81.060 - Ceramics
ICS 81.060 Details
Ceramics
Keramik
Ceramiques
Keramika
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This document describes a method for determining the etch pit density, which is used to detect dislocations and processing-introduced defects that occur on single-crystal GaN substrates or single-crystal GaN films. It is applicable to the defects specified in ISO 5618-1 from among the defects exposed on the surface of the following types of GaN substrates or films: single-crystal GaN substrate; single-crystal GaN film formed by homoepitaxial growth on a single-crystal GaN substrate; or single-crystal GaN film formed by heteroepitaxial growth on a single-crystal Al2O3, SiC, or Si substrate. It is applicable to defects with an etch pit density of ≤ 7 × 107 cm-2.
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This document gives specifications, test methods, sampling, marking and labelling of porcelain tableware that is used for the preparation and serving of foods.
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This document describes the methods for the determination of void and fibre with specific orientation contents in a polished cross section of continuous fibre-reinforced ceramic matrix composites by image analysis. The methods apply to all ceramic matrix composites with continuous fibre reinforcement: bidirectional (2D) and tridirectional (3D). The methods also apply to carbon-fibre-reinforced carbon matrix composites (also known as: carbon/carbon or C/C). NOTE The result obtained by the method is not volume content but area content.
- Technical specification8 pagesEnglish languagesale 15% off
ISO 26443:2008 specifies a method for the qualitative evaluation of the adhesion of ceramic coatings up to 20 µm thick by indentation with a Rockwell diamond indenter. The formation of cracks after indentation may also reveal cohesive failure. The indentations are made with a Rockwell hardness test instrument.
The method described may also be suitable for evaluating the adhesion of metallic coatings.
The test is not suitable for elastic coatings on hard substrates.
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This document gives a classification of the dislocations and process-induced defects, from among the various surface defects, that occur on single-crystal gallium nitride (GaN) substrates or single-crystal GaN films. It is applicable to the dislocations and process-induced defects exposed on the surface of the following types of GaN substrates or films: — single-crystal GaN substrate; — single-crystal GaN film formed by homoepitaxial growth on a single-crystal GaN substrate; — single-crystal GaN film formed by heteroepitaxial growth on a single-crystal aluminium oxide (Al2O3), silicon carbide (SiC) or silicon (Si) substrate. It is not applicable to defects exposed on the surface if the absolute value of the acute angle between the surface normal and the c-axis of GaN is ≥ 8°.
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This document specifies a method for the qualitative evaluation of the adhesion of ceramic coatings up to 20 μm thick by indentation with a Rockwell diamond indenter. The formation of cracks after indentation can also reveal cohesive failure. The indentations are made with a Rockwell hardness test instrument.
The method described in this document can also be suitable for evaluating the adhesion of metallic coatings.
The test is not suitable for elastic coatings on hard substrates.
- Standard13 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies the test method for the determination of thermal diffusivity from room temperature to at least 1 700 K by the flash method for homogeneous monolithic ceramics with porosity less than 10 %.
Flash methods, like laser flash, are applicable to homogeneous isotropic materials with thermal diffusivity values ranging from 0,1 to 1 000 mm2 s1 within the temperature range from approximately 100 K to 2 300 K.
The method described in Annex G describes how to estimate, on the basis of the thermal diffusivity test, the specific heat capacity and the thermal conductivity of homogeneous monolithic ceramics with porosity less than 10 %.
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This document specifies a method for the qualitative evaluation of the adhesion of ceramic coatings up to 20 μm thick by indentation with a Rockwell diamond indenter. The formation of cracks after indentation can also reveal cohesive failure. The indentations are made with a Rockwell hardness test instrument. The method described in this document can also be suitable for evaluating the adhesion of metallic coatings. The test is not suitable for elastic coatings on hard substrates.
- Standard6 pagesEnglish languagesale 15% off
- Standard7 pagesFrench languagesale 15% off
This document specifies the test method for the determination of thermal diffusivity from room temperature to at least 1 700 K by the flash method for homogeneous monolithic ceramics with porosity less than 10 %.
Flash methods, like laser flash, are applicable to homogeneous isotropic materials with thermal diffusivity values ranging from 0,1 to 1 000 mm2 s-1 within the temperature range from approximately 100 K to 2 300 K.
The method described in Annex G describes how to estimate, on the basis of the thermal diffusivity test, the specific heat capacity and the thermal conductivity of homogeneous monolithic ceramics with porosity less than 10 %.
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This document specifies a method for the determination of interlaminar shear strength at ambient temperature by the compression of a double-notched test piece and a method for the determination of interlaminar shear strength and modulus at ambient temperature by the Iosipescu test. This document applies to all ceramic matrix composites with a continuous fibre reinforcement, having unidirectional (1D), bidirectional (2D) and multidirectional (xD, with x > 2) fibre architecture, where a major part of reinforcements is a stack of plies. This document is applicable to material development, material comparison, quality assurance, characterization, reliability and design data generation. The simpler compression test method of a double-notched test piece is applicable only when the shear strength has to be measured.
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This document specifies methods for the chemical analysis of zirconium oxide powders used as the raw material for fine ceramics.
It stipulates the determination methods of the zirconium, aluminium, barium, calcium, cerium, cobalt, gadolinium, hafnium, iron, magnesium, potassium, silicon, sodium, strontium, titanium and yttrium contents in zirconium oxide powders for fine ceramics. The test sample is decomposed by acid pressure decomposition or alkali fusion. Contents of zirconium and yttrium are determined by using either a precipitation and gravimetric method or an inductively coupled plasma-optical emission spectrometry (ICP-OES) method. Contents of aluminium, barium, calcium, cerium, cobalt, gadolinium, hafnium, iron, magnesium, potassium, silicon, sodium, strontium and titanium are determined by using an ICP-OES method.
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This document specifies methods for the chemical analysis of metal impurities present in silicon dioxide powders used as a raw material for fine ceramics. It stipulates the methods for the determination of metal impurity elements in silicon dioxide powders that are decomposed by acid decomposition. The aluminium, cadmium, calcium, copper, iron, lead, lithium, magnesium, manganese, nickel, potassium, sodium, titanium, zinc and zirconium contents in the test solution are determined by inductively coupled plasma-optical emission spectrometry (ICP-OES).
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This document specifies a substitution measurement method to measure internal quantum efficiency, external quantum efficiency and absorptance of ceramic phosphor powders, which are used in white light-emitting diodes (LEDs) and emit visible light when excited by UV or blue light. In this method, commercially available measurement equipment, such as a fluorescence spectrophotometer or a spectroradiometer equipped with a monochromatic light source as incident light, are used to measure fluorescence spectra for reference materials whose quantum efficiencies and absorptance have been determined using the methods in ISO 23946 and a phosphor material under test.
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This document specifies methods for the chemical analysis of zirconium oxide powders used as the raw material for fine ceramics.
It stipulates the determination methods of the zirconium, aluminium, barium, calcium, cerium, cobalt, gadolinium, hafnium, iron, magnesium, potassium, silicon, sodium, strontium, titanium and yttrium contents in zirconium oxide powders for fine ceramics. The test sample is decomposed by acid pressure decomposition or alkali fusion. Contents of zirconium and yttrium are determined by using either a precipitation and gravimetric method or an inductively coupled plasma–optical emission spectrometry (ICP–OES) method. Contents of aluminium, barium, calcium, cerium, cobalt, gadolinium, hafnium, iron, magnesium, potassium, silicon, sodium, strontium and titanium are determined by using an ICP–OES method.
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This document specifies a test method for the determination of the self-cleaning performance of sheet-form materials that contain an indoor-light-active photocatalyst or have indoor-light-active photocatalytic films on the surface, under indoor lighting environment. This method is used to measure the change of water contact angle under indoor lighting environment, which is one of the indices reflecting the self-cleaning performance of semiconducting photocatalytic materials. This document is not applicable to permeable materials on which water droplets cannot hold and rough materials which obscure water droplets. This document is not applicable to materials of which the changes in the water contact angle due to decomposition of adhered organic matter cannot be evaluated because even if the surface is clean, the water contact angle is remarkably large or the water contact angle cannot be sufficiently increased by attaching organic matter to the surface.
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This document specifies wet chemical and inductively coupled plasma–optical emission spectrometry (ICP–OES)-based methods for the chemical analysis of calcium-phosphate-based powders for non-biomedical applications, such as those in the chemical industry, the treatment of air, water and soil contamination. It stipulates the methods used for the determination of major elements of calcium-phosphate-based powders and their impurities. Calcium-phosphate-based powders are decomposed by acid decomposition. The calcium content is determined using a titration method or an ICP–OES method. The phosphorus content is determined using a precipitation and gravimetric method or an ICP–OES method. Certain impurities, such as aluminium, barium, chromium, copper, iron, magnesium, manganese, nickel, potassium, selenium, silicon, sodium, strontium, titanium and zinc contents, are determined by an ICP–OES method. This document does not include calcium-phosphate-based powders for biomedical applications. The ISO 13779 series characterizes hydroxyapatite powders for biomedical applications using various methods, such as atomic absorption spectrometry (AAS), inductively coupled plasma–mass spectrometry (ICP–MS) and flame atomic absorption spectrometry (FAAS).
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This document specifies light emitting diodes (LED) for light source and radiometers used in the performance evaluation of semiconducting photocatalytic materials under indoor LED lighting environments in a laboratory. Light sources for indoor lighting environments do not include sunlight passing through window glass. This document does not replace ISO 14605.[1] Either document can apply depending on the lighting environment in which the photocatalytic material is used.
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This document specifies the measurement methods for the electronic transport properties of bulk-type thermoelectric materials at room and elevated temperatures. The measurement methods cover the simultaneous determination of Seebeck coefficient and electrical conductivity of bulk-type thermoelectric materials in a temperature range from 300 K to 1 200 K. The measurement methods are applicable to bulk-type thermoelectric materials used for power generation, energy harvesting, cooling and heating, among other things.
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This International Standard ISO 24370 specifies a test method for determining the fracture toughness of monolithic ceramic materials at room temperature by the chevron-notched beam (CNB) method.
This International Standard is applicable to monolithic ceramics and whisker- or particulate-reinforced ceramics that are regarded as macroscopically homogeneous. It is not applicable to continuous-fibre reinforced ceramic composites.
This International Standard is usually applicable to ceramic materials with a fracture toughness less than about 12 MPa(m1/2). The test method is applicable to materials with a flat crack-growth resistance curve and may be applicable to materials with a rising crack-growth resistance curve (R-curve).
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ISO 20509:2003 describes the method of test for determining the oxidation resistance of non-oxide monolithic ceramics, such as silicon nitride, sialon and silicon carbide at high temperatures. This International Standard is designed to provide an assessment of the mass and dimensional changes of test pieces following oxidation at high temperature in an oxidizing atmosphere, and to assess whether oxidation has a significant effect on the subsequent strength. This test method may be used for materials development, quality control, characterization, and design data generation purposes.
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ISO 17092:2005 describes the test method for determining the corrosion resistance of fine ceramics in acid and alkaline solutions, such as sulfuric acid and sodium hydroxide. This International Standard is designed to provide an assessment of the mass changes and dimensional changes of test specimens following the corrosion test immersed in the corrosive liquids, and to assess whether corrosion has a significant effect on the subsequent strength. This test method may be used for development of materials, quality control, characterization, and design-data generation purposes.
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The International Standard specifies the methods for the chemical analysis of fine silicon nitride powders used as the raw material for fine ceramics.
This International Standard stipulates the determination methods of total silicon, total nitrogen, aluminium, iron, calcium, oxygen, carbon, fluorine, and chlorine in fine silicone nitride powders.
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This document specifies the methods for the chemical analysis of fine silicon nitride powders used as the raw material for fine ceramics. It stipulates the determination methods of total silicon, total nitrogen, aluminium, iron, calcium, oxygen, carbon, fluorine, and chlorine in fine silicon nitride powders.
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ISO 24370:2005 specifies a test method for determining the fracture toughness of monolithic ceramic materials at room temperature by the chevron-notched beam (CNB) method.
ISO 24370:2005 is applicable to monolithic ceramics and whisker- or particulate-reinforced ceramics that are regarded as macroscopically homogeneous. It is not applicable to continuous-fibre reinforced ceramic composites.
ISO 24370:2005 is usually applicable to ceramic materials with a fracture toughness less than about 12 megapascal(square root metre). The test method is applicable to materials with a flat crack-growth resistance curve and may be applicable to materials with a rising crack-growth resistance curve (R-curve).
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ISO 17092:2005 describes the test method for determining the corrosion resistance of fine ceramics in acid and alkaline solutions, such as sulfuric acid and sodium hydroxide. This International Standard is designed to provide an assessment of the mass changes and dimensional changes of test specimens following the corrosion test immersed in the corrosive liquids, and to assess whether corrosion has a significant effect on the subsequent strength. This test method may be used for development of materials, quality control, characterization, and design-data generation purposes.
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ISO 20509:2003 describes the method of test for determining the oxidation resistance of non-oxide monolithic ceramics, such as silicon nitride, sialon and silicon carbide at high temperatures. This International Standard is designed to provide an assessment of the mass and dimensional changes of test pieces following oxidation at high temperature in an oxidizing atmosphere, and to assess whether oxidation has a significant effect on the subsequent strength. This test method may be used for materials development, quality control, characterization, and design data generation purposes.
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Fine ceramics (advanced ceramics, advanced technical ceramics) — Test method for determining tensile and shear creep of ceramic adhesive
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This document specifies a method for the qualitative and quantitative determination of the monoclinic phase present in yttria tetragonal zirconia polycrystal (Y-TZP) powders with an yttria content ≤ 6 mol% using X-ray powder diffraction. This method is also applicable for determining the monoclinic phase content in monolithic Y-TZP ceramics with an yttria content of ≤ 6 mol%. NOTE For quantitative determination of the monoclinic phase present in zirconia with a higher content of yttria or another stabilizer (e.g. MgO, CaO), this document can be referenced.
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This document covers the reporting of uniaxial strength data and the estimation of probability distribution parameters for advanced ceramics which fail in a brittle fashion. The failure strength of advanced ceramics is treated as a continuous random variable. Typically, a number of test specimens with well-defined geometry are brought to failure under well-defined isothermal loading conditions. The load at which each specimen fails is recorded. The resulting failure stresses are used to obtain parameter estimates associated with the underlying population distribution.
This document is restricted to the assumption that the distribution underlying the failure strengths is the two-parameter Weibull distribution with size scaling. Furthermore, this document is restricted to test specimens (tensile, flexural, pressurized ring, etc.) that are primarily subjected to uniaxial stress states. Subclauses 6.4 and 6.5 outline methods of correcting for bias errors in the estimated Weibull parameters, and to calculate confidence bounds on those estimates from data sets where all failures originate from a single flaw population (i.e. a single failure mode). In samples where failures originate from multiple independent flaw populations (e.g. competing failure modes), the methods outlined in 6.4 and 6.5 for bias correction and confidence bounds are not applicable.
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This document describes procedures for determination of the compressive behaviour of ceramic matrix composite materials with continuous fibre reinforcement at room temperature. This method applies to all ceramic matrix composites with a continuous fibre reinforcement, uni-directional (1D), bi-directional (2D) and tri-directional (xD, with 2 < x < 3), tested along one principal axis of reinforcement or off axis conditions. This method also applies to carbon-fibre-reinforced carbon matrix composites (also known as carbon/carbon or C/C). Two cases of testing are distinguished: compression between platens and compression using grips.
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This document specifies methods for the chemical analysis of impurities present in aluminium oxide powders used as a raw material for fine ceramics. Aluminium oxide powders are decomposed by acid pressure decomposition, acid decomposition or alkali fusion. The calcium, chromium, copper, iron, magnesium, manganese, potassium, silicon, sodium, titanium, zinc and zirconium contents in the test solution are determined by an inductively coupled plasma-optical emission spectrometer (ICP-OES).
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This document specifies a method for measuring the thermal resistance between a heater chip and a cold plate with the heater chip mounted on a metalized ceramic substrate, imitating a silicon carbide (SiC) high-output power module. This measurement represents an index of the heat dissipation characteristics of a metallized ceramic substrate used in a high-output power module.
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This document covers the reporting of uniaxial strength data and the estimation of probability distribution parameters for advanced ceramics which fail in a brittle fashion. The failure strength of advanced ceramics is treated as a continuous random variable. Typically, a number of test specimens with well-defined geometry are brought to failure under well-defined isothermal loading conditions. The load at which each specimen fails is recorded. The resulting failure stresses are used to obtain parameter estimates associated with the underlying population distribution.
This document is restricted to the assumption that the distribution underlying the failure strengths is the two-parameter Weibull distribution with size scaling. Furthermore, this document is restricted to test specimens (tensile, flexural, pressurized ring, etc.) that are primarily subjected to uniaxial stress states. Subclauses 6.4 and 6.5 outline methods of correcting for bias errors in the estimated Weibull parameters, and to calculate confidence bounds on those estimates from data sets where all failures originate from a single flaw population (i.e. a single failure mode). In samples where failures originate from multiple independent flaw populations (e.g. competing failure modes), the methods outlined in 6.4 and 6.5 for bias correction and confidence bounds are not applicable.
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This document describes procedures for determination of the compressive behaviour of ceramic matrix composite materials with continuous fibre reinforcement at room temperature. This method applies to all ceramic matrix composites with a continuous fibre reinforcement, uni-directional (1D), bi-directional (2D) and tri-directional (xD, with 2 < x < 3), tested along one principal axis of reinforcement or off axis conditions. This method also applies to carbon-fibre-reinforced carbon matrix composites (also known as carbon/carbon or C/C). Two cases of testing are distinguished: compression between platens and compression using grips.
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This document specifies methods for the chemical analysis of fine aluminium nitride powders used as the raw material for fine ceramics.
This document stipulates the determination methods of the aluminium, total nitrogen, boron, calcium, copper, iron, magnesium, manganese, molybdenum, nickel, potassium, silicon, sodium, titanium, tungsten, vanadium, zinc, zirconium, carbon, chlorine, fluorine, and oxygen contents in aluminium nitride powders. The aluminium content is determined by using either an acid pressure decomposition-CyDTA-zinc back titration method or an acid digestion-inductively coupled plasma-optical emission spectrometry (ICP-OES) method. The total nitrogen content is determined by using an acid pressure decomposition-distillation separation-acidimetric titration method, a direct decomposition-distillation separation-acidimetric titration method, or an inert gas fusion-thermal conductivity method. The boron, calcium, copper, iron, magnesium, manganese, molybdenum, nickel, potassium, silicon, sodium, titanium, tungsten, vanadium and zinc contents are determined by using an acid digestion-ICP-OES method or an acid pressure decomposition-ICP-OES method. The sodium and potassium contents are determined via an acid pressure decomposition-flame emission method or an acid pressure decomposition-atomic absorption spectrometry method. The oxygen content is determined by using an inert gas fusion-IR absorption spectrometry method, while that of carbon is determined via a combustion-IR absorption spectrometry method or a combustion-conductometry method. The chlorine and fluorine contents are determined by using a pyrohydrolysation method followed by ion chromatography or spectrophotometry.
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This document specifies the test method to determine the extent to which ceramic powder compacts made of granulated or ungranulated ceramic powders are densified, when they are sintered at a high temperature without the application of any external pressure or external densification force. The test method is applicable to pure oxides, mixtures of oxides and solid solutions, and is also applicable to non-oxides (e.g. carbides, nitrides) that can be sintered under vacuum or constant gas pressure (1 bar or less) to prevent oxidation or decomposition. The test method is not applicable to ceramics that can only be sintered using pressure-assisted sintering techniques such as hot pressing (HP), hot isostatic pressing (HIP), gas pressure sintering (GPS) or spark plasma sintering (SPS). Inorganic sintering additives can be used where their presence is reported.
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This document specifies the test method for the determination of thermal diffusivity from room temperature to at least 1 700 K by the flash method for homogeneous monolithic ceramics with porosity less than 10 %. Flash methods, like laser flash, are applicable to homogeneous isotropic materials with thermal diffusivity values ranging from 0,1 to 1 000 mm2 s-1 within the temperature range from approximately 100 K to 2 300 K. The method described in Annex G describes how to estimate, on the basis of the thermal diffusivity test, the specific heat capacity and the thermal conductivity of homogeneous monolithic ceramics with porosity less than 10 %.
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This document describes procedures for determination of the compressive behaviour of ceramic matrix composite materials with continuous fibre reinforcement at room temperature. This method applies to all ceramic matrix composites with a continuous fibre reinforcement, uni-directional (1D), bi-directional (2D) and tri-directional (xD, with 2 x
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This document specifies the test method to determine the extent to which ceramic powder compacts made of granulated or ungranulated ceramic powders are densified, when they are sintered at a high temperature without the application of any external pressure or external densification force. The test method is applicable to pure oxides, mixtures of oxides and solid solutions, and is also applicable to non-oxides (e.g. carbides, nitrides) that can be sintered under vacuum or constant gas pressure (1 bar or less) to prevent oxidation or decomposition. The test method is not applicable to ceramics that can only be sintered using pressure-assisted sintering techniques such as hot pressing (HP), hot isostatic pressing (HIP), gas pressure sintering (GPS) or spark plasma sintering (SPS). Inorganic sintering additives can be used where their presence is reported.
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This document specifies methods for the chemical analysis of fine aluminium nitride powders used as the raw material for fine ceramics.
This document stipulates the determination methods of the aluminium, total nitrogen, boron, calcium, copper, iron, magnesium, manganese, molybdenum, nickel, potassium, silicon, sodium, titanium, tungsten, vanadium, zinc, zirconium, carbon, chlorine, fluorine, and oxygen contents in aluminium nitride powders. The aluminium content is determined by using either an acid pressure decomposition-CyDTA-zinc back titration method or an acid digestion-inductively coupled plasma-optical emission spectrometry (ICP-OES) method. The total nitrogen content is determined by using an acid pressure decomposition-distillation separation-acidimetric titration method, a direct decomposition-distillation separation-acidimetric titration method, or an inert gas fusion-thermal conductivity method. The boron, calcium, copper, iron, magnesium, manganese, molybdenum, nickel, potassium, silicon, sodium, titanium, tungsten, vanadium and zinc contents are determined by using an acid digestion-ICP-OES method or an acid pressure decomposition-ICP-OES method. The sodium and potassium contents are determined via an acid pressure decomposition-flame emission method or an acid pressure decomposition-atomic absorption spectrometry method. The oxygen content is determined by using an inert gas fusion-IR absorption spectrometry method, while that of carbon is determined via a combustion-IR absorption spectrometry method or a combustion-conductometry method. The chlorine and fluorine contents are determined by using a pyrohydrolysation method followed by ion chromatography or spectrophotometry.
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ISO 21813 specifies methods for the chemical analysis of fine high purity barium titanate powders used as the raw material for fine ceramics.
ISO 21813 stipulates the determination methods of the barium, titanium, aluminium, cadmium, calcium, cobalt, dysprosium, iron, lead, magnesium, manganese, nickel, niobium, potassium, silicon, sodium, strontium, vanadium, zirconium, carbon, oxygen and nitrogen contents in high purity barium titanate powders. The barium and titanium contents, the major elements, are determined by using an acid decomposition-gravimetric method or an acid decomposition-inductively coupled plasma-optical emission spectrometry (ICP-OES) method. The aluminium, cadmium, calcium, chromium, cobalt, dysprosium, iron, lead, magnesium, manganese, nickel, niobium, potassium, silicon, strontium, vanadium and zirconium contents are simultaneously determined via an acid digestion-ICP-OES method. The nitrogen content is determined by using an inert gas fusion-thermal conductivity method, while that of oxygen is determined via an inert gas fusion-IR absorption spectrometry method. Finally, the carbon content is determined using a combustion-IR absorption spectrometry method or a combustion-conductometry method.
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ISO 21813 specifies methods for the chemical analysis of fine high purity barium titanate powders used as the raw material for fine ceramics.
ISO 21813 stipulates the determination methods of the barium, titanium, aluminium, cadmium, calcium, cobalt, dysprosium, iron, lead, magnesium, manganese, nickel, niobium, potassium, silicon, sodium, strontium, vanadium, zirconium, carbon, oxygen and nitrogen contents in high purity barium titanate powders. The barium and titanium contents, the major elements, are determined by using an acid decomposition-gravimetric method or an acid decomposition-inductively coupled plasma-optical emission spectrometry (ICP-OES) method. The aluminium, cadmium, calcium, chromium, cobalt, dysprosium, iron, lead, magnesium, manganese, nickel, niobium, potassium, silicon, strontium, vanadium and zirconium contents are simultaneously determined via an acid digestion-ICP-OES method. The nitrogen content is determined by using an inert gas fusion-thermal conductivity method, while that of oxygen is determined via an inert gas fusion-IR absorption spectrometry method. Finally, the carbon content is determined using a combustion-IR absorption spectrometry method or a combustion-conductometry method.
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This document describes the flash method for the determination of thermal diffusivity of ceramic matrix composites with continuous fibre reinforcement.
In order to conform with the unidimensional heat transfer hypothesis, the experimental conditions are defined such that the material behaves in a homogeneous manner. This involves performing tests in one symmetry axis of the composite.
The method is applicable to materials which are physically and chemically stable during the measurement, and covers the range of temperature from 100 K to 2 800 K. It is suitable for the measurement of thermal diffusivity values in the range 10−4 m2∙s−1 to 10−7 m2∙s−1.
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This document specifies the conditions for the determination of the distribution of strength and rupture strain of ceramic filaments within a multifilament tow at room temperature by performing a tensile test on a multifilament tow.
This document applies to dry tows of continuous ceramic filaments that are assumed to act freely and independently under loading and exhibit linear elastic behaviour up to failure. The outputs of this method are not to be mixed up with the strengths of embedded tows determined by using ISO 24046[1].
[1] Under preparation.
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This document specifies methods for the determination of the apparent solid density, bulk density, apparent porosity and geometric bulk density of fine ceramics, including all ceramic matrix composites.
Two methods are described and are designated as Methods A and B, as follows:
— Method A: Determination of bulk density, apparent solid density and apparent porosity by liquid displacement (Archimedes' method).
NOTE 1 This method is not appropriate for the determination of an apparent porosity greater than 10 %. For materials with higher porosity, the accuracy of the measurement might not be satisfactory. This method might also not give a satisfactory open porosity result if it is less than 0,5 %.
NOTE 2 This method is also not suitable for materials which are known to have an average pore size of greater than 600 µm.
— Method B: Determination of bulk density only, by measurement of geometric dimensions and mass.
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ISO 17138:2014 describes a method for the determination of the flexural strength of ceramic matrix composite materials with continuous fibre reinforcement, under three-point or four-point bend at room temperature. This method applies to all ceramic matrix composites with a continuous fibre reinforcement, unidirectional (1D), bidirectional (2D), and tridirectional xD with (2 < x ≤ 3) as defined in CEN/TR 13233, loaded along one principal axis of reinforcement.
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ISO 17139:2014 describes methods for the determination of linear thermal expansion characteristics of ceramic matrix composite materials up to 2 300 K, and is applicable to 1D, 2D, and nD materials. The method describes general principles of construction, calibration, and operation of the equipment.
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ISO 18608:2017 describes a method for the classification of ceramic matrix composite (CMC) materials with respect to their sensitivity to crack propagation using tensile tests on notched specimens with different notch depths. Two classes of ceramic matrix composite materials can be distinguished: materials whose strength is sensitive to the presence of notches and materials whose strength is not affected. For sensitive materials, this document defines a method for determining equivalent fracture toughness.
The parameter, Keq, is defined as the fracture toughness of a homogeneous material which presents the same sensitivity to crack propagation as the ceramic matrix composite material which is being considered. The definition of the Keq parameter offers the possibility to compare ceramic matrix composite materials with other materials with respect to sensitivity to crack propagation.
For notch insensitive materials, the concept of Keq does not apply.
ISO 18608:2017 applies to all ceramic matrix composites with a continuous fibre reinforcement, unidirectional (1 D), bidirectional (2 D), and tridirectional (x D, where 2 < x ≤ 3), loaded along one principal axis of reinforcement.
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This document specifies a method for the determination of the tensile strength, tensile modulus of elasticity and strain at the maximum force of a resin-impregnated yarn specimen at ambient temperature. This method is applicable to yarns of ceramic fibres that are used as reinforcements in composite materials. The test results obtained by this method are applicable for quality control and comparison of the ceramic fibres. The outputs of this method are not to be mixed up with the strength of filaments derived from tensile tests on dry tows specified in ISO 22459.
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This document specifies terms and associated definitions which are typically used for fine ceramic (advanced ceramic, advanced technical ceramic) materials, products, applications, properties and processes. This document also contains those abbreviated terms which have found general acceptance in scientific and technical literature; they are given together with the corresponding full terms and definitions or descriptions. In this document, terms are defined using the term ‘fine ceramic’. The definitions apply equally to ‘advanced ceramics’ and ‘advanced technical ceramics’, which are considered to be equivalent. This document does not include terms which, though used in the field of fine ceramics, are of a more general nature and are also well known in other fields of technology. NOTE Terms and definitions of a more general nature are available in ASTM C 1145-2019, EN 14232 and JIS R 1600.
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