.
See Annex A for information regarding theoretical background and additional information on the standard test method for the performance of ionizers.
CAUTION: Procedures and equipment described in this document can expose personnel to hazardous electrical and non-electrical conditions. Users of this document are responsible for selecting equipment that complies with applicable laws, regulatory codes and both external and internal policy. Users are cautioned that this document cannot replace or supersede any requirements for personnel safety. See Annex C for safety considerations.
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This document specifies requirements for the measurement of preheating temperature, interpass temperature and preheat maintenance temperature for fusion welding. This document can also be applied as appropriate in the case of other welding processes. This document does not apply to the measurement of post weld heat treatment temperatures.
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This part of IEC 61340 provides test methods and procedures for evaluating and selecting air ionization equipment and systems (ionizers). This document establishes measurement techniques, under specified conditions, to determine offset voltage (ion balance) and decay (charge neutralization) time for ionizers. This document does not include measurements of electromagnetic interference (EMI), or the use of ionizers in connection with ordnance, flammables, explosive items or electrically initiated explosive devices. As contained in this document, the test methods and test conditions can be used by manufacturers of ionizers to provide performance data describing their products. Users of ionizers are urged to modify the test methods and test conditions for their specific application in order to qualify ionizers for use, or to make periodic verifications of ionizer performance. The user will decide the extent of the data required for each application. See Annex A for information regarding theoretical background and additional information on the standard test method for the performance of ionizers. CAUTION: Procedures and equipment described in this document can expose personnel to hazardous electrical and non-electrical conditions. Users of this document are responsible for selecting equipment that complies with applicable laws, regulatory codes and both external and internal policy. Users are cautioned that this document cannot replace or supersede any requirements for personnel safety. See Annex C for safety considerations.
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This document specifies a method for the determination of reaction temperatures and times, enthalpies of reaction, and degrees of conversion using conventional differential scanning calorimetry (DSC) as specified in ISO 11357-1.
The method applies to monomers, prepolymers, and polymers in the solid or liquid state. The material can contain fillers and/or initiators in the solid or liquid state.
This document is not applicable to fast DSC as specified in ISO 23976.[1]
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This document specifies a method for the determination of the temperatures and enthalpies of melting and crystallization of crystalline or partially crystalline plastics using conventional DSC as specified in ISO 11357-1.
This document is not applicable to fast DSC as specified in ISO 23976.
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The EN 1434 series of standards provide technical principles and practical advice in selecting, installing and commissioning of thermal energy meters. However, because a standard cannot cover all areas completely, this document assists users of thermal energy meters.
- Technical report48 pagesEnglish languagee-Library read for1 day
The EN 1434 series of standards provide technical principles and practical advice in selecting, installing and commissioning of thermal energy meters. However, because a standard cannot cover all areas completely, this document assists users of thermal energy meters.
- Technical report48 pagesEnglish languagee-Library read for1 day
IEC 61340-4-7:2025 provides test methods and procedures for evaluating and selecting air ionization equipment and systems (ionizers). This document establishes measurement techniques, under specified conditions, to determine offset voltage (ion balance) and decay (charge neutralization) time for ionizers. This document does not include measurements of electromagnetic interference (EMI), or the use of ionizers in connection with ordnance, flammables, explosive items or electrically initiated explosive devices. As contained in this document, the test methods and test conditions can be used by manufacturers of ionizers to provide performance data describing their products. Users of ionizers are urged to modify the test methods and test conditions for their specific application in order to qualify ionizers for use, or to make periodic verifications of ionizer performance. The user will decide the extent of the data required for each application.
This edition includes the following significant technical changes with respect to the previous edition:
a) in Figure 5, a NOTE 3 was added to clarify that for AC bars and grids, a single emitter alternating between +/− polarity is used;
b) in Annex B, the relative error for measurement equipment was updated to include the consideration for the resolution of the voltmeter.
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This part of IEC 61340 provides electrical and mechanical test methods and performance limits for evaluation, acceptance and periodic verification testing of wrist straps. NOTE All dimensions are nominal except where indicated. This standard is intended for testing wrist straps and wrist strap systems used for the grounding of personnel engaged in working with ESD sensitive assemblies and devices. It does not address constant monitoring systems.
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This document specifies methods for the determination of oxidation induction time (isothermal OIT) and oxidation induction temperature (dynamic OIT) of polymeric materials by means of differential scanning calorimetry (DSC). It is applicable to polyolefin resins that are in a fully stabilized or compounded form, either as raw materials or finished products. It can be applicable to other plastics.
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IEC 61340-4-6:2025 provides electrical and mechanical test methods and performance limits for the evaluation, acceptance, and periodic verification testing of wrist straps. This document is intended for testing wrist straps and wrist strap systems used for the grounding of personnel engaged in working with ESD sensitive assemblies and devices. It does not address constant monitoring systems.
This edition includes the following significant technical changes with respect to the previous edition:
a) editorial comments made during the review of the second edition were reviewed and incorporated where appropriate;
b) normative references have been added to address the safety of equipment.
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This document specifies the general requirements of data exchange and interfaces for thermal energy meters.
This document is applicable to unidirectionally and bidirectionally transmitting thermal energy meters.
This document applies also to networks with up to 250 meters, for which a master unit with AC mains supply is necessary to control the M-Bus. In these cases, the document is only applicable in conjunction with EN 13757-2 (physical and link layer) and EN 13757-3 (application layer).
For wireless thermal energy meter communications, this document is only applicable in conjunction with EN 13757-4, which describes several alternatives of walk/drive-by readout via a mobile station or by using stationary receivers or a network.
NOTE Thermal energy meters are instruments intended for measuring the energy which in a heat-exchange circuit is absorbed (cooling) or given up (heating) by a liquid called the heat-conveying liquid. The meter indicates thermal energy in legal units.
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This document specifies the general requirements of data exchange and interfaces for thermal energy meters.
This document is applicable to unidirectionally and bidirectionally transmitting thermal energy meters.
This document applies also to networks with up to 250 meters, for which a master unit with AC mains supply is necessary to control the M-Bus. In these cases, the document is only applicable in conjunction with EN 13757-2 (physical and link layer) and EN 13757-3 (application layer).
For wireless thermal energy meter communications, this document is only applicable in conjunction with EN 13757-4, which describes several alternatives of walk/drive-by readout via a mobile station or by using stationary receivers or a network.
NOTE Thermal energy meters are instruments intended for measuring the energy which in a heat-exchange circuit is absorbed (cooling) or given up (heating) by a liquid called the heat-conveying liquid. The meter indicates thermal energy in legal units.
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This part of IEC 61340 provides test methods for measuring the electrical resistance of garments used for static control applications. These test methods can be used for evaluating outer garments that are homogenously conductive or homogeneously dissipative, or that utilize surface conductive or surface dissipative components or elements. NOTE The test methods defined in this standard might not be able to measure materials with buried conductive layers. The resistance point-to-point test method tests the electrical resistance between the two sleeves, any two panels or any two or more electrically interconnected components of the static control garment, including the electrical resistance across the seams and cuffs of the garment as applicable. An alternate sleeve-to-sleeve test method is allowed, using clamps to hang a garment. Static control garments that electrically bond to the wearer and provide a path to ground from the wearer are evaluated using the resistance point-to-point test method, the resistance point to groundable point test method, as well as a system test to determine the resistance from the person through the garment to the groundable point of the garment system. A band resistance measurement test is provided in IEC 61340-4-6 which can be used for garments so equipped with cuffs that are intended to perform the same function as a wrist strap band. The system test with a person wearing a groundable static control garment system includes the ground cord that connects to the groundable point of the garment.
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IEC 61340-4-9:2024 provides test methods for measuring the electrical resistance of garments used for static control applications. These test methods can be used for evaluating outer garments that are homogenously conductive or homogeneously dissipative, or that utilize surface conductive or surface dissipative components or elements.
NOTE It is possible that the test methods defined in this document will not be able to measure materials with buried conductive layers.
This third edition includes the following significant technical changes with respect to the previous edition:
a) IEC 61010-1 and IEC 61010-2-030 added as requirements for measurement equipment;
b) testing voltage range for personnel ground path changed from "7 V DC to 30 V DC" to "7 V DC to 100 V DC";
c) cleaning requirements changed from a minimum of five cycles of cleaning to a minimum of three cycles of cleaning;
d) moderate humidity requirements deleted;
e) figures replaced with generic drawings.
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EN 13611:2019, Clause 1 applies with the following modification and addition:
Modification:
The 1st paragraph of EN 13611:2019, Clause 1 is replaced by:
This document specifies the safety, design, construction, and performance requirements and testing for
mechanical thermostats intended for use with gas appliances and similar use, hereafter referred to as
“thermostats”.
This document is applicable to thermostats with declared maximum inlet pressures up to and including
50 kPa and of nominal connection sizes up to and including DN 50 for use with one or more fuel gases.
Addition:
This document is applicable to thermostats controlling the gas flow directly or indirectly through an
integral gas valve. This document applies to thermostats used with gas appliances which are not installed
in the open air.
Thermostats dealt with in this document are intended for control functions.
This document is not applicable to:
a) controls which use auxiliary energy (e.g. electrical energy supplied externally);
b) an assessment of the control regarding Performance Level (PL) and Safety Integrity Level (SIL).
The 4th paragraph of EN 13611:2019, Clause 1 is removed.
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IEC 60455-2:2023 is available as IEC 60455-2:2023 RLV which contains the International Standard and its Redline version, showing all changes of the technical content compared to the previous edition.
IEC 60455-2:2023 specifies methods of test to be used for testing resin based reactive compounds, their components and cured compounds used for electrical insulation. This fourth edition cancels and replaces the third edition published in 2015. This edition constitutes a technical revision. This edition includes the following significant technical changes with respect to the previous edition:
a) Introduction of test methods related to IEC 60455-3-8;
b) Additional and updated test methods for resins.
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SIGNIFICANCE AND USE
5.1 The crystallinity of UHMWPE will influence its mechanical properties, such as creep and stiffness. The reported crystallinity will depend on the integration range used to determine the heat of fusion, and the theoretical heat of fusion of 100 % crystalline polyethylene used to calculate the percent crystallinity in an unknown specimen. Differential scanning calorimetry is an effective means of accurately measuring both heat of fusion and melting temperature.
5.2 This test method is useful for both process control and research.
SCOPE
1.1 This quantitative test method discusses the measurement of the heat of fusion and the melting point of ultra-high molecular weight polyethylene (UHMWPE), and the subsequent calculation of the percentage of crystallinity. The method uses a differential scanning calorimeter and can be performed in the laboratory or in the field.
1.2 This test method can be used for UHMWPE in powder form, consolidated form, finished product, or a used product. It can also be used for irradiated or chemically crosslinked UHMWPE.
1.3 This test method does not suggest a desired range of crystallinity or melting points for specific applications.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The kinetic parameters provided in this practice may be used to evaluate the performance of a standard, apparatus, technique, or software for the determination parameters (such as Test Methods E698, E1641, E2041, or E2070) using thermal analysis techniques such as differential scanning calorimetry, and accelerating rate calorimetry (Guide E1981). The results obtained may be compared to the values provided by this practice.
Note 4: Not all reference materials are suitable for each measurement technique.
SCOPE
1.1 The purpose of this practice is to provide kinetic parameters for reference materials used to evaluate thermal analysis methods, apparatus, and software where enthalpy and temperature are measured. This practice addresses both exothermic and endothermic, nth order, and autocatalytic reactions.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The application of HFTs and temperature sensors to building envelopes provide in-situ data for evaluating the thermal performance of an opaque building envelope component under actual environmental conditions, as described in Practices C1046 and C1155. These applications require calibration of the HFTs at levels of heat flux and temperature consistent with end-use conditions.
5.2 This practice provides calibration procedures for the determination of the heat flux transducer sensitivity, S, that relates the HFT voltage output, E, to a known input value of heat flux, q.
5.2.1 The applied heat flux, q, shall be obtained from steady-state tests conducted in accordance with either Test Method C177, C518, C1114, C1363, or, for cryogenic applications, Guide C1774.
5.2.2 The resulting voltage output, E, of the heat flux transducer is measured directly using (auxiliary) readout instrumentation connected to the electrical output leads of the sensor.
Note 1: A heat flux transducer (see also Terminology C168) is a thin stable substrate having a low mass in which a temperature difference across the thickness of the device is measured with thermocouples connected electrically in series (that is, a thermopile). Commercial HFTs typically have a central sensing region, a surrounding guard, and an integral temperature sensor that are contained in a thin durable enclosure. Practice C1046, Appendix X2 includes detailed descriptions of the internal constructions of two types of HFTs.
5.3 The HFT sensitivity depends on several factors including, but not limited to, size, thickness, construction, temperature, applied heat flux, and application conditions including adjacent material characteristics and environmental effects.
5.4 The subsequent conversion of the HFT voltage output to heat flux under application conditions requires (1) a standardized technique for determining the HFT sensitivity for the application of interest; and, (2) a comprehensive understanding of t...
SCOPE
1.1 This practice, in conjunction with either Test Method C177, C518, C1114, or C1363, establishes procedures for the calibration of heat flux transducers that are dimensionally thin in comparison to their planar dimensions.
1.1.1 The thickness of the heat flux transducer shall be less than 30 % of the narrowest planar dimension of the heat flux transducer.
1.2 This practice describes techniques for determining the sensitivity, S, of a heat flux transducer when subjected to one dimensional heat flow normal to the planar surface or when installed in a building application.
1.3 This practice shall be used in conjunction with Practice C1046 and Practice C1155 when performing in-situ measurements of heat flux on opaque building envelope components. This practice is comparable, but not identical, to the calibration techniques described in ISO 9869-1.
1.4 This practice is not intended to determine the sensitivity of heat flux transducers used as components of heat flow meter apparatus, as in Test Method C518, or used for in-situ industrial applications, as covered in Practice C1041.
1.5 This practice does not preclude the laboratory calibration of heat flux transducers for large-scale insulation systems operated at temperatures lower or higher than that for building envelope components. For these applications, the heat flux transducers shall be calibrated at the temperatures that the transducer will be used.
1.5.1 For cryogenic applications, the test apparatuses described in Guide C1774 are acceptable methods for calibration.
1.6 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.
1.7 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered sta...
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SIGNIFICANCE AND USE
4.1 This practice describes the design of a guarded hot plate with circular line-heat sources and provides guidance in determining the mean temperature of the meter plate. It provides information and calculation procedures for: (1) control of edge heat loss or gain (Annex A1); (2) location and installation of line-heat sources (Annex A2); (3) design of the gap between the meter and guard plates (Appendix X1); and (4) location of heater leads for the meter plate (Appendix X2).
4.2 A circular guarded hot plate with one or more line-heat sources is amenable to mathematical analysis so that the mean surface temperature is calculated from the measured power input and the measured temperature(s) at one or more known locations. Further, a circular plate geometry simplifies the mathematical analysis of errors resulting from heat gains or losses at the edges of the specimens (see Refs (15, 16)).
4.3 The line-heat source(s) is (are) placed in the meter plate at a prescribed radius (radii) such that the temperature at the outer edge of the meter plate is equal to the mean surface temperature over the meter area. Thus, the determination of the mean temperature of the meter plate is accomplished with a small number of temperature sensors placed near the gap.
4.4 A guarded hot plate with one or more line-heat sources will have a radial temperature variation, with the maximum temperature differences being quite small compared to the average temperature drop across the specimens. Provided guarding is adequate, only the mean surface temperature of the meter plate enters into calculations of thermal transmission properties.
4.5 Care shall be taken to design a circular line-heat-source guarded hot plate so that the electric-current leads to each heater either do not significantly alter the temperature distributions in the meter and guard plates or else affect these temperature distributions in a known way so that appropriate corrections are applied.
4.6 The use of one o...
SCOPE
1.1 This practice covers the design of a circular line-heat-source guarded hot plate for use in accordance with Test Method C177.
Note 1: Test Method C177 describes the guarded-hot-plate apparatus and the application of such equipment for determining thermal transmission properties of flat-slab specimens. In principle, the test method includes apparatus designed with guarded hot plates having either distributed- or line-heat sources.
1.2 The guarded hot plate with circular line-heat sources is a design in which the meter and guard plates are circular plates having a relatively small number of heaters, each embedded along a circular path at a fixed radius. In operation, the heat from each line-heat source flows radially into the plate and is transmitted axially through the test specimens.
1.3 The meter and guard plates are fabricated from a continuous piece of thermally conductive material. The plates are made sufficiently thick that, for typical specimen thermal conductances, the radial and axial temperature variations in the guarded hot plate are quite small. By proper location of the line-heat source(s), the temperature at the edge of the meter plate is made equal to the mean temperature of the meter plate, thus facilitating temperature measurements and thermal guarding.
1.4 The line-heat-source guarded hot plate has been used successfully over a mean temperature range from − 10 to + 65°C, with circular metal plates and a single line-heat source in the meter plate. The chronological development of the design for circular line-heat-source guarded hot plates having a single line-heat source in the meter plate is given in Refs (1-9).2
1.5 For high-temperature applications, the line-heat-source guarded hot plate has been used successfully over a mean temperature from 7 to 160°C, with circular metal plates and multiple line-heat sources in the meter plate. The chronological development for circular line-heat-...
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SIGNIFICANCE AND USE
4.1 This practice provides a procedure for operating the apparatus so that the heat flow, Q′, through the meter section of the auxiliary insulation is small; determining Q′; and, calculating the heat flow, Q, through the meter section of the specimen.
4.2 This practice requires that the apparatus have independent temperature controls in order to operate the cold plate and auxiliary cold plate at different temperatures. In the single-sides mode, the apparatus is operated with the temperature of the auxiliary cold plate maintained at the same temperature of the hot plate face adjacent to the auxiliary insulation.
Note 4: In principle, if the temperature difference across the auxiliary insulation is zero and there are no edge heat losses or gains, all of the power input to the meter plate will flow through the specimen. In practice, a small correction is made for heat flow, Q′, through the auxiliary insulation.
4.3 The thermal conductance, C’, of the auxiliary insulation shall be determined from one or more separate tests using either Test Method C177, C1114, or as indicated in 5.4. Values of C’ shall be checked periodically, particularly when the temperature drop across the auxiliary insulation less than 1 % of the temperature drop across the test specimen.
4.4 This practice is used when it is necessary to determine the thermal properties of a single specimen. For example, the thermal properties of a single specimen are used to calibrate a heat-flow-meter apparatus for Test Method C518.
SCOPE
1.1 This practice covers the determination of the steady-state heat flow through the meter section of a specimen when a guarded-hot-plate apparatus or thin-heater apparatus is used in the single-sided mode of operation.
1.2 This practice provides a supplemental procedure for use in conjunction with either Test Method C177 or C1114 for testing a single specimen. This practice is limited to only the single-sided mode of operation, and, in all other particulars, the requirements of either Test Method C177 or C1114 apply.
Note 1: Test Methods C177 and C1114 describe the use of the guarded-hot-plate and thin-heater apparatus, respectively, for determining steady-state heat flux and thermal transmission properties of flat-slab specimens. In principle, these methods cover both the double- and single-sided mode of operation, and at present, do not distinguish between the accuracies for the two modes of operation. When appropriate, thermal transmission properties shall be calculated in accordance with Practice C1045.
1.3 This practice requires that the cold plates of the apparatus have independent temperature controls. For the single-sided mode of operation, a (single) specimen is placed between the hot plate and the cold plate. Auxiliary thermal insulation, if needed, is placed between the hot plate and the auxiliary cold plate. The auxiliary cold plate and the hot plate are maintained at the same temperature. The heat flow from the meter plate is assumed to flow only through the specimen, so that the thermal transmission properties correspond only to the specimen.
Note 2: The double-sided mode of operation requires similar specimens placed on either side of the hot plate. The cold plates that contact the outer surfaces of these specimens are maintained at the same temperature. The electric power supplied to the meter plate is assumed to result in equal heat flow through the meter section of each specimen, so that the thermal transmission properties correspond to an average for the two specimens.
1.4 This practice does not preclude the use of a guarded-hot-plate apparatus in which the auxiliary cold plate is either larger or smaller in lateral dimensions than either the test specimen or the cold plate.
Note 3: Most guarded-hot-plate apparatus are designed for the double-sided mode of operation (1).2 Consequently, the cold plate and the auxiliary cold plate are the same size and the spec...
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- Standard9 pagesEnglish languagesale 15% off
This document specifies the technical and functional characteristics for all types of thermometers (electronic, mechanical, etc.) for equipping the means used for the transport, storage and distribution of temperature sensitive goods and for measuring the ambient or internal temperature of the products between −80 °C and +85 °C.
It specifies the test methods which allow the verification of the equipment's conformity to suitability and performance requirements.
It applies to the whole thermometer and indicating device(s). The temperature sensor(s) can be integrated into the thermometer or remote from it (wired or wireless external temperature sensor(s)).
It does not specify the location of the thermometer and its sensors with respect to types of usage such as transport, storage and distribution.
NOTE Examples for the transport, storage and distribution of temperature sensitive goods between −80 °C and +85 °C include chilled, frozen, deep frozen and quick-frozen food; ice cream; fresh and hot food; pharmaceuticals; blood and organs; chemicals; biologicals; electronic and mechanical devices; flowers, plants and bulbs; raw materials and liquids; animals; art and furnishings.
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This document specifies the verification procedure for temperature recorders and thermometers for measuring the ambient or internal temperature of the products between −80 °C and +85 °C, which are intended to equip the means used for the transport, storage and distribution of temperature sensitive goods and which comply with standards EN 12830 and EN 13485 (measurement classes and ranges) and also others used for transport, distribution and/or storage of temperature sensitive goods.
It specifies the test methods which allow the verification of the equipment's conformity against class requirements identified in EN 12830 and EN 13485.
NOTE Examples for the transport, storage and distribution of temperature sensitive goods between −80 °C and +85 °C include chilled, frozen, deep frozen and quick-frozen food; ice cream; fresh and hot food; pharmaceuticals; blood and organs; chemicals; biologicals; electronic and mechanical devices; flowers, plants and bulbs; raw materials and liquids; animals; art and furnishings.
- Standard18 pagesEnglish languagee-Library read for1 day
This document specifies the verification procedure for temperature recorders and thermometers for measuring the ambient or internal temperature of the products between −80 °C and +85 °C, which are intended to equip the means used for the transport, storage and distribution of temperature sensitive goods and which comply with standards EN 12830 and EN 13485 (measurement classes and ranges) and also others used for transport, distribution and/or storage of temperature sensitive goods.
It specifies the test methods which allow the verification of the equipment's conformity against class requirements identified in EN 12830 and EN 13485.
NOTE Examples for the transport, storage and distribution of temperature sensitive goods between −80 °C and +85 °C include chilled, frozen, deep frozen and quick-frozen food; ice cream; fresh and hot food; pharmaceuticals; blood and organs; chemicals; biologicals; electronic and mechanical devices; flowers, plants and bulbs; raw materials and liquids; animals; art and furnishings.
- Standard18 pagesEnglish languagee-Library read for1 day
This document specifies the technical and functional characteristics for all types of thermometers (electronic, mechanical, etc.) for equipping the means used for the transport, storage and distribution of temperature sensitive goods and for measuring the ambient or internal temperature of the products between −80 °C and +85 °C.
It specifies the test methods which allow the verification of the equipment's conformity to suitability and performance requirements.
It applies to the whole thermometer and indicating device(s). The temperature sensor(s) can be integrated into the thermometer or remote from it (wired or wireless external temperature sensor(s)).
It does not specify the location of the thermometer and its sensors with respect to types of usage such as transport, storage and distribution.
NOTE Examples for the transport, storage and distribution of temperature sensitive goods between −80 °C and +85 °C include chilled, frozen, deep frozen and quick-frozen food; ice cream; fresh and hot food; pharmaceuticals; blood and organs; chemicals; biologicals; electronic and mechanical devices; flowers, plants and bulbs; raw materials and liquids; animals; art and furnishings.
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SCOPE
1.1 This terminology is a compilation of definitions of terms used by ASTM Committee E20 on Temperature Measurement.
1.2 Terms with definitions generally applicable to the fields of thermometry and hydrometry are listed in 3.1.
1.3 Terms with definitions applicable only to the indicated standards in which they appear are listed in 3.2.
1.4 Information about the International Temperature Scale of 1990 is given in Appendix X1.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This document specifies requirements and test methods for room temperature sensors used to control the room temperature.
This document is applicable to wall mounted and flush mounted room temperature sensors.
The following aspects are not covered by this document:
- pendulum temperature sensors;
- ceiling mounted temperature sensor;
- extract air temperature sensors.
NOTE The measured value available at the output of the sensor is influenced by the place where the sensor device is located and factors such as air velocity, wall temperature, self/waste heating of the device and the air temperature. The perceived temperature, which is important for the well-being of a person, depends among other factors on air temperature, temperature of the surrounding walls and air flow rate as indicated in EN ISO 7730.
The temperature sensor element can be combined with other sensors in one device. This document only deals with the room temperature sensing of this devices. Other sensors are not covered except of their influence on the room temperature sensing (e.g. self-heating).
This document specifies sensor characteristics contributing to the determination of the control accuracy of individual zone controller according to EN 15500 1.
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This document specifies requirements and test methods for room temperature sensors used to control the room temperature.
This document is applicable to wall mounted and flush mounted room temperature sensors.
The following aspects are not covered by this document:
- pendulum temperature sensors;
- ceiling mounted temperature sensor;
- extract air temperature sensors.
NOTE The measured value available at the output of the sensor is influenced by the place where the sensor device is located and factors such as air velocity, wall temperature, self/waste heating of the device and the air temperature. The perceived temperature, which is important for the well-being of a person, depends among other factors on air temperature, temperature of the surrounding walls and air flow rate as indicated in EN ISO 7730.
The temperature sensor element can be combined with other sensors in one device. This document only deals with the room temperature sensing of this devices. Other sensors are not covered except of their influence on the room temperature sensing (e.g. self-heating).
This document specifies sensor characteristics contributing to the determination of the control accuracy of individual zone controller according to EN 15500 1.
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SIGNIFICANCE AND USE
4.1 The oxygen consumption principle, used for the measurements described here, is based on the observation that, generally, the net heat of combustion is directly related to the amount of oxygen required for combustion (1).7 Approximately 13.1 MJ of heat are released per 1 kg of oxygen consumed. Test specimens in the test are burned in ambient air conditions, while being subjected to a prescribed external heating source.
4.1.1 This technique is not appropriate for use on its own when the combustible fuel is an oxidizer or an explosive agent, which release oxygen. Further analysis is required in such cases (see Appendix X2).
4.2 The heat release is determined by the measurement of the oxygen consumption, as determined by the oxygen concentration and the flow rate in the combustion product stream, in a full scale environment.
4.3 The primary measurements are oxygen concentration and exhaust gas flow rate. Additional measurements include the specimen ignitability, the smoke obscuration generated, the specimen mass loss rate, the effective heat of combustion and the yields of combustion products from the test specimen.
4.4 The oxygen consumption technique is used in different types of test methods. Intermediate scale (Test Method E1623, UL 1975) and full scale (Test Method D5424, Test Method D5537, Test Method E1537, Test Method E1590, Test Method E1822, ISO 9705, NFPA 265, NFPA 266, NFPA 267, NFPA 286, UL 1685) test methods, as well as unstandardized room scale experiments following Guide E603, using this technique involve a large instrumented exhaust hood, where oxygen concentration is measured, either standing alone or positioned outside a doorway. A large test specimen is placed either under the hood or inside the room. This practice is intended to address issues associated with equipment requiring a large instrumented hood and not stand-alone test apparatuses with small test specimens.
4.4.1 Small scale test methods using this technique, such as Tes...
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1.1 This practice deals with methods to construct, calibrate, and use full scale oxygen consumption calorimeters to help minimize testing result discrepancies between laboratories.
1.2 The methodology described herein is used in a number of ASTM test methods, in a variety of unstandardized test methods, and for research purposes. This practice will facilitate coordination of generic requirements, which are not specific to the item under test.
1.3 The principal fire-test-response characteristics obtained from the test methods using this technique are those associated with heat release from the specimens tested, as a function of time. Other fire-test-response characteristics also are determined.
1.4 This practice is intended to apply to the conduction of different types of tests, including both some in which the objective is to assess the comparative fire performance of products releasing low amounts of heat or smoke and some in which the objective is to assess whether flashover will occur.
1.5 This practice does not provide pass/fail criteria that can be used as a regulatory tool, nor does it describe a test method for any material or product.
1.6 For use of the SI system of units in referee decisions, see IEEE/ASTM SI-10. The units given in parentheses are provided for information only.
1.7 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.
Note 1: This is the standard caveat described in section F2.2.2.1 of the Form and Style for ASTM Standards manual for fire-test-response standards. In actual fact, this practice does not provide quantitative measures.
1.8 Fire testing of products and materials is inherently hazardous, and adequate safeguar...
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ABSTRACT
This specification contains reference tables that give temperature-electromotive force (emf) relationships for types B, E, J, K, N, R, S, T, and C thermocouples. These are the thermocouple types most commonly used in industry. Thermocouples and matched thermocouple wire pairs are normally supplied to the tolerances on initial values of emf versus temperature. Color codes for insulation on thermocouple grade materials, along with corresponding thermocouple and thermoelement letter designations are given. Four types of tables are presented: general tables, EMF versus temperature tables for thermocouples, EMF versus temperature tables for thermoelements, and supplementary tables.
SCOPE
1.1 This specification contains reference tables (Tables 8 to 25) that give temperature-electromotive force (emf) relationships for Types B, C, E, J, K, N, R, S, and T thermocouples.2 These are the thermocouple types most commonly used in industry. The tables contain all of the temperature-emf data currently available for the thermocouple types covered by this standard and may include data outside of the recommended upper temperature limit of an included thermocouple type.
1.2 In addition, the specification includes standard and special tolerances on initial values of emf versus temperature for thermocouples (Table 1), thermocouple extension wires (Table 2), and compensating extension wires for thermocouples (Table 3). Users should note that the stated tolerances apply only to the temperature ranges specified for the thermocouple types as given in Tables 1, 2, and 3, and do not apply to the temperature ranges covered in Tables 8 to 25.
1.3 Tables 4 and 5 provide insulation color coding for thermocouple and thermocouple extension wires as customarily used in the United States.
1.4 Recommendations regarding upper temperature limits for the thermocouple types referred to in 1.1 are provided in Table 6.
1.5 Tables 26 to 45 give temperature-emf data for single-leg thermoelements referenced to platinum (NIST Pt-67). The tables include values for Types BP, BN, JP, JN, KP (same as EP), KN, NP, NN, TP, and TN (same as EN).
1.6 Tables for Types RP, RN, SP, and SN thermoelements are not included since, nominally, Tables 18 to 21 represent the thermoelectric properties of Type RP and SP thermoelements referenced to pure platinum. Tables for the individual thermoelements of Type C are not included because materials for Type C thermocouples are normally supplied as matched pairs only.
1.7 Polynomial coefficients which may be used for computation of thermocouple emf as a function of temperature are given in Table 7. Coefficients for the emf of each thermocouple pair as well as for the emf of most individual thermoelements versus platinum are included. Coefficients for type RP and SP thermoelements are not included since they are nominally the same as for types R and S thermocouples, and coefficients for type RN or SN relative to the nominally similar Pt-67 would be insignificant. Coefficients for the individual thermoelements of Type C thermocouples have not been established.
1.8 Coefficients for sets of inverse polynomials are given in Table 46. These may be used for computing a close approximation of temperature (°C) as a function of thermocouple emf. Inverse functions are provided only for thermocouple pairs and are valid only over the emf ranges specified.
1.9 This specification is intended to define the thermoelectric properties of materials that conform to the relationships presented in the tables of this standard and bear the letter designations contained herein. Topics such as ordering information, physical and mechanical properties, workmanship, testing, and marking are not addressed in this specification. The user is referred to specific standards such as Specifications E235, E574, E585/E585M, E608/E608M, E1159, or E2181/E2181M for guidance in these areas.
1.10 The temperature-emf data in this specifica...
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SIGNIFICANCE AND USE
4.1 This guide describes a procedure for placing a water triple-point cell in service and for using it as a reference temperature in thermometer calibration.
4.2 The reference temperature attained is that of a fundamental state of pure water, the equilibrium between coexisting solid, liquid, and vapor phases.
4.3 The cell is subject to qualification but not to calibration. The cell may be qualified as capable of representing the fundamental state (see 4.2) by comparison with a bank of similar qualified cells of known history, and it may be so qualified and the qualification documented by its manufacturer.
4.4 The temperature to be attributed to a qualified water triple-point cell is exactly 273.16 K on the ITS-90, unless corrected for isotopic composition (refer to Appendix X3).
4.5 Continued accuracy of a qualified cell depends upon sustained physical integrity. This may be verified by techniques described in Section 6.
4.6 The commercially available triple point of water cells described in this standard are capable of achieving an expanded uncertainty (k=2) of between ±0.1 mK and ±0.05 mK, depending upon the method of preparation. Specified measurement procedures shall be followed to achieve these levels of uncertainty.
4.7 Commercially-available triple point of water cells of unknown isotopic composition should be capable of achieving an expanded uncertainty (k=2) of no greater than 0.25 mK, depending upon the actual isotopic composition (3). These types of cells are acceptable for use at this larger value of uncertainty.
SCOPE
1.1 This guide covers the nature of two commercial water triple-point cells (types A and B, see Fig. 1) and provides a method for preparing the cell to realize the water triple-point and calibrate thermometers. The qualifications concerning preparation and the types of glass used for a cell are discussed. Tests for assuring the integrity of a qualified cell and of cells yet to be qualified are given. Precautions for handling the cell to avoid breakage are also described.
FIG. 1 Configurations of two commonly used triple point of water cells, Type A and Type B, with ice mantle prepared for measurement at the ice/water equilibrium temperature. The cells are used immersed in an ice bath or water bath controlled close to 0.01 °C (see 5.5)
1.2 The effect of hydrostatic pressure on the temperature of a water triple-point cell is discussed.
1.3 Procedures for adjusting the observed SPRT resistance readings for the effects of self-heating and hydrostatic pressure are described in Appendix X1 and Appendix X2.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method is designed to measure and compare thermal properties of materials under controlled conditions and their ability to maintain required thermal conductance levels.
SCOPE
1.1 This test method covers a steady-state technique for the determination of the thermal conductivity of carbon materials in thicknesses of less than 25 mm. The test method is useful for homogeneous materials having a thermal conductivity in the approximate range 1−4 m2 ·K/W) over the approximate temperature range from 150 K to 600 K. It can be used outside these ranges with reduced accuracy for thicker specimens and for thermal conductivity values up to 60 W/(m·K).
Note 1: It is not recommended to test graphite cathode materials using this test method. Graphites usually have a very low thermal resistance, and the interfaces between the specimen to be tested and the instrument become more significant than the specimen itself.
1.2 This test method is similar in concept to Test Methods E1530 and C518. Significant attention has been paid to ensure that the thermal resistance of contacting surfaces is minimized and reproducible.
1.3 The values stated in SI units are regarded as standard.
1.3.1 Exception—The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This standard provides a description of test methods used in other ASTM specifications to establish certain acceptable methods for characterizing thermocouple assemblies and thermocouple cable. These test methods define how those characteristics shall be determined.
5.2 The usefulness and purpose of the included tests are given for the category of tests.
5.3 Warning—Users should be aware that certain characteristics of thermocouples might change with time and use. If a thermocouple’s designed shipping, storage, installation, or operating temperature has been exceeded, that thermocouple’s moisture seal may have been compromised and may no longer adequately prevent the deleterious intrusion of water vapor. Consequently, the thermocouple’s condition established by test at the time of manufacture may not apply later. In addition, inhomogeneities can develop in thermoelements because of exposure to higher temperatures, even in cases where maximum exposure temperatures have been lower than the suggested upper use temperature limits specified in Table 1 of Specification E608/E608M. For this reason, calibration of thermocouples destined for delivery to a customer is not recommended. Because the emf indication of any thermocouple depends upon the condition of the thermoelements along their entire length, as well as the temperature profile pattern in the region of any inhomogeneity, the emf output of a used thermocouple will be unique to its installation. Because temperature profiles in calibration equipment are unlikely to duplicate those of the installation, removal of a used thermocouple to a separate apparatus for calibration is not recommended. Instead, in situ calibration by comparison to a similar thermocouple known to be good is often recommended.
SCOPE
1.1 This document lists methods for testing Mineral-Insulated, Metal-Sheathed (MIMS) thermocouple assemblies and thermocouple cable, but does not require that any of these tests be performed nor does it state criteria for acceptance. The acceptance criteria are given in other ASTM standard specifications that impose this testing for those thermocouples and cable. Examples from ASTM thermocouple specifications for acceptance criteria are given for many of the tests. These tabulated values are not necessarily those that would be required to meet these tests, but are included as examples only.
1.2 These tests are intended to support quality control and to evaluate the suitability of sheathed thermocouple cable or assemblies for specific applications. Some alternative test methods to obtain the same information are given, since in a given situation, an alternative test method may be more practical. Service conditions are widely variable, so it is unlikely that all the tests described will be appropriate for a given thermocouple application. A brief statement is made following each test description to indicate when it might be used.
1.3 The tests described herein include test methods to measure the following properties of sheathed thermocouple material and assemblies.
1.3.1 Insulation Properties:
1.3.1.1 Compaction—direct method, absorption method, and tension method.
1.3.1.2 Thickness.
1.3.1.3 Resistance—at room temperature and at elevated temperature.
1.3.2 Sheath Properties:
1.3.2.1 Integrity—two water test methods and mass spectrometer.
1.3.2.2 Dimensions—length, diameter, and roundness.
1.3.2.3 Wall thickness.
1.3.2.4 Surface—gross visual, finish, defect detection by dye penetrant, and cold-lap detection by tension test.
1.3.2.5 Metallurgical structure.
1.3.2.6 Ductility—bend test and tension test.
1.3.3 Thermoelement Properties:
1.3.3.1 Calibration.
1.3.3.2 Homogeneity.
1.3.3.3 Drift.
1.3.3.4 Thermoelement diameter, roundness, and surface appearance.
1.3.3.5 Thermoelement spacing.
1.3.3.6 Thermoelement ductility.
1.3.3.7 Metallurgical structure.
1.3.4 Thermocouple Assembly Properti...
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SIGNIFICANCE AND USE
5.1 This test method can be used to quantify and compare the insulation provided by sleeping bags or sleeping bag systems. It can be used for material and design evaluations.
5.2 The measurement of the insulation provided by clothing (see Test Method F1291, ISO 15831) and sleeping bags (ISO 23537) is complex and dependent on the apparatus and techniques used. It is not practical in a test method of this scope to establish details sufficient to cover all contingencies. It is feasible that departures from the instructions in this test method will lead to significantly different test results. Technical knowledge concerning the theory of heat transfer, temperature and air motion measurement, and testing practices is needed to evaluate which departures from the instructions given in this test method are significant. Standardization of the method reduces, but does not eliminate, the need for such technical knowledge. Any departures need to be reported with the results.
SCOPE
1.1 This test method covers determination of the insulation value of a sleeping bag or sleeping bag system. It measures the resistance to dry heat transfer from a constant skin temperature manikin to a relatively cold environment. This is a static test that generates reproducible results, but the manikin cannot simulate real life sleeping conditions relating to some human and environmental factors, examples of which are listed in the introduction.
1.2 The insulation values obtained apply only to the sleeping bag or sleeping bag system, as tested, and for the specified thermal and environmental conditions of each test, particularly with respect to air movement past the manikin.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SCOPE
1.1 This is a compilation of only those terms and corresponding definitions included in or being considered for inclusion in ASTM documents relating to thermophysical properties. It is not intended as an all-inclusive listing of thermophysical property terms. Terms that are generally understood or defined adequately in other readily available sources are not included.
1.2 A definition is a single sentence with additional information included in a Discussion.
1.3 Definitions of terms specific to a particular field (such as dynamic mechanical measurements) are identified with an italicized introductory phrase.
1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SCOPE
1.1 This terminology is a compilation of definitions of terms used in ASTM documents relating to thermal analysis and rheology. This terminology includes only those terms for which ASTM either has standards or is contemplating some action. It is not intended to be an all-inclusive listing of terms related to thermal analysis and rheology.
1.2 This terminology specifically supports the single-word form for terms using thermo as a prefix, such as thermoanalytical or thermomagnetometry, while recognizing that for some terms a two-word form can be used, such as thermal analysis. This terminology does not support, nor does it recommend, use of the grammatically incorrect, single-word form using thermal as a prefix, such as, thermalanalytical or thermalmagnetometry.
1.3 A definition is a single sentence with additional information included in a Discussion area. It is reviewed every five years.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
6.1 These test methods are useful for research and development, quality assurance, regulatory compliance, and specification acceptance purposes.
6.2 The determination of the order of a chemical reaction or transformation at specific temperatures or time conditions is beyond the scope of these test methods.
6.3 The activation energy results obtained by these test methods may be compared with those obtained from Test Method E698 for nth order and accelerating reactions. Activation energy, pre-exponential factor, and reaction order results by these test methods may be compared to those for Test Method E2041 for nth order reactions.
SCOPE
1.1 Test Methods A, B, and C determine kinetic parameters for activation energy, pre-exponential factor and reaction order using differential scanning calorimetry (DSC) from a series of isothermal experiments over a small (≈10 K) temperature range. Test Method A is applicable to low nth order reactions. Test Methods B and C are applicable to accelerating reactions such as thermoset curing or pyrotechnic reactions and crystallization transformations in the temperature range from 300 K to 900 K (nominally 30 °C to 630 °C). These test methods are applicable only to these types of exothermic reactions when the thermal curves do not exhibit shoulders, double peaks, discontinuities or shifts in baseline.
1.2 Test Methods D and E also determines the activation energy of a set of time-to-event and isothermal temperature data generated by this or other procedures
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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IEC 60455-2:2023 is available as IEC 60455-2:2023 RLV which contains the International Standard and its Redline version, showing all changes of the technical content compared to the previous edition.IEC 60455-2:2023 specifies methods of test to be used for testing resin based reactive compounds, their components and cured compounds used for electrical insulation. This fourth edition cancels and replaces the third edition published in 2015. This edition constitutes a technical revision. This edition includes the following significant technical changes with respect to the previous edition: a) Introduction of test methods related to IEC 60455-3-8; b) Additional and updated test methods for resins.
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SIGNIFICANCE AND USE
4.1 The practice contained herein can be used as a basis for establishing conditions for the safe operation of critical structural components. The practices provide for general plant assessment and verification that materials continue meet design criteria and may in addition be of use for asset protection or life extension. The test specimens and procedures presented in this practice are for guidance when establishing a surveillance program.
4.2 This practice for high-temperature materials surveillance programs is used when nuclear reactor component materials are monitored by specimen testing. Periodic testing is performed through the service life of the components to assess changes in selected material properties that are caused by neutron irradiation, thermal effects, chemical reactions, and mechanical stress. The properties of interest are those used as design criteria for the respective nuclear components or well correlated to said criteria (see 5.1.6). The need for surveillance arises from the need to assess predictions of aging material performance to ensure adequate component performance.
4.3 This practice describes specimens and procedures required for the surveillance of multiple components. A surveillance program for a particular component will not necessarily require all test types described herein.
SCOPE
1.1 This practice covers procedures for surveillance program design and specimen testing to establish changes occurring in the mechanical properties of ferrous and nickel-based materials due to irradiation and thermal effects of nuclear component metallic materials used for high-temperature structural applications above 370 °C (700 °F). This should include consideration of gamma heating. This practice currently only applies to an initial program based on initial estimates of design life of components.
1.2 This practice was developed for non-light-water moderated nuclear power reactors.
1.3 This practice does not provide specific procedures for extending surveillance programs beyond their original design lifetimes.
1.4 This practice does not consider in-situ monitoring techniques but may provide insights into the proper periodicity and design of such.
1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method is intended to be used by wire producers and thermocouple manufacturers for certification of refractory metal thermocouples. It is intended to provide a consistent method for calibration of refractory metal thermocouples referenced to a calibrated radiation thermometer. Uncertainty in calibration and operation of the radiation thermometer, and proper construction and use of the test furnace are of primary importance.
5.2 Calibration establishes the temperature-emf relationship for a particular thermocouple under a specific temperature and chemical environment. However, during high temperature calibration or application at elevated temperatures in vacuum, oxidizing, reducing or contaminating environments, and depending on temperature distribution, local irreversible changes may occur in the Seebeck Coefficient of one or both thermoelements. If the introduced inhomogeneities are significant, the emf from the thermocouple will depend on the distribution of temperature between the measuring and reference junctions.
5.3 At high temperatures, the accuracy of refractory metal thermocouples may be limited by electrical shunting errors through the ceramic insulators of the thermocouple assembly. This effect may be reduced by careful choice of the insulator material, but above approximately 2100 °C, the electrical shunting errors may be significant even for the best insulators available.
SCOPE
1.1 This test method covers the calibration of refractory metal thermocouples using a radiation thermometer as the standard instrument. This test method is intended for use with types of thermocouples that cannot be exposed to an oxidizing atmosphere. These procedures are appropriate for thermocouple calibrations at temperatures above 800 °C (1472 °F).
1.2 The calibration method is applicable to the following thermocouple assemblies:
1.2.1 Type 1—Bare-wire thermocouple assemblies in which vacuum or an inert or reducing gas is the only electrical insulating medium between the thermoelements.
1.2.2 Type 2—Assemblies in which loose fitting ceramic insulating pieces, such as single-bore or double-bore tubes, are placed over the thermoelements.
1.2.3 Type 2A—Assemblies in which loose fitting ceramic insulating pieces, such as single-bore or double-bore tubes, are placed over the thermoelements, permanently enclosed and sealed in a loose fitting metal or ceramic tube.
1.2.4 Type 3—Swaged assemblies in which a refractory insulating powder is compressed around the thermoelements and encased in a thin-walled tube or sheath made of a high melting point metal or alloy.
1.2.5 Type 4—Thermocouple assemblies in which one thermoelement is in the shape of a closed-end protection tube and the other thermoelement is a solid wire or rod that is coaxially supported inside the closed-end tube. The space between the two thermoelements can be filled with an inert or reducing gas, or with ceramic insulating materials, or kept under vacuum.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Fixed-cell differential scanning calorimeters are used to determine the transition temperatures and energetics of materials in solution. For this information to be accepted with confidence in an absolute sense, temperature and heat calibration of the apparatus or comparison of the resulting data to that of known standard materials is required.
5.2 This practice is useful in calibrating the temperature and heat flow axes of fixed-cell differential scanning calorimeters.
SCOPE
1.1 This practice covers the calibration of fixed-cell differential scanning calorimeters over the temperature range from –10 °C to +120 °C.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 7.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Thermomechanical analyzers are employed in their various modes of operation (penetration, expansion, flexure, etc.) to characterize a wide range of materials. In most cases, the value to be assigned in thermomechanical measurements is the temperature of the transition (or event) under study. Therefore, the temperature axis (abscissa) of all TMA thermal curves must be accurately calibrated either by direct reading of a temperature sensor or by adjusting the programmer temperature to match the actual temperature over the temperature range of interest.
SCOPE
1.1 This test method describes the temperature calibration of thermomechanical analyzers from −50 °C to 1500 °C. (See Note 1.)
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 Warning—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 7 and Note 12.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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- Standard5 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
5.1 Most thermal analysis experiments are carried out under increasing temperature conditions where temperature is the independent parameter. Some experiments, however, are carried out under isothermal temperature conditions where the elapsed time to an event is measured as the independent parameter. Isothermal Kinetics (Test Methods E2070), Thermal Stability (Test Method E487), Oxidative Induction Time (OIT) (Test Methods D3895, D4565, D5483, E1858, and Specification D3350) and Loss-on-Drying (Test Methods E1868) are common examples of these kinds of experiments.
5.2 Modern scientific instruments, including thermal analyzers, usually measure elapsed time with excellent precision and accuracy. In such cases, it may only be necessary to confirm the performance of the instrument by comparison to a suitable reference. Only rarely will it may be required to correct the calibration of an instrument's elapsed time signal through the use of a calibration factor.
5.3 It is necessary to obtain elapsed time signal conformity only to 0.1 times the repeatability relative standard deviation (standard deviation divided by the mean value) expressed as a percent for the test method in which the thermal analyzer is to be used. For those test methods listed in Section 2 this conformity is 0.1 %.
SCOPE
1.1 This test method describes the calibration or performance confirmation of the elapsed-time signal from thermal analyzers.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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- Standard3 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
5.1 This method is suitable for determining the total heat of hydration of hydraulic cement at constant temperature at ages up to 7 days to confirm specification compliance.
5.2 This method compliments Practice C1679 by providing details of calorimeter equipment, calibration, and operation. Practice C1679 emphasizes interpretation significant events in cement hydration by analysis of time dependent patterns of heat flow, but does not provide the level of detail necessary to give precision test results at specific test ages required for specification compliance.
SCOPE
1.1 This test method specifies the apparatus and procedure for determining total heat of hydration of hydraulic cementitious materials at test ages up to 7 days by isothermal conduction calorimetry.
1.2 This test method also outputs data on rate of heat of hydration versus time that is useful for other analytical purposes, as covered in Practice C1679.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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- Standard8 pagesEnglish languagesale 15% off
SCOPE
1.1 Validation of methods and apparatus is requested or required for quality initiatives or where results may be used for legal purposes.
1.2 This standard provides terminology relating to validating performance of thermal analysis and rheology methods and instrumentation. Terms that are generally understood or defined adequately in other readily available sources are not included.
1.3 The terminology described in this standard is that of the validation process and may differ from that traditionally encountered in ASTM standards.
1.4 A definition is a single sentence with additional information included in a Discussion.
1.5 This terminology only includes those terms that are included in an ASTM standard or for which some action is under consideration. It is not intended as an all-inclusive listing of terms relating to performance validation.
1.6 Terminology commonly used in the study of precision and bias, in thermal analysis, rheology, and thermophysical properties may be found in Practice E177 and Terminologies E473 and E1142. Additional information on method validation may be found in the U.S. Pharmacopeia and National Formulary.2
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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- Standard3 pagesEnglish languagesale 15% off