77.120.50 - Titanium and titanium alloys
ICS 77.120.50 Details
Titanium and titanium alloys
Titan und -legierungen
Titane et alliages de titane
Titan in titanove zlitine
General Information
Frequently Asked Questions
ICS 77.120.50 is a classification code in the International Classification for Standards (ICS) system. It covers "Titanium and titanium alloys". The ICS is a hierarchical classification system used to organize international, regional, and national standards, facilitating the search and identification of standards across different fields.
There are 112 standards classified under ICS 77.120.50 (Titanium and titanium alloys). These standards are published by international and regional standardization bodies including ISO, IEC, CEN, CENELEC, and ETSI.
The International Classification for Standards (ICS) is a hierarchical classification system maintained by ISO to organize standards and related documents. It uses a three-level structure with field (2 digits), group (3 digits), and sub-group (2 digits) codes. The ICS helps users find standards by subject area and enables statistical analysis of standards development activities.
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This document specifies how a preliminary welding procedure specification (pWPS) is qualified by welding procedure tests.
This document specifies the conditions for the execution of welding procedure tests and the qualification range for welding procedures for all practical welding operations within the range of variables listed in Clause 8.
This document specifies the required tests. Additional tests can be required by application standards.
This document applies to the arc welding of titanium, zirconium and their alloys in all product forms. Arc welding is covered by the following processes in accordance with ISO 4063:
131 – metal inert gas welding, MIG welding;
14 – tungsten inert gas welding, TIG welding;
15 – plasma arc welding.
The principles of this document can be applied to other fusion welding processes.
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This document defines terms and definitions related to titanium and titanium alloys.
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SIGNIFICANCE AND USE
5.1 This procedure is suitable for manufacturing control and for verifying that the product meets specifications. It provides rapid, multi-element determinations with sufficient accuracy to assure product quality. The analytical performance data included may be used as a benchmark to determine if similar X-ray spectrometers provide equivalent precision and accuracy, or if the performance of a particular spectrometer has changed.
SCOPE
1.1 This test method covers the analysis of nickel and cobalt based alloys by wavelength dispersive X-ray fluorescence spectrometry for determination of the following elements:
Element
Composition Range
Aluminum
0.0X to X.XX
Chromium
0.XX to XX.XX
Copper
0.0X to XX.XX
Cobalt
0.XX to XX.XX
Hafnium
0.0X to 0.XX
Iron
0.XX to XX.XX
Manganese
0.XX to X.XX
Molybdenum
0.0X to XX.XX
Nickel
XX.XX to XX.XX
Niobium
0.XX to X.XX
Phosphorus
0.00X to 0.0XX
Silicon
0.0X to 0.XX
Tantalum
0.00X to X.XX
Titanium
0.XX to X.XX
Tungsten
0.XX to X.XX
Vanadium
0.00X to 0.XX
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This method has been interlaboratory tested for the elements and quantification ranges specified in 1.1. The ranges in 1.1 indicate intervals within which results have been demonstrated to be quantitative by the interlaboratory study. It may be possible to extend this method to other elements or different composition ranges provided that a method validation study as described in Guide E2857 is performed and that the results of this study show that the method extension is meeting laboratory data quality objectives.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method provides a rapid, economical method for determination of transformation temperatures.
5.2 Measurement of the specimen motion closely parallels many shape memory applications and provides a result that is applicable to the function of the material.
5.3 This test method uses a wire, tube, strip specimen, or a wire, tube, or strip specimen extracted from a component; thus, it provides an assessment of a nickel titanium product in its semifinished or finished form.
5.4 This test method may be used on annealed samples to determine the transformation temperatures and ensure the alloy formulation, since chemical analysis is not precise enough to adequately determine the nickel-to-titanium ratio of shape memory alloys.
5.5 In general, the transformation temperatures measured by this method will not be the same as those measured by the DSC method defined in Test Method F2004. Therefore, the results of DSC and BFR cannot be compared directly.
5.5.1 The BFR method measures the transformation temperatures by tracking shape recovery of stress-induced martensite deformed below the R′s temperature or the As temperature. In contrast, the DSC method measures the start, peak, and finish temperatures of the thermal transformation of martensite to R-phase or to austenite. See Refs (1-4).
5.6 The test method is applicable to shape memory alloys with Af temperatures in the range of approximately –25 to 90 °C.
SCOPE
1.1 This test method describes a procedure for quantitatively determining the martensite-to-austenite or the martensite to R-phase transformation temperature of annealed, aged, shape-set, or tempered nickel-titanium alloy specimens by deforming the specimen in bending and measuring the deformation recovered during heating through the thermal transformation (BFR method). See 3.1.1.
Note 1: For aged, shape-set, or tempered specimens the transformation may be from martensite to austenite or from martensite to R-phase. See Reference (1)2 for details.
1.2 The test specimen may be wire, tube, or strip or a specimen extracted from a semifinished or finished component.
1.2.1 For specimens not in the form of a wire, tube, or strip that are extracted from semifinished or finished components, a wire, tube, or strip shaped test specimen shall be made from the component such that the deformation mode in the test specimen is pure bending.
1.2.2 Other specimen geometries or displacements resulting in a more complex strain state, such as bending with torsion or buckling, are beyond the scope of this standard.
1.3 Ruggedness tests have demonstrated that sample Af must be limited to obtain good test results. See 5.6 for details. Ruggedness tests have demonstrated that deformation strain, deformation temperature, and equilibration time at the deformation temperature must be controlled to obtain good test results. See 9.1, 9.2, and 9.4 for details.
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This document specifies an inductively coupled plasma atomic emission spectrometric method for the determination of the contents (mass fraction) of aluminium and vanadium in 6Al-4V titanium alloys. This method is applicable to all kinds of 6Al-4V titanium alloys specified in ISO 23515 (designation of titanium alloys) for aluminium in the range from 4,70 % to 7,00 % and vanadium in the range from 3,00 % to 5,00 %.
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This document specifies an infrared absorption method after combustion in an induction furnace under oxygen atmosphere for the determination of carbon in titanium and titanium alloys. The method is applicable to carbon contents between 0,003 % (mass fraction) and 0,050 % (mass fraction).
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This document specifies requirements for the manufacture and technical delivery conditions of bar, rod and billet made from titanium and titanium alloys.
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This document specifies requirements for the manufacture and technical delivery conditions of plate, sheet and strip made from titanium and titanium alloys.
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This document specifies general requirements for the manufacture and technical delivery conditions of strips made from titanium and titanium alloys for welded tubes.
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SIGNIFICANCE AND USE
5.1 This test method is intended for the routine analysis of reactive metals and reactive metal alloys to verify compliance with compositional specifications such as those specified by Committees B09 and B10. It is expected that all who use this test method will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that the work will be performed in a properly equipped laboratory.
SCOPE
1.1 This test method applies to the determination of hydrogen in reactive metals and reactive metal alloys, particularly titanium and zirconium, with mass fractions from 9 mg/kg to 320 mg/kg.
1.2 This method has been interlaboratory tested for titanium and zirconium and alloys of these metals and can provide quantitative results in the range specified in 1.1. It may be possible to extend the quantitative range of this method provided a method validation study, as described in Guide E2857, is performed and the results of the study show the method extension meets laboratory data quality objectives. This method may also be extended to alloys other than titanium and zirconium provided a method validation study, as described in Guide E2857, is performed.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazards, see Section 9.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This document specifies a designation system of titanium and titanium alloys in terms of their chemical composition and impurities contents.
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SIGNIFICANCE AND USE
5.1 This test method is primarily intended as a test for compliance with compositional specifications. It is assumed that all who use this test method will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that the work will be performed in a properly equipped laboratory.
SCOPE
1.1 This test method covers the determination of oxygen in titanium and titanium alloys in mass fractions from 0.01 % to 0.5 % and the determination of nitrogen in titanium and titanium alloys in mass fractions from 0.003 % to 0.11 %.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in 8.8.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification covers the chemical, mechanical, and metallurgical requirements for wrought titanium-13niobium-13zirconium alloy (UNS R58130) bars and wires to be used in the manufacture of surgical implants. The mill products may be supplied as specified by the purchaser with a descaled or pickled, abrasive blasted, chemically milled, ground, machined, peeled, or polished finish. Materials shall be furnished in the unannealed, solution-treated, or capability-aged condition. The mechanical properties to which the alloys shall conform are tensile strength, yield strength, elongation, and reduction of area.
SCOPE
1.1 This specification covers the chemical, mechanical, and metallurgical requirements for wrought titanium-13niobium-13zirconium alloy to be used in the manufacture of surgical implants (1).2
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method for the chemical analysis of titanium and titanium alloys is primarily intended to test material for compliance with specifications of chemical composition such as those under the jurisdiction of ASTM Committee B10. It may also be used to test compliance with other specifications that are compatible with the test method.
5.2 It is assumed that all who use this test method will be trained analysts capable of performing common laboratory procedures skillfully and safely and that the work will be performed in a properly equipped laboratory.
5.3 This is a performance-based test method that relies more on the demonstrated quality of the test result than on strict adherence to specific procedural steps. It is expected that laboratories using this test method will prepare their own work instructions. These work instructions will include detailed operating instructions for the specific laboratory, the specific reference materials used, and performance acceptance criteria. It is also expected that, when applicable, each laboratory will participate in proficiency test programs, such as described in Practice E2027, and that the results from the participating laboratory will be satisfactory.
SCOPE
1.1 This method describes the analysis of titanium and titanium alloys, such as specified by committee B10, by inductively coupled plasma atomic emission spectrometry (ICP-AES) and direct current plasma atomic emission spectrometry (DCP-AES) for the following elements:
Element
Application
Range (wt.%)
Quantitative
Range (wt.%)
Aluminum
0–8
0.009 to 8.0
Boron
0–0.04
0.0008 to 0.01
Cobalt
0-1
0.006 to 0.1
Chromium
0–5
0.005 to 4.0
Copper
0–0.6
0.004 to 0.5
Iron
0–3
0.004 to 3.0
Manganese
0–0.04
0.003 to 0.01
Molybdenum
0–8
0.004 to 6.0
Nickel
0–1
0.001 to 1.0
Niobium
0-6
0.008 to 0.1
Palladium
0-0.3
0.02 to 0.20
Ruthenium
0-0.5
0.004 to 0.10
Silicon
0–0.5
0.02 to 0.4
Tantalum
0-1
0.01 to 0.10
Tin
0–4
0.02 to 3.0
Tungsten
0-5
0.01 to 0.10
Vanadium
0–15
0.01 to 15.0
Yttrium
0–0.04
0.001 to 0.004
Zirconium
0–5
0.003 to 4.0
1.2 This test method has been interlaboratory tested for the elements and ranges specified in the quantitative range part of the table in 1.1. It may be possible to extend this test method to other elements or broader mass fraction ranges as shown in the application range part of the table above provided that test method validation is performed that includes evaluation of method sensitivity, precision, and bias. Additionally, the validation study shall evaluate the acceptability of sample preparation methodology using reference materials or spike recoveries, or both. Guide E2857 provides information on validation of analytical methods for alloy analysis.
1.3 Because of the lack of certified reference materials (CRMs) containing bismuth, hafnium, and magnesium, these elements were not included in the scope or the interlaboratory study (ILS). It may be possible to extend the scope of this test method to include these elements provided that method validation includes the evaluation of method sensitivity, precision, and bias during the development of the testing method.
1.4 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific safety hazards statements are given in Section 9.
1.6 This international standard was developed in accordance with internationally recognized principle...
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SIGNIFICANCE AND USE
5.1 This test method for the chemical analysis of titanium alloys is primarily intended to test material for compliance to compositional requirements of specifications such as those under jurisdiction of ASTM Committee B10. It may also be used to test compliance with other specifications that are compatible with the test method.
5.2 This is a performance-based test method that relies more on the demonstrated quality of the test result than on strict adherence to specific procedural steps. It is assumed that all who use this test method will be trained analysts capable of performing common laboratory procedures skillfully and safely, and that the work will be performed in a properly equipped laboratory.
5.3 It is expected that laboratories using this test method will prepare their own work instructions. These work instructions will include detailed operating instructions for the specific laboratory, the specific reference materials employed, and performance acceptance criteria.
SCOPE
1.1 This test method describes the analysis of titanium and its alloys by spark atomic emission spectrometry (Spark-AES) and glow discharge atomic emission spectrometry (GD-AES). The titanium specimen to be analyzed may be in the form of a disk, casting, foil, sheet, plate, extrusion, or some other wrought form or shape. The elements and ranges covered in the scope by spark-AES of this test method are listed below.
Element
Tested Mass Fraction Range (%)
Aluminum
0.008 to 7.0
Chromium
0.006 to 0.1
Copper
0.014 to 0.1
Iron
0.043 to 0.3
Manganese
0.005 to 0.1
Molybdenum
0.014 to 0.1
Nickel
0.006 to 0.1
Silicon
0.018 to 0.1
Tin
0.02 to 0.1
Vanadium
0.015 to 5.0
Zirconium
0.013 to 0.1
1.1.1 The elements oxygen, nitrogen, carbon, niobium, boron, yttrium, palladium, and ruthenium, were included in the ILS but the data did not contain the required six laboratories. Precision tables were provided for informational use only.
1.2 The elements and ranges covered in the scope by GD-AES of this test method are listed below.
Element
Tested Mass Fraction Range (%)
Aluminum
0.02 to 7.0
Carbon
0.02 to 0.1
Chromium
0.006 to 0.1
Copper
0.028 to 0.1
Iron
0.09 to 0.3
Molybdenum
0.016 to 0.1
Nickel
0.006 to 0.1
Silicon
0.018 to 0.1
Tin
0.022 to 0.1
Vanadium
0.054 to 5.0
Zirconium
0.026 to 0.1
1.2.1 The elements boron, manganese, oxygen, nitrogen, niobium, yttrium, palladium, and ruthenium were included in the ILS, but the data did not contain the required six laboratories. Precision tables were provided for informational use only.
1.3 The elements and mass fractions given in the above scope tables are the ranges validated through the interlaboratory study. However, it is known that the techniques used in this standard allow the useable range, for the elements listed, to be extended higher or lower based on individual instrument capability, available reference materials, laboratory capabilities, and the spectral characteristics of the specific element wavelength being used. It is also acceptable to analyze elements not listed in 1.1 or 1.2 and still meet compliance to this standard test method. Laboratories must provide sufficient evidence of method validation when extending the analytical range or when analyzing elements not reported in Section 18 (Precision and Bias), as described in Guide E2857.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific safety hazard statements are given in Section 9.
1.5 This international standard was developed in accordance with internationally recognized pri...
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SIGNIFICANCE AND USE
4.1 The procedure described in this test method is designed to provide a method by which the coating weight of titanium treatments on metal substrates may be determined.
4.2 This test method is applicable for determination of the total coating weight and the titanium coating weight of a titanium-containing treatment.
SCOPE
1.1 This test method covers the use of wavelength dispersive X-ray fluorescence (WDXRF) techniques for determination of the coating weight of titanium treatments on metal substrates. These techniques are applicable for determination of the coating weight as titanium or total coating weight of a titanium containing treatment, or both, on a variety of metal substrates.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification covers additively manufactured titanium-6aluminum-4vanadium (Ti-6Al-4V) components using full-melt powder bed fusion such as electron beam melting and laser melting. It indicates the classifications of the components, the feedstock used to manufacture Class 1, 2, and 3 components, as well as the microstructure of the components. This specification also identifies the mechanical properties, chemical composition, and minimum tensile properties of the components.
SCOPE
1.1 This specification covers additively manufactured titanium-6aluminum-4vanadium (Ti-6Al-4V) components using full-melt powder bed fusion such as electron beam melting and laser melting. The components produced by these processes are used typically in applications that require mechanical properties similar to machined forgings and wrought products. Components manufactured to this specification are often, but not necessarily, post processed via machining, grinding, electrical discharge machining (EDM), polishing, and so forth to achieve desired surface finish and critical dimensions.
1.2 This specification is intended for the use of purchasers or producers, or both, of additively manufactured Ti-6Al-4V components for defining the requirements and ensuring component properties.
1.3 Users are advised to use this specification as a basis for obtaining components that will meet the minimum acceptance requirements established and revised by consensus of the members of the committee.
1.4 User requirements considered more stringent may be met by the addition to the purchase order of one or more Supplementary Requirements, which may include, but are not limited to, those listed in S1-S16.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification establishes the requirements for additively manufactured titanium-6aluminum-4vanadium with extra low interstitials (Ti-6Al-4V ELI) components using full-melt powder bed fusion such as electron beam melting and laser melting. The standard covers the classification of materials, ordering information, manufacturing plan, feedstock, process, chemical composition, microstructure, mechanical properties, thermal processing, hot isostatic pressing, dimensions and mass, permissible variations, retests, inspection, rejection, certification, product marking and packaging, and quality program requirements.
SCOPE
1.1 This specification covers additively manufactured titanium-6aluminum-4vanadium with extra low interstitials (Ti-6Al-4V ELI) components using full-melt powder bed fusion such as electron beam melting and laser melting. The components produced by these processes are used typically in applications that require mechanical properties similar to machined forgings and wrought products. Components manufactured to this specification are often, but not necessarily, post processed via machining, grinding, electrical discharge machining (EDM), polishing, and so forth to achieve desired surface finish and critical dimensions.
1.2 This specification is intended for the use of purchasers or producers or both of additively manufactured Ti-6Al-4V ELI components for defining the requirements and ensuring component properties.
1.3 Users are advised to use this specification as a basis for obtaining components that will meet the minimum acceptance requirements established and revised by consensus of the members of the committee.
1.4 User requirements considered more stringent may be met by the addition to the purchase order of one or more supplementary requirements, which may include, but are not limited to, those listed in S1-S4 and S1-S16 in Specification F2924.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SCOPE
1.1 This terminology is a compilation of definitions of terms used in ASTM documents relating to nickel-titanium shape memory alloys used for medical devices. This terminology includes only those terms for which ASTM either has standards or which are used in ASTM standards for nickel-titanium shape memory alloys. It is not intended to be an all-inclusive list of terms related to shape memory alloys.
1.2 Definitions that are similar to those published by another standards body are identified with abbreviations of the name of that organization; for example, ICTAC is the International Confederation for Thermal Analysis and Calorimetry.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This document specifies requirements for the classification of solid wire electrodes, solid wires and rods for fusion welding of titanium and titanium alloys. The classification is based on their chemical composition.
The compositions of solid wire electrodes for metal inert gas (MIG) welding are the same as solid wire electrodes, solid wires and rods for tungsten inert gas (TIG) arc welding, plasma arc welding, laser beam welding, and other fusion welding processes.
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ABSTRACT
This specification covers titanium and titanium alloy ingots. The chemical requirements and permissible variations in product analysis are specified. This standard does not claim to address all of the safety concerns, if any, associated with its use.
SCOPE
1.1 This specification covers titanium and titanium alloy ingots as follows:
1.1.1 Grade 1—UNS R50250. Unalloyed titanium,
1.1.2 Grade 2—UNS R50400. Unalloyed titanium,
1.1.3 Grade 3—UNS R50550. Unalloyed titanium,
1.1.4 Grade 4—UNS R50700. Unalloyed titanium,
1.1.5 Grade 5—UNS R56400. Titanium alloy (6 % aluminum, 4 % vanadium),
1.1.6 Grade 6—UNS R54520. Titanium alloy (5 % aluminum, 2.5 % tin),
1.1.7 Grade 7—UNS R52400. Unalloyed titanium plus 0.12 to 0.25 % palladium,
1.1.8 Grade 9—UNS R56320. Titanium alloy (3 % aluminum, 2.5 % vanadium),
1.1.9 Grade 11—UNS R52250. Unalloyed titanium plus 0.12 to 0.25 % palladium,
1.1.10 Grade 12—UNS R53400. Titanium alloy (0.3 % molybdenum, 0.8 % nickel),
1.1.11 Grade 13—UNS R53413. Titanium alloy (0.5 % nickel, 0.05 % ruthenium),
1.1.12 Grade 14—UNS R53414. Titanium alloy (0.5 % nickel, 0.05 % ruthenium),
1.1.13 Grade 15—UNS R53415. Titanium alloy (0.5 % nickel, 0.05 % ruthenium),
1.1.14 Grade 16—UNS R52402. Unalloyed titanium plus 0.04 to 0.08 % palladium,
1.1.15 Grade 17—UNS R52252. Unalloyed titanium plus 0.04 to 0.08 % palladium,
1.1.16 Grade 18—UNS R56322. Titanium alloy (3 % aluminum, 2.5 % vanadium) plus 0.04 to 0.08 % palladium,
1.1.17 Grade 19—UNS R58640. Titanium alloy (3 % aluminum, 8 % vanadium, 6 % chromium, 4 % zirconium, 4 % molybdenum),
1.1.18 Grade 20—UNS R58645. Titanium alloy (3 % aluminum, 8 % vanadium, 6 % chromium, 4 % zirconium, 4 % molybdenum) plus 0.04 to 0.08 % palladium,
1.1.19 Grade 21—UNS R58210. Titanium alloy (15 % molybdenum, 3 % aluminum, 2.7 % niobium, 0.25 % silicon),
1.1.20 Grade 23—UNS R56407. Titanium alloy (6 % aluminum, 4 % vanadium with extra low interstitials, ELI),
1.1.21 Grade 24—UNS R56405. Titanium alloy (6 % aluminum, 4 % vanadium) plus 0.4 to 0.8 % palladium,
1.1.22 Grade 25—UNS R56403. Titanium alloy (6 % aluminum, 4 % vanadium) plus 0.3 to 0.8 % nickel and 0.04 to 0.08 % palladium,
1.1.23 Grade 26—UNS R56404. Unalloyed titanium plus 0.08 to 0.14 % ruthenium,
1.1.24 Grade 27—UNS R52254. Unalloyed titanium plus 0.08 to 0.14 % ruthenium,
1.1.25 Grade 28—UNS R56323. Titanium alloy (3 % aluminum, 2.5 % vanadium) plus 0.08 to 0.14 % ruthenium,
1.1.26 Grade 29—UNS R56404. Titanium alloy (6 % aluminum, 4 % vanadium, extra low interstitial elements, ELI) plus 0.08 to 0.14 % ruthenium,
1.1.27 Grade 30—UNS R53530. Titanium alloy (0.3 % cobalt, 0.05 % palladium),
1.1.28 Grade 31—UNS R53532. Titanium alloy (0.3 % cobalt, 0.05 % palladium),
1.1.29 Grade 32—UNS R55111. Titanium alloy (5 % aluminum, 1 % tin, 1 % zirconium, 1 % vanadium, 0.8 % molybdenum),
1.1.30 Grade 33—UNS R53442. Titanium alloy (0.4 % nickel, 0.015 % palladium, 0.025 % ruthenium, 0.15 % chromium),
1.1.31 Grade 34—UNS R53445. Titanium alloy (0.4 % nickel, 0.015 % palladium, 0.025 % ruthenium, 0.15 % chromium),
1.1.32 Grade 35—UNS R56340. Titanium alloy (4.5 % aluminum, 2 % molybdenum, 1.6 % vanadium, 0.5 % iron, 0.3 % silicon),
1.1.33 Grade 36—UNS R58450. Titanium alloy (45 % niobium),
1.1.34 Grade 37—UNS R52815. Titanium alloy (1.5 % aluminum),
1.1.35 Grade 38—UNS R54250. Titanium alloy (4 % aluminum, 2.5 % vanadium, 1.5 % iron), and
1.1.36 Grade 39—UNS R53390. Titanium alloy (0.25 % iron, 0.4 % silicon).
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.3 The following caveat pertains only to the test method portions of this speci...
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ABSTRACT
This specification covers three grades of zirconium and zirconium alloy forgings. The forgings shall be formed with conventional forging equipment normally found in primary ferrous and nonferrous metal plants. The forgings are furnished in three grades as Grade R60702, Grade R60702, and Grade R60705. Forgings shall be furnished in the annealed conditions. The material shall conform to the requirements as to chemical composition and tensile properties prescribed. Two tension tests shall be made from each lot. Two chemistry tests for hydrogen and nitrogen content shall be made from each lot of finished product. If the results of any tests of any lot do not conform to the requirements specified, retests shall be made on additional forgings of double the original number of the same lot, each of which shall conform to the requirements specified.
SCOPE
1.1 This specification covers niobium-titanium alloy billets, bars, and rods, at 46 to 48 % titanium. This material is used in the manufacture of wire for superconducting applications.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 The following precautionary caveat pertains only to the test methods portion, Section 14, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This method is suitable for providing data on the chemical composition of titanium alloys having compositions within the scope of the standard. It is intended for routine production control and for determination of chemical composition for the purpose of certifying material specification compliance. Additionally, the analytical performance data included with this method may be used as a benchmark to determine if similar X-ray spectrometers provide equivalent precision and accuracy.
5.2 Compositions outside the ranges in 1.1 may be reported if proper method validation is performed. Refer to Guide E2857 for information on method validation.
SCOPE
1.1 This test method2 covers the X-ray fluorescence analysis of titanium alloys for the following elements in the ranges indicated:
Element
Range, %
Aluminum
0.041 to 8.00
Chromium
0.013 to 4.00
Copper
0.015 to 0.60
Iron
0.023 to 2.00
Manganese
0.003 to 9.50
Molybdenum
0.005 to 4.00
Nickel
0.005 to 0.80
Niobium
0.004 to 7.50
Palladium
0.014 to 0.200
Ruthenium
0.019 to 0.050
Silicon
0.014 to 0.15
Tin
0.017 to 3.00
Vanadium
0.017 to 15.50
Yttrium
0.0011 to 0.0100
Zirconium
0.007 to 4.00
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 10.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification covers the chemical, particle size, and cleanliness requirements for unalloyed titanium and titanium-6aluminum-4vanadium alloy powders for use as coatings, formed by sintering or thermal spraying techniques, onto titanium alloy surgical implants. The powders may be manufactured by the plasma rotating electrode, inert gas atomization, or hydride-dehydride process, or other method capable of producing powder meeting the requirements of this specification. This specification addresses only the powder requirements, and not the properties of the coatings formed from them.
SCOPE
1.1 This specification covers the requirements for unalloyed titanium and Ti-6Al-4V alloy powders for use in fabricating coatings on titanium alloy implants.
1.2 Powders covered under this specification may be used to form coatings by sintering or thermal spraying techniques.
1.3 This specification covers powder requirements only. It does not address properties of the coatings formed from them.
1.4 Finely divided titanium powder may be considered pyrophoric and should be handled in accordance with the appropriate guidelines.
1.5 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Differential scanning calorimetry provides a rapid method for determining the transformation temperature(s) of nickel-titanium shape memory alloys.
5.2 This test method uses small, stress-free, annealed samples to determine whether a sample of nickel-titanium alloy containing nominally 54.5 to 57.0 % nickel by weight is austenitic or martensitic at a particular temperature. Since chemical analysis of these alloys does not have sufficient precision to determine the transformation temperature by measuring the nickel-to-titanium ratio of the alloy, direct measurement of the transformation temperature of an annealed sample of known thermal history is recommended.
5.3 This test method is useful for quality control, specification acceptance, and research.
5.4 Transformation temperatures derived from differential scanning calorimetry (DSC) may not agree with those obtained by other test methods due to the effects of strain and load on the transformation. For example, transformation temperatures measured in accordance with Test Method F2082 will differ from those measured by the current standard.
5.5 The use of this test method for finished or semi-finished components without annealing (as in 8.2) shall be agreed upon between the purchaser and the supplier.
SCOPE
1.1 This test method defines procedures for determining the transformation temperatures of nickel-titanium shape memory alloys, produced in accordance with Specification F2063, by differential scanning calorimetry.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and to determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This International Standard specifies properties of titanium sponge used for malleable materials and castings.
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ISO 28401:2010 gives a classification of titanium and titanium alloys. It also gives terms and definitions in the field of titanium and its alloys.
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ISO 22962:2008 specifies an inductively coupled plasma atomic emission spectrometric method for the determination of the mass fraction of iron in titanium and titanium alloys. The method is applicable to titanium and titanium alloys with a mass fraction of iron in the range from 0,01 % to 3,0 %.
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ISO 12963:2008 specifies an infrared method after fusion under inert gas for the determination of the mass fraction of oxygen in titanium and titanium alloys. The method is applicable to titanium and titanium alloys with a mass fraction of oxygen in the range from 0,02 % to 0,4 %.
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ISO 22960:2008 specifies a molecular absorption spectrometric method using 1, 10-phenanthroline for the determination of the mass fraction of iron in titanium and titanium alloys. The method is applicable to titanium and titanium alloys with a mass fraction of iron in the range from 0,005 % to 2,0 %.
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ISO 22961:2008 specifies an atomic absorption spectrometric method for the determination of the mass fraction of iron in titanium and titanium alloys. The method is applicable to titanium and titanium alloys with a mass fraction of iron in the range from 0,005 % to 2,0 %.
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This standard specifies essential requirements, ranges of approval, test conditions, acceptance requirements and certification for the approval testing of welder performance for the welding of titanium and zirconium. This standard applies to the approval testing of welders for the fusion welding of titanium and zirconium. This standard is intended to provide basis for the mutual recognition by examining bodies for approval relating to welders' competence in the various fields of application.
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ISO 5832-3:2016 specifies the characteristics of, and corresponding test methods for, the wrought titanium alloy known as titanium 6-aluminium 4-vanadium alloy (Ti 6-AI4-V alloy) for use in the manufacture of surgical implants.
NOTE The mechanical properties of a sample obtained from a finished product made of this alloy may not necessarily comply with the specifications given in this part of ISO 5832.
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This document specifies the characteristics of, and corresponding test methods for, unalloyed titanium for use in the manufacture of surgical and dental implants.
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Specifies the characteristics of, and corresponding test methods for, the wrought titanium alloy known as titanium 6-aluminium 4-vanadium alloy (Ti 6-Al 4-V alloy) for use in the manufacture of surgical implants.
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ISO 15614-5:2004 specifies how a welding procedure specification is qualified by welding procedure tests.
It defines the conditions for the execution of welding procedure tests and the range of qualification for welding procedures for all practical welding operations within the range of variables listed in Clause 8.
It is intended that tests be carried out in accordance with this International Standard. Additional tests may be required by application standards.
ISO 15614-5:2004 applies to the arc welding of titanium, zirconium and their alloys in all product forms.
Arc welding is covered by the following processes in accordance with EN ISO 4063.
131 -- metal inert gas welding, MIG welding
141 -- tungsten inert gas welding, TIG welding
15 -- plasma arc welding
The principles of this International Standard may be applied to other fusion welding processes.
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ISO 24034:2010 specifies requirements for the classification of solid wire electrodes, solid wires and rods for fusion welding of titanium and titanium alloys. The classification is based on their chemical composition.
The compositions of solid wire electrodes for metal inert gas (MIG) welding are the same as solid wire electrodes, solid wires and rods for tungsten inert gas (TIG) arc welding, plasma arc welding, laser beam welding, and other fusion welding processes.
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This document specifies the characteristics of, and corresponding test methods for, unalloyed titanium for use in the manufacture of surgical and dental implants.
- Standard9 pagesEnglish languagee-Library read for1 day
Specifies the characteristics of, and corresponding test methods for, the wrought titanium alloy known as titanium 6-aluminium 4-vanadium alloy (Ti 6-Al 4-V alloy) for use in the manufacture of surgical implants.
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ABSTRACT
This specification deals with powder metallurgy structural components fabricated from commercially pure titanium powder mixed with master alloy powder and elemental powders to yield combined material chemistries comparable to ingot metallurgy alloys Titanium 6A1-4V and Titanium 6A1-6V2Sn. The following are the materials covered: Type I and II, Grade 1 and 2, and Class A and B. The chemical composition shall conform to the required values of aluminum, vanadium, tin, iron, copper, oxygen, hydrogen, nitrogen, carbon, sodium, chlorine, silicon, and titanium. Chemical analysis shall be made. Physical properties such as density shall be determined. Mechanical properties shall conform to the required tension properties: tensile strength, yield strength, elongation and reduction of area.
SCOPE
1.1 This specification covers powder metallurgy (PM) structural components fabricated from commercially pure (CP) titanium powder mixed with master alloy powder and elemental powders in appropriate quantity to yield combined material chemical compositions comparable to ingot metallurgy (I/M) alloys Titanium 6A1-4V and Titanium 6A1-6V-2Sn.
1.2 This specification covers the following materials:
1.2.1 Two types depending on alloy composition as detailed in Table 1.
1.2.1.1 Type I is comparable to I/M Ti-6A1-4V.
1.2.1.2 Type II is comparable to I/M Ti-6A1-6V-2Sn.
1.2.2 Two grades of each type that result from the specific titanium powder used are as follows:
1.2.2.1 Grade 1 is made from sponge fines with residual levels of chlorine and sodium.
1.2.2.2 Grade 2 is made from hydride/dehydride (HDH) or other process titanium with significantly lower chlorine and sodium content.
1.2.3 Two classes as a function of density (see Table 2) are as follows:
1.2.3.1 Class A density ratio is 94 % minimum.
1.2.3.2 Class B density ratio is 99 % minimum. (Warning—CP titanium powder may be pyrophoric; its use may involve an explosion hazard.)
1.3 The values stated in inch-pound units are to be regarded as the standard. The SI units given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 1.2.3.2.
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SCOPE
1.1 These test methods cover procedures for the chemical analysis of titanium and titanium alloys containing the following elements in the concentration ranges listed: Element Concentration Range, % Aluminum 1 to 10 Chloride 0.02 to 1.0 Chromium 0.005 to 20 Columbium 0.25 to 5.0 Copper 0.001 to 1.1 Iron 0.005 to 20 Magnesium 0.02 to 1.0 Manganese 0.005 to 20 Molybdenum 0.005 to 5 Nitrogen 0.005 to 0.20 Oxygen 0.03 to 0.50 Palladium 0.10 to 0.25 Silicon 0.005 to 5.0 Tantalum 0.25 to 5.0 Tin 0.25 to 10 Tungsten 0.005 to 1.0 Vanadium 0.5 to 20 Zirconium 1.0 to 20
1.2 The test methods in this standard are contained in the sections indicated as follows: Sections Aluminum: 8-Quinolinol (Gravimetric) Test Method 2 8 to 14 Chloride by the Gravimetric Test Method 2 15 to 22 Copper: Cuprizone (Photometric) Test Method 23 to 32 Diethyldithiocarbamate (Photometric) Test Method 33 to 42 Manganese: Periodate (Photometric) Test Method 43 to 52 Molybdenum Thiocyanate-Extraction (Photometric) Test Method 53 to 62 Thiocyanate 2-(2-Butoxyethoxy) Ethanol (Photometric) Test Method 63 to 72 Nitrogen by the Distillation-Titration Test Method 2 73 to 80 Palladium by the 1-Nitroso-2-Naphthol (Photometric) Test 81 to 90 Method Vanadium by the Potassium Permanganate (Titrimetric) Test 91 to 97 Method Zirconium by the Mandelic Acid (Gravimetric) Test Method 98 to 104
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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