75.100 - Lubricants, industrial oils and related products
ICS 75.100 Details
Lubricants, industrial oils and related products
Schmierstoffe
Lubrifiants, huiles industrielles et produits connexes
Maziva
General Information
Frequently Asked Questions
ICS 75.100 is a classification code in the International Classification for Standards (ICS) system. It covers "Lubricants, industrial oils and related products". The ICS is a hierarchical classification system used to organize international, regional, and national standards, facilitating the search and identification of standards across different fields.
There are 2272 standards classified under ICS 75.100 (Lubricants, industrial oils and related products). These standards are published by international and regional standardization bodies including ISO, IEC, CEN, CENELEC, and ETSI.
The International Classification for Standards (ICS) is a hierarchical classification system maintained by ISO to organize standards and related documents. It uses a three-level structure with field (2 digits), group (3 digits), and sub-group (2 digits) codes. The ICS helps users find standards by subject area and enables statistical analysis of standards development activities.
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This document is a part of a package of standards: EN 12080, EN 12081, EN 12082-1 and EN 12082-2. This document specifies the quality requirements of greases intended for the lubrication of axlebox rolling bearings according to EN 12080, required for reliable operation of trains on European networks. It covers the requirements for conformity assessment of new greases, as well as requirements for quality batch control and change management.
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This document is a part of a package of standards: EN 12080, EN 12081, EN 12082-1 and EN 12082-2. This document specifies the quality requirements of greases intended for the lubrication of axlebox rolling bearings according to EN 12080, required for reliable operation of trains on European networks. It covers the requirements for conformity assessment of new greases, as well as requirements for quality batch control and change management.
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Creation of a Technical Report summarizing the information on the biodegradation testing of fully formulated biobased lubricants. The document will comprise general and advanced technical information on the study and on the results.
- Technical report26 pagesEnglish languagee-Library read for1 day
Creation of a Technical Report summarizing the information on the biodegradation testing of fully formulated biobased lubricants. The document will comprise general and advanced technical information on the study and on the results.
- Technical report26 pagesEnglish languagee-Library read for1 day
This document provides test procedures for evaluating coated proppants used in hydraulic fracturing operation. This document provides a consistent methodology for tests performed on coated proppants used in hydraulic fracturing operations.
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This document provides guidance and requirements for the maintenance in service of mineral oils used as lubricating oils and control fluids used to lubricate steam, gas and combined cycle turbines in service. This document is applicable to lubricants classified in ISO 6743-5 and specified in ISO 8068, except the grades TSD, TGD and TCD (phosphate esters) for which ISO 11365 is more relevant, and the grades TGCE, THA, THCH, THCE and THE. This document also gives guidance and requirements with respect to the corrective actions that are taken to maximize service life.
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This document specifies a test method for determining the coefficient of friction and its evolution in mechanical transmission fluids tribologically interacting with materials used in synchronizers in manual transmission (MT) gears under high-frequency linear oscillation motion using the linear-oscillation (SRV) test machine. A flat areal contact geometry is applied.
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This document specifies a procedure for the evaluation of the filterability of dry lubricating oils. The procedure only applies to mineral-based oils, since fluids manufactured from other materials (e.g. fire-resistant fluids) can be incompatible with the specified test membranes. This document is applicable to oils of viscosity up to ISO viscosity grade (VG) 100, as defined in ISO 3448. These oils are widely used as hydraulic fluids, and within the range described, the variation in filterability due to viscosity is included within the precision range of this document. The procedure is not suitable for some hydraulic oils on which specific properties are conferred by the use of insoluble or partially soluble additives, or by particularly large molecular species. These additives include some viscosity index modifiers and some friction modifying additives. This document can also be applied to oils of ISO viscosity grades (VG) 150, 220 and 320, as defined in ISO 3448, using the specified 3,0 µm rated membranes. These oils are widely used as heavy-duty lubricants in equipment such as paper making machines and rolling mills. Within the range described, the filterability as defined is not dependent on the viscosity of the oil.
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This document specifies a procedure for the evaluation of the filterability of lubricating oils in the presence of water. The procedure only applies to mineral-based oils, since fluids manufactured from other materials (e.g. fire-resistant fluids) can be incompatible with the specified test membranes. This document is applicable to oils of viscosity up to ISO viscosity grade (VG) 100, as defined in ISO 3448. Within the range described, the variation in filterability due to viscosity is included within the precision range of this document. The procedure is not suitable for some hydraulic oils on which specific properties are conferred by the use of insoluble or partially soluble additives, or by particularly large molecular species. These additives include some viscosity index modifiers and some friction modifying additives. This document can also be applied to oils of ISO viscosity grades (VG) 150, 220 and 320, as defined in ISO 3448, using the specified 3,0 µm rated membranes. These oils are widely used as heavy-duty lubricants in equipment such as paper making machines and rolling mills. Within the range described, the filterability as defined is not dependent on the viscosity of the oil.
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This document specifies a procedure to determine the consistency of a metal-saponified lubricating grease by an oscillatory rheometer. This test method is applicable for fresh, as well as used, lubricating greases where only small quantities of the grease are present and the worked penetration that is usually used cannot be determined due to the small quantity. The determined calibration is only valid for metal-saponified lubricating greases like lithium, lithium-calcium and, also, lithium- and calcium complex. The method described in this document is applicable for lubricating greases with NLGI grades 00, 0, 1, 2 and 3 according to ISO 6743-99.
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This document specifies a test method to determine the flow point of lubricating greases using an oscillatory rheometer with a parallel-plate measuring system. It also specifies a test method to evaluate further specific viscoelastic properties of lubricating greases.
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This document provides testing procedures for evaluating proppants used in hydraulic fracturing and gravel packing operations.
NOTE Proppants mentioned in this document refer to sand, ceramic, resin-coated, gravel packing proppants, and other materials used for hydraulic fracturing and gravel packing operations.
This document supplements API Std 19C, 2nd edition (2018), the requirements of which are applicable with the exceptions specified in this document.
This document provides consistent methodology for testing performed on hydraulic fracturing and/or gravel packing proppants.
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This document describes a procedure for the determination of the mass percentage of sulfated ash from unused lubricating oils containing additives and from additive concentrates used in compounding. These additives usually contain one or more of the following metals: barium, calcium, magnesium, zinc, potassium, sodium and tin. The elements sulfur, phosphorus and chlorine can also be present in combined form. This document is also applicable to fatty acid methyl esters (FAME).
This test method is applicable to products having sulphated ash contents in the range mass fraction of 0,005 % to 25,00 %. Application of this procedure to sulfated ash levels below a mass fraction of 0,02 % is restricted to oil products containing ashless additives.
This document is not intended for the analysis of used engine oils containing lead, nor for the analysis of non-additive lubricating oils, for which ISO 6245 is suitable.
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This document describes a procedure for the determination of the mass percentage of sulfated ash from unused lubricating oils containing additives and from additive concentrates used in compounding. These additives usually contain one or more of the following metals: barium, calcium, magnesium, zinc, potassium, sodium and tin. The elements sulfur, phosphorus and chlorine can also be present in combined form. This document is also applicable to fatty acid methyl esters (FAME). This test method is applicable to products having sulphated ash contents in the range mass fraction of 0,005 % to 25,00 %. Application of this procedure to sulfated ash levels below a mass fraction of 0,02 % is restricted to oil products containing ashless additives. This document is not intended for the analysis of used engine oils containing lead, nor for the analysis of non-additive lubricating oils, for which ISO 6245 is suitable.
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This document specifies the minimum requirements for lubricants for turbines, as delivered. It is intended to be used in conjunction with ISO 6743-5.
This document specifies the requirements for a wide variety of lubricants for the lubrication of most types of turbines for power generation, including steam turbines, gas turbines, single shaft combined cycle turbines with common lubrication system and hydraulic turbines. This document does not specify the requirements for lubricants for wind turbines, which are covered in ISO 12925-1.
The following lubricants are considered:
- mineral oils, of either API groups I, II, II+, III, including group III from GTL (gas to liquid) process, and III+. Some API groups II and III are suitable for high temperature gas turbines;
- synthetic lubricants, esters (API group V) and polyalphaolefins (API group IV), intended for high temperature gas turbines;
- synthetic lubricants, esters (API group V) and polyalphaolefins (API group IV), environmentally acceptable for use in hydraulic turbines;
- fire resistant phosphate-ester type lubricants.
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This standard specifies requirements and methods of test for lubricants to be used in gas appliances of all categories including auxilliary equipment mounted or intended to be mounted on such appliances and which may be in contact with combustible gases, except those designed for use in industrial processes.
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This document establishes the specifications relative to family C (gears) for lubricants, industrial oils and related products of class L (see ISO 6743-6). This document deals only with lubricants for enclosed gear systems. Lubricants for open gears and greases for gears (enclosed or open) are covered by the other parts of the ISO 12925 series (i.e. ISO 12925-2 and ISO 12925-3). This document is intended to be read in conjunction with ISO 6743-6. The following categories specified in ISO 6743-6 are covered by this document: CKB, CKC, CKD, CKE, CKSMP, CKTG, CKES, CKPG, CKPR, CSPG, CSPR, CTPG and CTPR. Detailed information about the different types of gear, and lubricants, and their selection for gearbox design and service conditions can be found in ISO/TR 18792.
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SIGNIFICANCE AND USE
5.1 This test method measures a lubricant's ability to protect hypoid final drive axles from abrasive wear, adhesive wear, plastic deformation, and surface fatigue when subjected to low-speed, high-torque conditions. Lack of protection can lead to premature gear or bearing failure, or both.
5.2 This test method is used, or referred to, in specifications and classifications of rear-axle gear lubricants such as:
5.2.1 Specification D7450.
5.2.2 American Petroleum Institute (API) Publication 1560.
5.2.3 SAE J308.
5.2.4 SAE J2360.
SCOPE
1.1 This test method, commonly referred to as the L-37-1 test, describes a test procedure for evaluating the load-carrying capacity, wear performance, and extreme pressure properties of a gear lubricant in a hypoid axle under conditions of low-speed, high-torque operation.3
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.2.1 Exceptions—Where there is no direct SI equivalent such as National Pipe threads/diameters, tubing size, or where there is a sole source supply equipment specification.
1.2.1.1 The drawing in Annex A6 is in inch-pound units.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are provided in 7.2 and 10.1.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This document specifies the minimum requirements for lubricants for turbines, as delivered. It is intended to be used in conjunction with ISO 6743-5. This document specifies the requirements for a wide variety of lubricants for the lubrication of most types of turbines for power generation, including steam turbines, gas turbines, single shaft combined cycle turbines with common lubrication system and hydraulic turbines. This document does not specify the requirements for lubricants for wind turbines, which are covered in ISO 12925-1. The following lubricants are considered: - mineral oils, of either API groups I, II, II+, III, including group III from GTL (gas to liquid) process, and III+. Some API groups II and III are suitable for high temperature gas turbines; - synthetic lubricants, esters (API group V) and polyalphaolefins (API group IV), intended for high temperature gas turbines; - synthetic lubricants, esters (API group V) and polyalphaolefins (API group IV), environmentally acceptable for use in hydraulic turbines; - fire resistant phosphate-ester type lubricants.
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SIGNIFICANCE AND USE
5.1 This test method was developed to evaluate automotive lubricant’s effect on controlling valve-train wear and overall engine wear for overhead camshaft engines with direct acting bucket lifters.
5.2 Average intake lifter volume loss is used as a measure of an oil’s ability to prevent valve-train wear.
5.3 End-of-test oil iron concentration is used as a measure of an oil’s ability to prevent overall engine wear.
Note 2: This test method may be used for engine oil specifications such as API SP, and ILSAC GF- 6A, and GF-6B.
SCOPE
1.1 This test method measures the ability of an engine crankcase oil to control valve-train wear in spark-ignition engines at low operating temperature conditions. This test method is designed to simulate extended engine cyclic vehicle operation. The Sequence IVB Test Method uses a Toyota 2NR-FE water cooled, 4 cycle, in-line cylinder, 1.5 L engine. The primary result is bucket lifter wear. Secondary results include cam lobe nose wear and measurement of iron (Fe) wear metal concentration in the used engine oil. Other determinations such as fuel dilution of the crankcase oil, non-ferrous wear metal concentrations, total fuel consumption, and total oil consumption, can be useful in the assessment of the validity of the test results.2
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.2.1 Exceptions—Where there is no direct SI equivalent such as pipe fittings, tubing, NPT screw threads/diameters, or single source equipment specified.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are provided throughout this document as necessary in each particular section.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method was developed to evaluate the viscosity increase and soot concentration (loading) performance of engine oils in turbocharged and intercooled four-cycle diesel engines equipped with EGR. Obtain results from used oil analysis.
5.2 The test method can be used for engine oil specification acceptance when all details of the procedure are followed.
SCOPE
1.1 This test method covers an engine test procedure for evaluating diesel engine oils for performance characteristics in a diesel engine equipped with exhaust gas recirculation, including viscosity increase and soot concentrations (loading).2 This test method is commonly referred to as the Mack T-11.
1.1.1 This test method also provides the procedure for running an abbreviated length test, which is commonly referred to as the T-11A. The procedures for the T-11A are identical to the T-11 with the exception of the items specifically listed in Annex A7. Additionally, the procedure modifications listed in Annex A7 refer to the corresponding section of the T-11 procedure.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.2.1 Exceptions—Where there is no direct SI equivalent such as screw threads, National Pipe Threads/diameters, tubing size, or where there is a sole source supply equipment specification.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See Annex A6 for specific safety hazards.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method is used to evaluate automotive engine oils for protection of engines against bearing weight loss.
5.2 This test method is also used to evaluate the SIG capabilities of multiviscosity-graded oils.
5.3 Correlation of test results with those obtained in automotive service has not been established.
5.4 Use—The Sequence VIII test method is useful for engine oil specification acceptance. It is used in specifications and classifications of engine lubricating oils, such as the following:
5.4.1 Specification D4485.
5.4.2 API Publication 1509 Engine Oil Licensing and Certification System.7
5.4.3 SAE Classification J304.
SCOPE
1.1 This test method covers the evaluation of automotive engine oils (SAE grades 0W, 5W, 10W, 20, 30, 40, and 50, and multi-viscosity grades) intended for use in spark-ignition gasoline engines. The test procedure is conducted using a carbureted, spark-ignition Cooperative Lubrication Research (CLR) Oil Test Engine (also referred to as the Sequence VIII test engine in this test method) run on unleaded fuel. An oil is evaluated for its ability to protect the engine and the oil from deterioration under high-temperature and severe service conditions. The test method can also be used to evaluate the viscosity stability of multi-viscosity-graded oils. Companion test methods used to evaluate engine oil performance for specification requirements are discussed in the latest revision of Specification D4485.
1.2 Correlation of test results with those obtained in automotive service has not been established. Furthermore, the results obtained in this test are not necessarily indicative of results that will be obtained in a full-scale automotive spark-ignition or compression-ignition engine, or in an engine operated under conditions different from those of the test. The test can be used to compare one oil with another.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3.1 Exceptions—The values stated in inch-pounds for certain tube measurements, screw thread specifications, and sole source supply equipment are to be regarded as standard.
1.3.1.1 The bearing wear in the text is measured in grams and described as weight loss, a non-SI term.
1.4 This test method is arranged as follows:
Subject
Section
Introduction
Scope
1
Referenced Documents
2
Terminology
3
Summary of Test Method
4
Before Test Starts
4.1
Power Section Installation
4.2
Engine Operation (Break-in)
4.3
Engine Operation (Test/Samples)
4.4
Stripped Viscosity
4.5
Test Completion (BWL)
4.6
Significance and Use
5
Evaluation of Automotive oils
5.1
Stay in Grade Capabilities
5.2
Correlation of Results
5.3
Use
5.4
Apparatus
6
Test Engineering, Inc.
6.1
Fabricated or Specially Prepared Items
6.2
Instruments and Controls
6.3
Procurement of Parts
6.4
Reagents and Materials
7
Reagents
7.1
Cleaning Materials
7.2
Expendable Power Section-Related Items
7.3
Power Section Coolant
7.4
Reference Oils
7.5
Test Fuel
7.6
Test Oil Sample Requirements
8
Selection
8.1
Inspection
8.2
Quantity
8.3
Preparation of Apparatus
9
Test Stand Preparation
9.1
Conditioning Test Run on Power Section
9.2
General Power Section Rebuild Instructions
9.3
Reconditioning of Power Section After Each Test
9.4
Calibration
10
Power Section and Test Stand Calibration
10.1
Instrumentation Calibration
10.2
Calibration of AFR Measurement Equipment
10.3
Calibration of Torque Wrenches
10.4
Engin...
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SIGNIFICANCE AND USE
5.1 Fluid analysis is one of the pillars in determining fluid and equipment conditions. The results of fluid analysis are used for planning corrective maintenance activities, if required.
5.2 The objective of a proper fluid sampling process is to obtain a representative fluid sample from critical location(s) that can provide information on both the equipment and the condition of the lubricant or hydraulic fluid.
5.3 The additional objective is to reduce the probability of outside contamination of the system and the fluid sample during the sampling process.
5.4 The intent of this guide is to help users in obtaining representative and repeatable fluid samples in a safe manner while preventing system and fluid sample contamination.
SCOPE
1.1 This guide is applicable for collecting representative fluid samples for the effective condition monitoring of steam and gas turbine lubrication and generator cooling gas sealing systems in the power generation industry. In addition, this guide is also applicable for collecting representative samples from power generation auxiliary equipment including hydraulic systems.
1.2 The fluid may be used for lubrication of turbine-generator bearings and gears, for sealing generator cooling gas as well as a hydraulic fluid for the control system. The fluid is typically supplied by dedicated pumps to different points in the system from a common or separate reservoirs. Some large steam turbine lubrication systems may also have a separate high pressure pump to allow generation of a hydrostatic fluid film for the most heavily loaded bearings prior to rotation. For some components, the lubricating fluid may be provided in the form of splashing formed by the system components moving through fluid surfaces at atmospheric pressure.
1.3 Turbine lubrication and hydraulic systems are primarily lubricated with petroleum based fluids but occasionally also use synthetic fluids.
1.4 For large lubrication and hydraulic turbine systems, it may be beneficial to extract multiple samples from different locations for determining the condition of a specific component.
1.5 The values stated in SI units are regarded as standard.
1.5.1 The values given in parentheses are for information only.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Some oils are formulated with organo-metallic additives, which act, for example, as detergents, antioxidants, and antiwear agents. Some of these additives contain one or more of these elements: calcium, phosphorus, sulfur, and zinc. This test method provides a means of determining the concentrations of these elements, which in turn provides an indication of the additive content of these oils.
5.2 Several additive elements and their compounds are added to the lubricating oils to give beneficial performance (Table 2).
5.3 This test method is primarily intended to be used at a manufacturing location for monitoring of additive elements in lubricating oils. It can also be used in central and research laboratories.
SCOPE
1.1 This test method covers the quantitative determination of additive elements in unused lubricating oils, as shown in Table 1.
1.2 This test method is limited to the use of energy dispersive X-ray fluorescence (EDXRF) spectrometers employing an X-ray tube for excitation in conjunction with the ability to separate the signals of adjacent elements.
1.3 This test method uses interelement correction factors calculated from empirical calibration data.
1.4 This test method is not suitable for the determination of magnesium and copper at the concentrations present in lubricating oils.
1.5 This test method excludes lubricating oils that contain chlorine or barium as an additive element.
1.6 This test method can be used by persons who are not skilled in X-ray spectrometry. It is intended to be used as a routine test method for production control analysis.
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations to use.
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The life cycle and cleanliness of a recirculating steel mill rolling oil dispersion is affected by the amount of iron present. This iron consists mainly of iron from acid pickling residues and iron from attrition of the steel sheet or rolls during cold rolling. In sampling rolling oils for total iron it is difficult to prevent adherence of iron containing sludge to the sample container. Thus, the accuracy of a total iron determination from an aliquot sample is suspect. This practice provides a means for ensuring that all iron contained in a sample is included in the analysis.
5.2 Although less significant, the ash content is still an essential part of the procedure for obtaining a total iron analysis. Generally, the ash will be mostly iron, and in many cases, could be used as a substitute for total iron in determining when to change the dispersion.
FIG. 1 Possible Holding Fixture and Assembly System
SCOPE
1.1 This test method describes a procedure for sampling and testing dispersions of rolling oils in water from operating steel rolling mills for determination of ash and total iron content. Its purpose is to provide a test method such that a representative sample may be taken and phenomenon such as iron separation, fat-emulsion separation, and so forth, do not contribute to analytical error in determination of ash and total iron.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Sections 7 and 8.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Final drive axles are often subjected to severe service where they encounter high speed shock torque conditions, characterized by sudden accelerations and decelerations. This severe service can lead to scoring distress on the ring gear and pinion surface. This test method measures anti-scoring properties of final drive lubricants.
5.2 This test method is used or referred to in the following documents:
5.2.1 American Petroleum Institute (API) Publication 1560.7
5.2.2 SAE J308 and SAE J2360.
SCOPE
1.1 This test method covers the determination of the anti-scoring properties of final drive axle lubricating oils when subjected to high-speed and shock conditions. This test method is commonly referred to as the L-42 test.2
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.2.1 Exceptions—SI units are provided for all parameters except where there is no direct equivalent such as the units for screw threads, National Pipe Threads/diameters, tubing size, and single source equipment suppliers.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning information is given in Sections 4 and 7.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method was developed to evaluate the oxidation resistance performance of engine oils in turbocharged and intercooled four-cycle diesel engines equipped with EGR and running on ultra-low sulfur diesel fuel. Obtain results from used oil analysis and component measurements before and after test.
5.2 The test method may be used for engine oil specification acceptance when all details of the procedure are followed.
SCOPE
1.1 This test method covers an engine test procedure for evaluating diesel engine oils for oxidation performance characteristics in an engine equipped with exhaust gas recirculation and running on ultra-low sulfur diesel fuel.2 This test method is commonly referred to as the Volvo T-13.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.2.1 Exception—Where there is no direct SI equivalent, such as the units for screw threads, National Pipe Threads/diameters, tubing size, and single source supply equipment specifications.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See Annex A10 for specific safety precautions.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The linear flame propagation rate of a sample is a property that is relevant to the overall assessment of the flammability or relative ignitability of fire resistance lubricants and hydraulic fluids. It is intended to be used as a bench-scale test for distinguishing between the relative resistance to ignition of such materials. It is not intended to be used for the evaluation of the relative flammability of flammable, extremely flammable, or volatile fuels, solvents, or chemicals.
SCOPE
1.1 This test method covers the determination of the linear flame propagation rates of lubricating oils and hydraulic fluids supported on the surfaces of and impregnated into ceramic fiber media. Data thus generated are to be used for the comparison of relative flammability.
1.2 This test method should be used to measure and describe the properties of materials, products, or assemblies in response to heat and flame under controlled laboratory conditions and should not be used to describe or appraise the fire hazard or fire risk of materials, products, or assemblies under actual fire conditions. However, results of this test method may be used as elements of fire risk which takes into account all of the factors that are pertinent to an assessment of the fire hazard of a particular end use.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The composition of the oil included in rubber compounds has a large effect on the characteristics and uses of the compounds. The determination of the saturates, aromatics, and polar compounds is a key analysis of this composition.
5.2 The determination of the saturates, aromatics, and polar compounds and further analysis of the fractions produced is often used as a research method to aid understanding of oil effects in rubber and other uses.
SCOPE
1.1 This test method covers a procedure for classifying oil samples of initial boiling point of at least 260 °C (500 °F) into the hydrocarbon types of polar compounds, aromatics and saturates, and recovery of representative fractions of these types. This classification is used for specification purposes in rubber extender and processing oils.
Note 1: See Test Method D2226.
1.2 This test method is not directly applicable to oils of greater than 0.1 % by mass pentane insolubles. Such oils can be analyzed after removal of these materials, but precision is degraded (see Appendix X1).
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in 6.1, Section 7, A1.4.1, and A1.5.5.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 This practice is intended to assist the user, in particular the power-plant operations and maintenance departments, to maintain effective lubrication of all parts of the turbine and guard against the onset of problems associated with oil degradation and contamination. The values of the various test parameters mentioned in this practice are purely indicative. In fact, for proper interpretation of the results, many factors, such as type of equipment, operation workload, design of the lubricating oil circuit, and top-up level, should be taken into account.
SCOPE
1.1 This practice covers the requirements for the effective monitoring of mineral turbine oils in service in steam and gas turbines, as individual or combined cycle turbines, used for power generation. This practice includes sampling and testing schedules to validate the condition of the lubricant through its life cycle and by ensuring required improvements to bring the present condition of the lubricant within the acceptable targets. This practice is not intended for condition monitoring of lubricants for auxiliary equipment; it is recommended that the appropriate practice be consulted (see Practice D6224).
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This document specifies the requirements for environmentally acceptable hydraulic fluids and is intended for hydraulic systems, particularly hydraulic fluid power systems. The purpose of this document is to provide guidance and requirements for suppliers and users of environmentally acceptable hydraulic fluids, and for the direction of original equipment manufacturers of hydraulic systems.
This document stipulates the requirements for environmentally acceptable hydraulic fluids at the time of delivery.
Classification of fluids used in hydraulic application is defined in ISO 6743-4. This document encompasses the four categories of environmentally acceptable fluids covered by ISO 6743-4, namely HETG (triglycerides), HEPG (polyglycols), HEES (synthetic esters) and HEPR (polyalphaolefins and other synthetic hydrocarbons).
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SIGNIFICANCE AND USE
5.1 This test method is intended for use in analytical laboratories including onsite in-service oil analysis laboratories.
5.2 Hard particles in lubricating or fluid power systems have a detrimental effect on the system as they cause operating components to wear and also accelerate the degradation of the oil. Hard particles in the oil originate from a variety of sources including generation from within an operating fluid system or contamination, which may occur during the storage and handling of new oils or via ingress into an operating fluid system.
5.3 High levels of contaminants can cause filter blockages and hard particles can have a serious impact on the life of pumps, pistons, gears, bearings, and other moving parts by accelerating wear and erosion.
5.4 Particle count results can be used to aid in assessing the capability of the filtration system responsible for cleaning the fluid, determining if off-line recirculating filtration is needed to clean up the fluid system, or aiding in the decision of whether or not a fluid change is required.
5.5 To accurately measure hard particle contamination levels, it is necessary to negate the particle counts contributed by the presence of small levels of free water. This method includes a process by which this can be accomplished using a water-masking diluent technique whereby water droplets of a size below the target level are finely distributed.
5.6 Certain additives or additive by-products that are semi-insoluble or insoluble in oil, namely the polydimethylsiloxane defoamant additive and oxidation by-products, are known to cause light scattering in automatic particle counters, which in turn causes falsely high counts. These and similar materials are commonly termed “soft particles” (see 3.2.4) and are not known to directly increase wear and erosion within an operating system. The contribution of these particles to the particle size cumulative count is negated with this method.
5.7 The use of dilution i...
SCOPE
1.1 This test method covers the determination of particle concentration and particle size distribution in new and in-service oils used for lubrication and hydraulic purposes.
1.2 Particles considered are in the range from 4 µm (c) to 200 µm (c) with the upper limit being dependent on the specific automatic particle counter being used.
Note 1: For the purpose of this test method, water droplets not masked by the diluent procedure are detected as particles, and agglomerated particles are detected and reported as a single larger particle.
Note 2: The subscript (c) is used to denote that the apparatus has been calibrated in accordance with ISO 11171. This subscript (c) strictly only applies to particles up to 50 µm.
1.3 Lubricants that can be analyzed by this test method are categorized as petroleum products or synthetic based products, such as: polyalpha olefin, polyalkylene glycol, or phosphate ester. Applicable viscosity range is up to 1000 mm2/s at 40 °C. This procedure may be appropriate for other petroleum and synthetic based lubricants not included in the precision statement.
1.4 Samples containing visible particles may not be suitable for analysis using this test method.
1.5 Samples that are opaque after dilution are not suitable for analysis using this test method.
1.6 The test method is specific to automatic particle counters that use the light extinction principle and are calibrated according to the latest revision of ISO 11171.
1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.9 This international standard was d...
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SIGNIFICANCE AND USE
5.1 Knowledge of the water content of lubricating oils, additives, and similar products is important in the manufacture, purchase, sale, transfer, or use of such petroleum products to help in predicting their quality and performance characteristics.
5.2 For lubricating oils, the presence of water can lead to premature corrosion and wear, an increase in the debris load resulting in diminished lubrication and premature plugging of filters, impedance to the effect of additives, and undesirable support of deleterious bacterial growth.
SCOPE
1.1 This test method covers the quantitative determination of water in new and in-service lubricating oils and additives in the range of 10 mg/kg to 100 000 mg/kg (0.001 wt./wt. to 10 % wt./wt.) using a relative humidity (RH) sensor. Methanol, acetonitrile, and other compounds are known to interfere with this test method.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 Warning—Samples tested in this test method can be flammable, explosive, and toxic. Use caution when handling them before and after testing.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method can be used to determine anti-wear properties and coefficient of friction of greases in order to prevent “fretting” wear under linear oscillation with associated low strokes and high Hertzian contact pressures at selected temperatures and loads specified for use in applications in which induced, high-speed vibrational motions are present for extended periods of time. It has found application as a screening test for grease lubricants used in ball and roller bearings, roller or ball screw (spindle) drives or side shaft systems (Tripode or Rzeppa type) for example, so-called constant velocity (CV) joints. Users of this test method should determine whether results correlate with field performance or other applications.
SCOPE
1.1 This test method covers a procedure for determining the lubricating action of greases in order to prevent “fretting” wear under linear oscillation with associated low strokes and high Hertzian contact pressures under high-frequency linear-oscillation motion using the SRV test machine. By performing additional, nonmandatory extreme-pressure tests in accordance with Test Method D5706, the test grease should be shown to be able to withstand a Hertzian contact pressure of at least 2200 MPa without adhesive failure.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This document specifies a method for evaluating the change of consistency of a grease when it is submitted to working and prolonged working in presence of 10 % of water.
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SCOPE
1.1 This terminology standard covers the compilation of terminology developed by Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants, except that it does not include terms/definitions specific only to the standards in which they appear.
1.1.1 The terminology, mostly definitions, is unique to petroleum, petroleum products, lubricants, and certain products from biomass and chemical synthesis. Meanings of the same terms outside of applications to petroleum, petroleum products, and lubricants can be found in other compilations and in dictionaries of general usage.
1.1.2 The terms/definitions exist in two places: (1) in the standards in which they appear and (2) in this compilation.
1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This laboratory test method can be used to quickly determine extreme pressure properties of lubricating greases at selected temperatures specified for use in applications where high-speed vibrational or start-stop motions are present with high Hertzian point contact. This test method has found wide application in qualifying lubricating greases used in constant velocity joints of front-wheel-drive automobiles. Users of this test method should determine whether results correlate with field performance or other applications.
SCOPE
1.1 This test method covers a procedure for determining extreme pressure properties of lubricating greases under high-frequency linear-oscillation motion using the SRV test machine. This test method can also be used for evaluating extreme pressure properties of lubricating fluid.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SCOPE
1.1 Significance and Determination of Viscosity—The purpose of this guide is to provide sufficient knowledge for a person with some technical background in lubrication or condition monitoring from which they can determine the best choice for measuring viscosity of an in-service oil. Such information from this guide should enable the user to engage in productive discussions with colleagues, service providers, managers, and service personnel about obtaining and using information on and from viscosity. There are a number of different approaches to viscometric measurement, and this guide is intended to be a helpful resource in selecting the most appropriate viscometric approach to gain information for the in-service fluid.
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 This test method measures the net change in pressure resulting from consumption of oxygen by oxidation and gain in pressure due to formation of volatile oxidation by-products. This test method may be used for quality control to indicate batch-to-batch uniformity. It predicts neither the stability of greases under dynamic service conditions, nor the stability of greases stored in containers for long periods, nor the stability of films of greases on bearings and motor-parts. It should not be used to estimate the relative oxidation resistance of different grease types.
SCOPE
1.1 This test method determines resistance of lubricating greases to oxidation when stored statically in an oxygen atmosphere in a sealed system at an elevated temperature under conditions of test.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.2.1 Exception—Pressure measurement appears in kPa with psi provided for information only.
1.2.2 Exception—In Fig. A1.1, A1.1, and Appendix X1, all dimensions are in millimeters, with inches provided in parentheses for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements see Sections 6 and 7.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method can be used to determine antiwear properties and coefficient of friction of EP lubricating oils at selected temperatures and loads specified for use in applications in which high-speed vibrational or start-stop motions are present for extended periods of time under initial high Hertzian point contact pressures. It has found application as a screening test for lubricants used in gear or cam/follower systems. Users of this test method should determine whether results correlate with field performance or other applications.
SCOPE
1.1 This test method covers an extreme pressure (EP) lubricating oil's coefficient of friction and its ability to protect against wear when subjected to high-frequency, linear oscillation motion. The procedure is identical to that described in DIN 51834.
1.2 This test method can also be used to determine the ability of a non-EP lubricating oil to protect against wear and its coefficient of friction under similar test conditions.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 A petroleum products, liquid fuels, and lubricants testing laboratory plays a crucial role in product quality management and customer satisfaction. It is essential for a laboratory to provide quality data. This document provides guidance for establishing and maintaining a quality management system in a laboratory.
4.1.1 The word ‘customer’ can refer to both customers internal and external to the laboratory or organization.
SCOPE
1.1 This practice covers the establishment and maintenance of the essentials of a quality management system in laboratories engaged in the analysis of petroleum products, liquid fuels, and lubricants. It is designed to be used in conjunction with Practice D6299.
Note 1: This practice is based on the quality management concepts and principles advocated in ANSI/ISO/ASQ Q9000 standards, ISO/IEC 17025, ASQ Manual,2 and ASTM standards such as D3244, D4182, D4621, D6299, D6300, D7372, E29, E177, E456, E548, E882, E994, E1301, E1323, STP 15D,3 and STP 1209.4
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory requirements prior to use.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Periodic sampling and analysis of lubricants have long been used as a means to determine overall machinery health. Atomic emission (AE) and atomic absorption (AA) spectroscopy are often employed for wear metal analysis (for example, Test Method D5185). A number of physical property tests complement wear metal analysis and are used to provide information on lubricant condition (for example, Test Methods D445, D2896, and D6304). Molecular analysis of lubricants and hydraulic fluids by FT-IR spectroscopy produces direct information on molecular species of interest, including additives, fluid breakdown products and external contaminants, and thus complements wear metal and other analyses used in a condition monitoring program (1, 2-6).
SCOPE
1.1 This practice covers the use of FT-IR in monitoring additive depletion, contaminant buildup and base stock degradation in machinery lubricants, hydraulic fluids and other fluids used in normal machinery operation. Contaminants monitored include water, soot, ethylene glycol, fuels and incorrect oil. Oxidation, nitration and sulfonation of base stocks are monitored as evidence of degradation. The objective of this monitoring activity is to diagnose the operational condition of the machine based on fault conditions observed in the oil. Measurement and data interpretation parameters are presented to allow operators of different FT-IR spectrometers to compare results by employing the same techniques.
1.2 This practice is based on trending and distribution response analysis from mid-infrared absorption measurements. While calibration to generate physical concentration units may be possible, it is unnecessary or impractical in many cases. Warning or alarm limits (the point where maintenance action on a machine being monitored is recommended or required) can be determined through statistical analysis, history of the same or similar equipment, round robin tests or other methods in conjunction with correlation to equipment performance. These warning or alarm limits can be a fixed maximum or minimum value for comparison to a single measurement or can also be based on a rate of change of the response measured (1) .2 This practice describes distributions but does not preclude using rate-of-change warnings and alarms.
Note 1: It is not the intent of this practice to establish or recommend normal, cautionary, warning or alert limits for any machinery. Such limits should be established in conjunction with advice and guidance from the machinery manufacturer and maintenance group.
1.3 Spectra and distribution profiles presented herein are for illustrative purposes only and are not to be construed as representing or establishing lubricant or machinery guidelines.
1.4 This practice is designed as a fast, simple spectroscopic check for condition monitoring of in-service lubricants and can be used to assist in the determination of general machinery health through measurement of properties observable in the mid-infrared spectrum such as water, oil oxidation, and others as noted in 1.1. The infrared data generated by this practice is typically used in conjunction with other testing methods. For example, infrared spectroscopy cannot determine wear metal levels or any other type of elemental analysis. The practice as presented is not intended for the prediction of lubricant physical properties (for example, viscosity, total base number, total acid number, etc.). This practice is designed for monitoring in-service lubricants and can aid in the determination of general machinery health and is not designed for the analysis of lubricant composition, lubricant performance or additive package formulations.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of t...
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SIGNIFICANCE AND USE
5.1 Many web materials do not convey satisfactorily in manufacture or work, or both, as intended in service unless their surface contains a very thin layer of lubricant in the form of a wax, particulate, thin film coating, or fluid. It is often very expensive and time consuming to use surface chemical analysis techniques to quantify the presence of these films. A simple friction test like this one performs this function.
5.2 This test has been used for over twenty years to detect the presence of lubricants on the surface of photographic films at various stages in manufacture. In this instance the surfaces are lubricated with waxes and this test reliably detects if the wax is present. It is not used to quantify the amount of wax, only if it is present. This test can be used as a quality test to make sure that a lubricant is present. Test samples are normally compared with an unlubricated reference specimen. The coefficient of friction of the test samples is compared with the coefficient of friction of the unlubricated reference specimens to determine if a lubricant is present.
SCOPE
1.1 This test method has been used since 1988 as an ANSI/ISO standard test for determination of lubrication on processed photographic films. Its purpose was to determine the presence of process-surviving lubricants on photographic films. It is the purpose of this test method to expand the applicability of this test method to other flexible webs that may need lubrication for suitable performance. This test measures the breakaway (static) coefficient of friction of a metal rider on the web by the inclined plane method. The objective of the test is to determine if a web surface has a lubricant present or not. It is not intended to assign a friction coefficient to a material. It is not intended to rank lubricants.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 This practice is intended to help users, particularly power plant operators, maintain effective control over their mineral lubricating oils and lubrication monitoring program. This practice may be used to perform oil changes based on oil condition and test results rather than on the basis of service time or calendar time. It is intended to save operating and maintenance expenses.
4.2 This practice is also intended to help users monitor the condition of mineral lubricating oils and guard against excessive component wear, oil degradation, or contamination, thereby minimizing the potential of catastrophic machine problems that are more likely to occur in the absence of such an oil condition monitoring program.
4.3 This practice does not necessarily reference all of the current oil testing technologies and is not meant to preclude the use of alternative instrumentation or test methods that provide meaningful or trendable test data, or both. Some oil testing devices and sensors (typically used for screening oils that will be tested according to standard methods) provide trendable indicators that correlate to water, particulates, and other contaminants but do not directly measure these.
4.4 This practice is intended for mineral oil products, and not for synthetic type of products, with the exception of phosphate esters fluids typically used in power plant control systems.
SCOPE
1.1 This practice covers the requirements for the effective monitoring of mineral oil and phosphate ester fluid lubricating oils in service auxiliary (non-turbine) equipment used for power generation. Auxiliary equipment covered includes gears, hydraulic systems, diesel engines, pumps, compressors, and electrohydraulic control (EHC) systems. It includes sampling and testing schedules and recommended action steps, as well as information on how oils degrade.
Note 1: Other types of synthetic lubricants are sometimes used but are not addressed in this practice because they represent only a small fraction of the fluids in use. Users of these fluids should consult the manufacturer to determine recommended monitoring practices.
1.2 This practice does not cover the monitoring of lubricating oil for steam and gas turbines. Rather, it is intended to complement Practice D4378.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method can be used to determine wear properties and coefficient of friction of lubricating greases at selected temperatures and loads specified for use in applications where high-speed vibrational or start-stop motions are present for extended periods of time under initial high Hertzian point contact pressures. This test method has found application in qualifying lubricating greases used in constant velocity joints of front-wheel-drive automobiles and for lubricating greases used in roller bearings. Users of this test method should determine whether results correlate with field performance or other applications.
SCOPE
1.1 This test method covers a procedure for determining a lubricating grease's coefficient of friction and its ability to protect against wear when subjected to high-frequency, linear-oscillation motion using an SRV test machine at a test load of 200 N, frequency of 50 Hz, stroke amplitude of 1.00 mm, duration of 2 h, and temperature within the range of the test machine, specifically, ambient to 280 °C. Other test loads (10 N to 1200 N for SRVI-model, 10 N to 1400 N for SRVII-model, and 10 N to 2000 N for SRVIII-model), frequencies (5 Hz to 500 Hz) and stroke amplitudes (0.1 mm up to 4.0 mm) can be used, if specified. The precision of this test method is based on the stated parameters and test temperatures of 50 °C and 80 °C. Average wear scar dimensions on ball and coefficient of friction are determined and reported.
Note 1: Optimol Instruments supplies an upgrade kit to allow SRVI/II-machines to operate with 1600 N, if needed.
1.2 This test method can also be used for determining a fluid lubricant's ability to protect against wear and its coefficient of friction under similar test conditions.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This laboratory test method can be used to quickly determine extreme pressure properties of lubricating oils at selected temperatures specified for use in applications where not only high-speed vibrational or start-stop motions are present with high Hertzian point contact. This test method has found wide application in qualifying lubricating oils used in constant velocity joints of front-wheel-drive automobiles, gear-hydraulic circuit, rear axles, gears and engine components. Users of this test method should determine whether results correlate with field performance or other applications.
SCOPE
1.1 This test method covers a procedure for determining extreme pressure properties of lubricating oils for hydraulics, gears, and engines under high-frequency linear-oscillation motion using the SRV test machine.
Note 1: This test method was developed and the international round robin tests were jointly performed with the DIN 51834 working group. This procedure is based on the 2005 revision of Test Method D5706 for greases and differs regarding the stroke length and the cleaning solvent.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
3.1 Personnel from a wide range of disciplines contribute to metalworking fluid management and plant environment health and safety management. Consequently, terms familiar to some stakeholders will be unfamiliar to others.
3.2 This terminology standard provides, in a single document, a compilation of definitions used by personnel involved with both metalworking environment health and safety and fluid management.
3.3 Use of terms as defined in this terminology standard will enable all stakeholders to use metalworking industry terms in the appropriate context, thereby improving interdisciplinary communications.
SCOPE
1.1 This terminology standard provides a compilation of ASTM and non-ASTM consensus definitions of terms used in the metalworking industry.
1.2 This terminology standard does not purport to be an exhaustive lexicon. Rather, it defines terms relevant to metalworking fluid management and metalworking fluid health and safety.
1.3 This terminology standard defines primary metalworking operations, fluid types, and other terms germane to the practice of metalworking fluid management.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The low-temperature, low-shear-rate viscosity of automatic transmission fluids, gear oils, torque and tractor fluids, and industrial and automotive hydraulic oils (see Appendix X4) are of considerable importance to the proper operation of many mechanical devices. Measurement of the viscometric properties of these oils and fluids at low temperatures is often used to specify their acceptance for service. This test method is used in a number of specifications.
5.2 Initially this test method was developed to determine whether an automatic transmission fluid (ATF) would meet OEM low temperature performance criterion originally defined using a particular model viscometer.6, 7 The viscosity range covered in the original ATF performance correlation studies was from less than 1000 mPa·s to more than 60 000 mPa·s. The success of the ATF correlation and the development of this test method has over time been applied to other fluids and lubricants such as gear oils, hydraulic fluids, and so forth.
5.3 Procedures A, B, C, and D of this test method describe how to measure apparent viscosity directly without the errors associated with earlier techniques that extrapolated experimental viscometric data obtained at higher temperatures.
Note 1: Low temperature viscosity values obtained by either interpolation or extrapolation of oils may be subject to errors caused by gelation and other forms of non-Newtonian response to spindle speed and torque.
5.4 Procedures A, B, C, and D; If viscosity measurements are difficult to stabilize or a noticeable decrease in viscosity is seen at a constant speed between an initial measurement made during the 5 s to 10 s after the spindle rotation commences and the stabilized measurement between 60 s and 180 s, then this most likely indicates time-dependent, structural breakdown in the fluid. Some formulated fluid types may form wax structures when soaked at or below a certain low temperature which varies among fluids. The rotating spindle ...
SCOPE
1.1 This test method covers the use of rotational viscometers with an appropriate torque range and specific spindle for the determination of the low-shear-rate viscosity of automatic transmission fluids, gear oils, hydraulic fluids, and some lubricants. This test method covers the viscosity range of 300 mPa·s to 900 000 mPa·s
1.2 This test method was previously titled “Low-Temperature Viscosity of Lubricants Measured by Brookfield Viscometer.” In the lubricant industry, D2983 test results have often been referred to as “Brookfield2 Viscosity” which implies a viscosity determined by this method.
1.3 This test method contains four procedures: Procedure A is used when only an air bath is used to cool samples in preparation for viscosity measurement. Procedure B is used when a mechanically refrigerated programmable liquid bath is used to cool samples in preparation for viscosity measurement. Procedure C is used when a mechanically refrigerated constant temperature liquid bath is used to cool samples by means of a simulated air cell (SimAir)3 Cell in preparation for viscosity measurement. Procedure D automates the determination of low temperature, low-shear-rate viscosity by utilizing a thermoelectrically heated and cooled temperature-controlled sample chamber along with a programmable rotational viscometer.
1.4 There are multiple precision studies for this test method.
1.4.1 The viscosity data used for the precision studies for Procedures A, B, and C covered a range from 300 mPa·s to 170 000 mPa·s at test temperatures of –12 °C, –26 °C, and –40 °C. Appendix X5 includes precision data for –55 °C test temperature and includes samples with viscosities greater 500 000 mPa·s.
1.4.2 The viscosity data used for Procedure D precision study was from 6400 mPa·s to 256 000 mPa·s at test temperatures of –26 °C and –40 °C.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement ar...
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SIGNIFICANCE AND USE
5.1 The bromine number is useful as a measure of aliphatic unsaturation in petroleum samples. When used in conjunction with the calculation procedure described in Annex A2, it can be used to estimate the percentage of olefins in petroleum distillates boiling up to approximately 315 °C (600 °F).
5.2 The bromine number of commercial aliphatic monoolefins provides supporting evidence of their purity and identity.
SCOPE
1.1 This test method3 covers the determination of the bromine number of the following materials:
1.1.1 Petroleum distillates that are substantially free of material lighter than isobutane and that have 90 % distillation points (by Test Method D86) under 327 °C (626 °F). This test method is generally applicable to gasoline (including leaded, unleaded, and oxygenated fuels), kerosine, and distillates in the gas oil range that fall in the following limits:
90 % Distillation Point, °C (°F)
Bromine Number, max3
Under 205 (400)
175
205 to 327 (400 to 626)
10
1.1.2 Commercial olefins that are essentially mixtures of aliphatic mono-olefins and that fall within the range of 95 to 165 bromine number (see Note 1). This test method has been found suitable for such materials as commercial propylene trimer and tetramer, butene dimer, and mixed nonenes, octenes, and heptenes. This test method is not satisfactory for normal alpha-olefins.
Note 1: These limits are imposed since the precision of this test method has been determined only up to or within the range of these bromine numbers.
1.2 The magnitude of the bromine number is an indication of the quantity of bromine-reactive constituents, not an identification of constituents; therefore, its application as a measure of olefinic unsaturation should not be undertaken without the study given in Annex A1.
1.3 For petroleum hydrocarbon mixtures of bromine number less than 1.0, a more precise measure for bromine-reactive constituents can be obtained by using Test Method D2710. If the bromine number is less than 0.5, then Test Method D2710 or the comparable bromine index methods for industrial aromatic hydrocarbons, Test Methods D1492 or D5776 must be used in accordance with their respective scopes. The practice of using a factor of 1000 to convert bromine number to bromine index is not applicable for these lower values of bromine number.
1.4 The values stated in SI units are to be regarded as the standard.
1.4.1 Exception—The values given in parentheses are for information only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Sections 7, 8, and 9.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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