Fine ceramics (advanced ceramics, advanced technical ceramics) - Methods for chemical analysis of impurities in aluminium oxide powders using inductively coupled plasma-optical emission spectrometry (ISO 3169:2023)

This document specifies methods for the chemical analysis of impurities present in aluminium oxide powders used as a raw material for fine ceramics.
Aluminium oxide powders are decomposed by acid pressure decomposition, acid decomposition or alkali fusion. The calcium, chromium, copper, iron, magnesium, manganese, potassium, silicon, sodium, titanium, zinc and zirconium contents in the test solution are determined by an inductively coupled plasma-optical emission spectrometer (ICP-OES).

Hochleistungskeramik - Verfahren zur chemischen Analyse von Verunreinigungen in Aluminiumoxidpulvern mittels optischer Emissionsspektrometrie mit induktiv gekoppeltem Plasma (ISO 3169:2023)

Céramiques techniques (céramiques avancées, céramiques techniques avancées) - Méthodes d'analyse chimique des impuretés contenues dans les poudres d'oxyde d'aluminium à l'aide de la spectrométrie d'émission optique par plasma à couplage inductif (ISO 3169:2023)

Le présent document spécifie des méthodes d’analyse chimique des impuretés présentes dans les poudres d’oxyde d’aluminium utilisées comme matière première pour les céramiques techniques.
Les poudres d’oxyde d’aluminium sont décomposées par décomposition sous pression en milieu acide, décomposition en milieu acide ou fusion alcaline. Les teneurs en calcium, chrome, cuivre, fer, magnésium, potassium, silicium, sodium, titane, zinc et zirconium dans la solution d’essai sont déterminées par un spectromètre d’émission optique par plasma à couplage inductif (ICP-OES).

Fina keramika (sodobna keramika, sodobna tehnična keramika) - Metode za kemijsko analizo nečistoč v prahu aluminijevega oksida z uporabo induktivno sklopljene plazme v optični emisijski spektrometriji (ISO 3169:2023)

General Information

Status
Published
Public Enquiry End Date
22-Oct-2025
Publication Date
07-Dec-2025
Technical Committee
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
04-Dec-2025
Due Date
08-Feb-2026
Completion Date
08-Dec-2025
Standard
SIST EN ISO 3169:2026
English language
19 pages
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Standards Content (Sample)


SLOVENSKI STANDARD
01-januar-2026
Fina keramika (sodobna keramika, sodobna tehnična keramika) - Metode za
kemijsko analizo nečistoč v prahu aluminijevega oksida z uporabo induktivno
sklopljene plazme v optični emisijski spektrometriji (ISO 3169:2023)
Fine ceramics (advanced ceramics, advanced technical ceramics) - Methods for
chemical analysis of impurities in aluminium oxide powders using inductively coupled
plasma-optical emission spectrometry (ISO 3169:2023)
Hochleistungskeramik - Verfahren zur chemischen Analyse von Verunreinigungen in
Aluminiumoxidpulvern mittels optischer Emissionsspektrometrie mit induktiv
gekoppeltem Plasma (ISO 3169:2023)
Céramiques techniques (céramiques avancées, céramiques techniques avancées) -
Méthodes d'analyse chimique des impuretés contenues dans les poudres d'oxyde
d'aluminium à l'aide de la spectrométrie d'émission optique par plasma à couplage
inductif (ISO 3169:2023)
Ta slovenski standard je istoveten z: EN ISO 3169:2025
ICS:
81.060.30 Sodobna keramika Advanced ceramics
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 3169
EUROPEAN STANDARD
NORME EUROPÉENNE
November 2025
EUROPÄISCHE NORM
ICS 81.060.30
English Version
Fine ceramics (advanced ceramics, advanced technical
ceramics) - Methods for chemical analysis of impurities in
aluminium oxide powders using inductively coupled
plasma-optical emission spectrometry (ISO 3169:2023)
Céramiques techniques - Méthodes d'analyse chimique Hochleistungskeramik - Verfahren zur chemischen
des impuretés contenues dans les poudres d'oxyde Analyse von Verunreinigungen in
d'aluminium à l'aide de la spectrométrie d'émission Aluminiumoxidpulvern mittels optischer
optique par plasma à couplage inductif (ISO Emissionsspektrometrie mit induktiv gekoppeltem
3169:2023) Plasma (ISO 3169:2023)
This European Standard was approved by CEN on 24 November 2025.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2025 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 3169:2025 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
The text of ISO 3169:2023 has been prepared by Technical Committee ISO/TC 206 "Fine ceramics” of
the International Organization for Standardization (ISO) and has been taken over as EN ISO 3169:2025
by Technical Committee CEN/TC 184 “Advanced technical ceramics” the secretariat of which is held by
DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by May 2026, and conflicting national standards shall be
withdrawn at the latest by May 2026.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
Any feedback and questions on this document should be directed to the users’ national standards body.
A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the
United Kingdom.
Endorsement notice
The text of ISO 3169:2023 has been approved by CEN as EN ISO 3169:2025 without any modification.

INTERNATIONAL ISO
STANDARD 3169
First edition
2023-01
Fine ceramics (advanced ceramics,
advanced technical ceramics) —
Methods for chemical analysis of
impurities in aluminium oxide
powders using inductively coupled
plasma-optical emission spectrometry
Céramiques techniques (céramiques avancées, céramiques techniques
avancées) — Méthodes d'analyse chimique des impuretés contenues
dans les poudres d'oxyde d'aluminium à l'aide de la spectrométrie
d'émission optique par plasma à couplage inductif
Reference number
ISO 3169:2023(E)
ISO 3169:2023(E)
© ISO 2023
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
ISO 3169:2023(E)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Analytical range .1
5 Preparation of test sample . 1
5.1 General . 1
5.2 Sampling . 2
5.3 Drying . 2
5.4 Weighing . 2
6 Reporting analytical values . 2
6.1 Number of analyses . 2
6.2 Blank test . 2
6.3 Evaluation of analytical results . 2
6.4 Expression of analytical results . 2
7 Decomposition of test sample .2
7.1 Classification of decomposition methods . 2
7.2 Acid pressure decomposition . 3
7.2.1 Reagents . 3
7.2.2 Apparatus and instruments . 3
7.2.3 Sample decomposition procedure . 4
7.2.4 Blank test . 5
7.3 Acid decomposition . 5
7.3.1 Reagents . 5
7.3.2 Apparatus and instruments . 5
7.3.3 Sample decomposition procedure . 5
7.3.4 Blank test . 5
7.4 Alkali fusion . 6
7.4.1 Reagents . 6
7.4.2 Apparatus and instruments . 6
7.4.3 Sample decomposition . 6
7.4.4 Blank test . 6
8 Determination of impurity elements .7
8.1 Principle . 7
8.2 Reagents . 7
8.2.1 Aluminium standard solution (Al 10 mg/ml). 7
8.2.2 Elemental standard solutions. 7
8.2.3 Mixed standard solution (each element 50 mg/l). . 7
8.3 Apparatus and instruments. 8
8.3.1 ICP-OES. . 8
8.4 Preparation of calibration standard solutions . 8
8.5 Measurement . 8
8.5.1 Set-up of the instruments . 8
8.5.2 Measurement of sample test solution and calibration standard solutions . 9
8.5.3 Measurement of blank test solution . 9
8.6 Drawing of calibration curve . 9
8.7 Calculation . 10
9 Test report .10
Annex A (informative) Interlaboratory chemical analysis of impurity in alumina powder .12
iii
ISO 3169:2023(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www.iso.org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO's adherence to
the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see
www.iso.org/iso/foreword.html.
This document was prepared by Technical Committee ISO/TC 206, Fine ceramics.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www.iso.org/members.html.
iv
INTERNATIONAL STANDARD ISO 3169:2023(E)
Fine ceramics (advanced ceramics, advanced technical
ceramics) — Methods for chemical analysis of impurities
in aluminium oxide powders using inductively coupled
plasma-optical emission spectrometry
1 Scope
This document specifies methods for the chemical analysis of impurities present in aluminium oxide
powders used as a raw material for fine ceramics.
Aluminium oxide powders are decomposed by acid pressure decomposition, acid decomposition or
alkali fusion. The calcium, chromium, copper, iron, magnesium, manganese, potassium, silicon, sodium,
titanium, zinc and zirconium contents in the test solution are determined by an inductively coupled
plasma-optical emission spectrometer (ICP-OES).
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 3696, Water for analytical laboratory use — Specification and test methods
ISO 6353-2, Reagents for chemical analysis — Part 2: Specifications — First series
ISO 8656-1, Refractory products — Sampling of raw materials and unshaped products — Part 1: Sampling
scheme
3 Terms and definitions
No terms and definitions are listed in this document.
ISO and IEC maintain terminology databases for use in standardization at the following addresses:
— ISO Online browsing platform: available at https:// www .iso .org/ obp
— IEC Electropedia: available at https:// www .electropedia .org/
4 Analytical range
Each element, range of 0,000 5 % to 0,5 % (mass fraction).
5 Preparation of test sample
5.1 General
Prepare the sample in accordance with ISO 8656-1, unless otherwise mutually agreed upon by t
...

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