This document describes a method for the analysis of mass fractions of the impurities Al, B, Ca, Cr, Cu, Fe, Mg, Ni, Ti, V and Zr in powdered and grain-shaped silicon carbide of ceramic raw materials and ceramic materials. This application can also be extended to other metallic elements and other similar non-metallic powdered and grain-shaped materials such as carbides, nitrides, graphite, carbon blacks, cokes, carbon, as well as a number of further oxidic raw and basic materials after appropriate testing.
NOTE   There is positive experience with materials such as, for example, graphite, boron carbide (B4C), boron nitride (BN), tungsten carbide (WC) and several refractory metal oxides.
This testing procedure is applicable to mass fractions of the impurities mentioned above from approximately 1 mg/kg up to approximately 3 000 mg/kg, after verification. In some cases, it is possible to extend the range up to 5 000 mg/kg depending on element, emission lines, DCArc parameters, and sample mass.

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This document specifies a method for the determination of the mass fractions of the elements Al, Ca, Cr, Cu, Fe, Mg, Ni, Ti, V and Zr in powdered and granular silicon carbide.
Dependent on element, emission lines, plasma conditions and sample mass, this test method is applicable for mass fractions of the above trace contaminations from about 0,1 mg/kg to about 1 000 mg/kg, after evaluation also from 0,001 mg/kg to about 5 000 mg/kg.
NOTE 1   Generally for optical emission spectrometry using inductively coupled plasma and electrothermal vaporization (ETV-ICP-OES) there is a linear working range of up to four orders of magnitude. This range can be expanded for the respective elements by variation of the sample mass or by choosing emission lines with different sensitivity.
After adequate verification, this document is also applicable to further metallic elements (excepting Rb and Cs) and some non-metallic contaminations (like P and S) and other allied non-metallic powdered or granular materials like carbides, nitrides, graphite, soot, coke, coal, and some other oxidic materials (see [1], [4], [5], [6], [7], [8], [9] and [10]).
NOTE 2   There is positive experience with materials like, for example, graphite, boron carbide (B4C), silicon nitride (Si3N4), boron nitride (BN) and several metal oxides as well as with the determination of P and S in some of these materials.

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This document specifies a method for the determination of the mass fractions of the elements Al, Ca, Cr, Cu, Fe, Mg, Ni, Ti, V and Zr in powdered and granular silicon carbide.
Dependent on element, emission lines, plasma conditions and sample mass, this test method is applicable for mass fractions of the above trace contaminations from about 0,1 mg/kg to about 1 000 mg/kg, after evaluation also from 0,001 mg/kg to about 5 000 mg/kg.
NOTE 1   Generally for optical emission spectrometry using inductively coupled plasma and electrothermal vaporization (ETV-ICP-OES) there is a linear working range of up to four orders of magnitude. This range can be expanded for the respective elements by variation of the sample mass or by choosing emission lines with different sensitivity.
After adequate verification, this document is also applicable to further metallic elements (excepting Rb and Cs) and some non-metallic contaminations (like P and S) and other allied non-metallic powdered or granular materials like carbides, nitrides, graphite, soot, coke, coal, and some other oxidic materials (see [1], [4], [5], [6], [7], [8], [9] and [10]).
NOTE 2   There is positive experience with materials like, for example, graphite, boron carbide (B4C), silicon nitride (Si3N4), boron nitride (BN) and several metal oxides as well as with the determination of P and S in some of these materials.

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This document describes a method for the analysis of mass fractions of the impurities Al, B, Ca, Cr, Cu, Fe, Mg, Ni, Ti, V and Zr in powdered and grain-shaped silicon carbide of ceramic raw materials and ceramic materials. This application can also be extended to other metallic elements and other similar non-metallic powdered and grain-shaped materials such as carbides, nitrides, graphite, carbon blacks, cokes, carbon, as well as a number of further oxidic raw and basic materials after appropriate testing.
NOTE   There is positive experience with materials such as, for example, graphite, boron carbide (B4C), boron nitride (BN), tungsten carbide (WC) and several refractory metal oxides.
This testing procedure is applicable to mass fractions of the impurities mentioned above from approximately 1 mg/kg up to approximately 3 000 mg/kg, after verification. In some cases, it is possible to extend the range up to 5 000 mg/kg depending on element, emission lines, DCArc parameters, and sample mass.

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SIGNIFICANCE AND USE
3.1 Sieve analyses are carried out to determine the particle size distribution of powders which, in turn, are used to qualify those materials as to their usefulness in the process under consideration. Since particle size analyses have only relative significance, the results should be considered only where they correlate with process characteristics. The parameter that is being measured in this test is the amount of material that will pass through a cloth having theoretically square openings. It must be remembered that all the holes are not square, nor uniform in size, and the question of whether a given particle will go through is a statistical one. Since each particle size analysis method measures a unique physical parameter, the results from one method may not agree with those from another. Particle size distributions play a role in such properties as bulk density, dustiness, and handling characteristics. Care should be taken, however, when interpretations are made from one or two points (sieves) on the distribution curve.
SCOPE
1.1 This test method covers the determination of the particle size distribution of nonplastic ceramic powders such as alumina, silica, feldspar, pyrophyllite, nepheline syenite, talc, titanates, and zircon using wire cloth sieves.  
1.2 Materials containing a large amount of fines, containing agglomerates, or that are nonfree-flowing, are wet-sieved to remove excessive fines or to disperse agglomerates before performing the test. This technique is not applicable to materials that are, to any degree, water soluble.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units, or are other customary units (in the case of sieve frame diameter and sieve number), that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
3.1 This test method is useful to both sellers and purchasers of alumina and quartz powders for determining particle size distributions for materials specifications, manufacturing control, and development and research.
SCOPE
1.1 This test method, one of several found valuable for the measurement of particle size, covers the determination of the particle size distribution of alumina or quartz powders (0.6 μm to 56.0 μm) using electrical sensing zone particle size analyzers. These instruments use an electric current path of small dimensions which is modulated by individual particle passage through an aperture, and produces individual pulses of amplitude proportional to the particle volume.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
4.1 Composite materials consist by definition of a reinforcement phase/s in a matrix phase/s. The composition and structure of these constituents in the composites are commonly tailored for a specific application with detailed performance requirements. For fiber reinforced ceramic composites the tailoring involves the selection of the reinforcement fibers (composition, properties, morphology, interface coatings, etc.), the matrix (composition, properties, and morphology), the composite structure (component fractions, reinforcement architecture, interface coatings, porosity structure, microstructure, etc.), and the fabrication conditions (assembly, forming, densification, finishing, etc.). The final engineering properties (physical, mechanical, thermal, electrical, etc) can be tailored across a broad range with major directional anisotropy in the properties. (5-9)  
4.2 This classification system assists the ceramic composite designer/user/producer in identifying and organizing different types of silicon carbide-silicon carbide (SiC-SiC) composites (based on fibers, matrix, architecture, physical properties, and mechanical properties) for structural applications. It is meant to assist the ceramic composite community in developing, selecting, and using SiC-SiC composites with the appropriate composition, construction, and properties for a specific application.  
4.3 This classification system is a top level identification tool which uses a limited number of composites properties for high level classification. It is not meant to be a complete, detailed material specification, because it does not cover the full range of composition, architecture, physical, mechanical, fabrication, and durability requirements commonly defined in a full design specification. Guide C1793 provides direction and guidance in preparing a complete material specification for a given SiC-SiC composite component.
SCOPE
1.1 This classification covers silicon carbide-silicon carbide (SiC-SiC) composite structures (flat plates, rectangular bars, round rods, and tubes) manufactured for structural components. The SiC-SiC composites consist of continuous silicon carbide fibers in a silicon carbide matrix produced by four different matrix densification methods.  
1.2 The classification system provides a means of identifying and organizing different SiC-SiC composites, based on the fiber type, architecture class, matrix densification, physical properties, and mechanical properties. The system provides a top-level identification system for grouping different types of SiC-SiC composites into different classes and provides a means of identifying the general structure and properties of a given SiC-SiC composite. It is meant to assist the ceramics community in developing, selecting, and using SiC-SiC composites with the appropriate composition, construction, and properties for a specific application.  
1.3 The classification system produces a classification code for a given SiC-SiC composite, which shows the type of fiber, reinforcement architecture, matrix type, fiber volume fraction, density, porosity, and tensile strength and modulus (room temperature).  
1.3.1 For example, Composites Classification Code, SC2-A2C-4D10-33—a SiC-SiC composite material/component (SC2) with a 95 %+ polymer precursor (A) based silicon carbide fiber in a 2-D (2) fiber architecture with a CVI matrix (C), a fiber volume fraction of 45 % (4 = 40 % to 45 %), a bulk density of 2.3 g/cc (D = 2.0 g/cc to 2.5 g/cc), an apparent porosity of 12 % (10 = 10 % to 15 %), an average ultimate tensile strength of 350 MPa (3 = 300 MPa to 399 MPa), and an average tensile modulus of 380 GPa (3 = 300 GPa to 399 GPa).  
1.4 This classification system is a top level identification tool which uses a limited number of composite properties for high level classification. It is not meant to be a complete, detailed material specification, because it does not cover the full rang...

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ABSTRACT
This test method covers the determination of free moisture in ceramic whiteware clays. Whiteware clays may be shipped as a bulk shipment in lumps, a bulk shipment of shredded or coarsely ground clay, or in bagged lots of ground or airfloated clay. Directions are given in this test method for obtaining representative samples of the clay shipment to be used in subsequent tests for the properties of the clay in the shipment. Percentage of free moisture shall be calculated to the nearest 0.1%.
SCOPE
1.1 This test method covers the determination of free moisture in ceramic whiteware clays. Whiteware clays may be shipped as a bulk shipment in lumps, a bulk shipment of shredded or coarsely ground clay, or in bagged lots of ground or airfloated clay. Directions are given in this test method for obtaining representative samples of the clay shipment to be used in subsequent tests for the properties of the clay in the shipment.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
4.1 Both sellers and purchasers of alumina and quartz will find the test method useful to determine the specific surface area and indirectly as a measure of the particle size for material specifications, manufacturing control, and research and development.
SCOPE
1.1 This test method covers the determination of the specific surface area of aluminas and silicas used in the manufacture of ceramics. The test method is a general one, permitting the use of any modern commercial nitrogen adsorption apparatus but strictly defining the outgassing procedure. Calculations are based on the Brunauer-Emmett-Teller (BET) equation.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ABSTRACT
This test method details the standard procedures for the determination of the particle size distribution of alumina or quartz powders using X-ray monitoring of gravity sedimentation. This test procedure shall make use of an X-ray sedimentation apparatus, and ultrasonic probe or bath. An aqueous homogeneous dispersion of the specimen is permitted to settle in a cell. The decrease in particle concentration over a programmed settling distance is monitored by an X-ray beam passing through the sedimenting dispersion to a detector. The specimen concentration at any given sedimentation distance is inversely proportional to the X-ray flux and the equivalent diameter (spherical) is calculated from Stokes' law.
SCOPE
1.1 This test method covers the determination of the particle size distribution of alumina or quartz powders in the range from 0.5 μm to 50 μm and having a median particle diameter from 2.5 μm to 10 μm using a sedimentation method. This test method is one of several found valuable for the measurement of particle size. Instruments used for this test method employ a constant intensity X-ray beam that is passed through a sedimenting dispersion of particles.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 7.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ABSTRACT
This test method covers the procedures for determining soluble sulfate ions present in water or a filtrate using a photometer to measure the turbidity of precipitated barium sulfate. This test method also details a method for standardizing the photometer to be used. The soluble sulfate ions may be removed from clays or clay-water slurries by leaching with water during mixing and then filter pressing. An impractical number of washings would be needed to remove all sulfate ions, therefore, this test method should be considered only as a control test and not a quantitative analysis for sulfate ions. Test apparatus include a balance, high speed mixer, filter press, glass beakers, transfer pipets, spectrophotometer, measuring spoon, and other laboratory equipment. All reagents to be used should be of the required purity and concentration.
SCOPE
1.1 This test method covers the determination of soluble sulfate ions present in water or a filtrate by means of a photometer measuring the turbidity of precipitated barium sulfate. A method of standardizing the photometer for this test method is also given.  
1.2 Soluble sulfate ions may be removed from clays or clay-water slurries by leaching with water during mixing and subsequent filter pressing. To remove all the sulfate ions would require an impractical number of washings; therefore, this test method should be considered a control test and not a quantitative analysis for SO4 ions.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ABSTRACT
This guide covers the wet sieve analysis of ceramic whiteware clays. This guide is intended for use in testing shipments of clay as well as for plant control tests. The apparatus to be used include stirring device and sieves. The following procedure shall be followed in the analysis of the ceramic whiteware clays: transferring of duplicate portions of the dried clay sample; agitating of the slurry by means of a mechanical stirrer to ensure complete separation of clay from nonplastic impurities; transferring of the slaked and stirred sample, without loss, to the finest sieve to be employed in the test; washing of the residue remaining on the finest sieve into the pan; nesting the top sieve on the pan, which shall contain a certain amount of clear water; refilling of the pan with the proper amount of water, then nesting the top sieve and its residue on the pan; carefully blotting each sieve on its underside with a soft, damp sponge, and placing the sieve either in a drying oven or under infrared lamps until thoroughly dry; nesting the dried residues and sieves in the proper order, with due care to prevent dusting of the residues; and separating the nested sieves and carefully brushing the residue from each onto a weighing paper.
SCOPE
1.1 This guide covers the wet sieve analysis of ceramic whiteware clays. This guide is intended for use in testing shipments of clay as well as for plant control tests.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ABSTRACT
This standard test method covers the rate determination of clay-water paste layer formation from a clay-water slip under pressure filtration. Filter pressing of clay shall be in accordance to the procedure indicated in this specification. Calculation of filtration rate and void fraction shall depend on thickness of wet filter cake and filtration time. Void fraction in the filter cake shall depend on filter cake weight, filter press cross-sectional area, and wet filter cake thickness.
SCOPE
1.1 This test method covers the determination of the rate at which a layer of clay-water paste is formed from a clay-water slip under pressure filtration. The filtration rate is directly related to such whiteware operations as filter pressing, slip casting, and drying of ware in which water permeability through a clay-water paste is the controlling mechanism.  
1.2 A straight-line relationship exists between the time of filter pressing and the square of the thickness of the paste layer. The filtration rate is directly related to the filter press pressure and the void fraction of the paste layer, and is inversely related to the square of the clay surface area, the ratio of solids to liquid in the slip, and the viscosity of water at the testing temperature.  
1.3 The values stated in acceptable metric units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
4.1 The estimation of average particle size has two chief functions: (1) as a guide to the degree of fineness or coarseness of a powder as this, in turn, is related to the flow and packing properties, and (1) as a control test on the uniformity of a product.  
4.2 These test methods provide procedures for determining the envelope-specific surface area of powders, from which is calculated an “average” particle diameter, assuming the particles are monosize, smooth surface, nonporous, spherical particles. For this reason, values obtained by these test methods will be reported as an average particle size or Fisher Number. The degree of correlation between the results of these test methods and the quality of powders in use will vary with each particular application and has not been fully determined.  
4.3 These test methods are generally applicable to alumina and silica powders, for particles having diameters between 0.2 and 75 μm (MIC SAS) or between 0.5 and 50 μm (FSSS). They may be used for other similar ceramic powders, with caution as to their applicability. They should not be used for powders composed of particles whose shape is too far from equiaxed—that is, flakes or fibers. In these cases, it is permissible to use the test methods described only by agreement between the parties concerned. These test methods shall not be used for mixtures of different powders, nor for powders containing binders or lubricants. When the powder contains agglomerates, the measured surface area may be affected by the degree of agglomeration. Methods of de-agglomeration may be used if agreed upon between the parties concerned.  
4.4 When an “average” particle size of powders is determined using either the MIC SAS or the FSSS, it should be clearly kept in mind that this average size is derived from the determination of the specific surface area of the powder using a relationship that is true only for powders of uniform size and spherical shape. Thus, the results of these methods are ...
SCOPE
1.1 These test methods cover the estimation of the average particle size in micrometres of alumina and silica powders using an air permeability method. The test methods are intended to apply to the testing of alumina and silica powders in the particle size range from 0.2 to 75 μm.  
1.2 The values stated in SI units are to be regarded as standard, with the exception of the values for density and the mass used to determine density, for which the use of the gram per cubic centimetre (g/cm3) and gram (g) units is the long-standing industry practice; and the units for pressure, cm H2O—also long-standing practice.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
4.1 It is important to recognize that the results obtained by this method or any other method for particle size distribution utilizing different physical principles may disagree. The results are strongly influenced by the physical principles employed by each method of particle size analysis. The results of any particle sizing method should be used only in a relative sense, and should not be regarded as absolute when comparing results obtained by other methods.  
4.2 Light scattering theory that is used for determination of particle size has been available for many years. Several manufacturers of testing equipment have units based on these principles. Although each type of testing equipment utilizes the same basic principles for light scattering as a function of particle size, different assumptions pertinent to applications of the theory and different models for converting light measurements to particle size may lead to different results for each instrument. Therefore, the use of this test method cannot guarantee directly comparable results from the various manufacturers' instruments.  
4.3 Manufacturers and purchasers of alumina and quartz will find the method useful to determine particle size distributions for materials specifications, manufacturing control, and research and development.
SCOPE
1.1 This test method covers the determination of particle size distribution of alumina or quartz using laser light-scattering instrumentation in the range from 0.1 to 500 μm.  
1.2 The procedure described in this test method may be applied to other nonplastic ceramic powders. It is at the discretion of the user to determine the method's applicability.  
1.3 This test method applies to analysis using aqueous dispersions.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 Quartz has been classified by IARC as a Group I carcinogen. For specific hazard information in handling this material, see the supplier's Material Safety Data Sheet.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
5.1 Manufacturers and users of alumina powders will find this test method useful to determine the particle size distribution of these materials for product specification, quality control, and research and development testing.
SCOPE
1.1 This test method covers the determination of the particle size distribution of alumina in the range from 0.1 to 20 μm having a median particle diameter from 0.5 to 5.0 μm.  
1.2 The procedure described in this test method may be successfully applied to other ceramic powders in this general size range. It is the responsibility of the user to determine the applicability of this test method to other material.  
1.3 The values stated in SI units are to regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
4.1 Both suppliers and users of pulverized ceramic powders will find this test method useful to determine particle size distributions for materials specifications, manufacturing control, development, and research.  
4.2 The test method is simple, although tedious, uses inexpensive equipment, and will provide a continuous curve with data obtained with standardized woven sieves.
SCOPE
1.1 This guide covers the determination of the particle size distribution of pulverized alumina and quartz for particle sizes from 45 to 5 μm by wet sieving.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 The only exception is in the Section 5, Apparatus, 5.1 where there is no relevant SI equivalent.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
2.1 The purpose of this test is to obtain values of shrinkage after drying and firing of clays or bodies or both, under various processing conditions to enable designers to determine the proper size of mold or die so as to produce a predetermined size of fired ware.
SCOPE
1.1 This test method covers the determination of linear shrinkage of ceramic whiteware clays, both unfired and fired.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ISO 14720-1:2013 defines a method for the determination of sulfur in powdered and granular non-oxidic ceramic raw materials and materials, such as silicon carbides, silicon nitrides, graphites, carbon blacks, cokes, carbon powders. If proved by the recovery rate, this method can also be applied for other non-metallic powdered and granular materials, e.g. silicon dioxide.
ISO 14720-1:2013 is applicable for materials with mass fractions of sulfur from 0,005 % to 2 %.
ISO 14720-1:2013 can also be applied for materials with higher mass fractions of sulfur after verification of the particular case.

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This part of ISO 14720 defines a method for the determination of sulfur in powdered and granular non-oxidic ceramic raw materials and materials, which are completely oxidized at a higher temperature in an oxygen atmosphere, e.g. carbon and graphite materials.
For materials which are not completely oxidizable under these conditions, it is possible to determine sulfur that can be released under these conditions, e.g. the adherent sulfur.
This part of ISO 14720 is applicable for materials with mass fractions of sulfur ≤ 10 % and mass fractions of ash  < 20 %, The defined method is limited for materials with mass fractions of barium < 10 mg/kg, because the sulfur bonded in barium sulfate is not detectable with this method.
For the lower detection limit of this method, a mass fraction of sulfur of 0,5 mg/kg in the case of inductively coupled plasma optical emission spectrometry (ICP/OES) and 5 mg/kg in the case of ion chromatography (IC) has to be considered as a recommended value.

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ISO 14720-1:2013 defines a method for the determination of sulfur in powdered and granular non-oxidic ceramic raw materials and materials, such as silicon carbides, silicon nitrides, graphites, carbon blacks, cokes, carbon powders. If proved by the recovery rate, this method can also be applied for other non-metallic powdered and granular materials, e.g. silicon dioxide.
ISO 14720-1:2013 is applicable for materials with mass fractions of sulfur from 0,005 % to 2 %.
ISO 14720-1:2013 can also be applied for materials with higher mass fractions of sulfur after verification of the particular case.

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This part of ISO 14720 defines a method for the determination of sulfur in powdered and granular non-oxidic ceramic raw materials and materials, which are completely oxidized at a higher temperature in an oxygen atmosphere, e.g. carbon and graphite materials.
For materials which are not completely oxidizable under these conditions, it is possible to determine sulfur that can be released under these conditions, e.g. the adherent sulfur.
This part of ISO 14720 is applicable for materials with mass fractions of sulfur ≤ 10 % and mass fractions of ash  < 20 %, The defined method is limited for materials with mass fractions of barium < 10 mg/kg, because the sulfur bonded in barium sulfate is not detectable with this method.
For the lower detection limit of this method, a mass fraction of sulfur of 0,5 mg/kg in the case of inductively coupled plasma optical emission spectrometry (ICP/OES) and 5 mg/kg in the case of ion chromatography (IC) has to be considered as a recommended value.

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This part of ISO 14720 defines a method for the determination of sulfur in powdered and granular non-oxidic ceramic raw materials and materials, which are completely oxidized at a higher temperature in an oxygen atmosphere, e.g. carbon and graphite materials. For materials which are not completely oxidizable under these conditions, it is possible to determine sulfur that can be released under these conditions, e.g. the adherent sulfur. This part of ISO 14720 is applicable for materials with mass fractions of sulfur ≤ 10 % and mass fractions of ash For the lower detection limit of this method, a mass fraction of sulfur of 0,5 mg/kg in the case of inductively coupled plasma optical emission spectrometry (ICP/OES) and 5 mg/kg in the case of ion chromatography (IC) has to be considered as a recommended value.

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ISO 14720-1:2013 defines a method for the determination of sulfur in powdered and granular non-oxidic ceramic raw materials and materials, such as silicon carbides, silicon nitrides, graphites, carbon blacks, cokes, carbon powders. If proved by the recovery rate, this method can also be applied for other non-metallic powdered and granular materials, e.g. silicon dioxide. ISO 14720-1:2013 is applicable for materials with mass fractions of sulfur from 0,005 % to 2 %. ISO 14720-1:2013 can also be applied for materials with higher mass fractions of sulfur after verification of the particular case.

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ISO 14719:2011 specifies a spectral photometric method with 1,10-phenanthroline for the quantitative determination of Fe2+ and Fe3+ in oxidic raw and basic materials for ceramics, glass and glazes, e.g. feldspar, kaolinites, clay, limestone, quartz refractory materials. ISO 14719:2011 could be extended to other aluminosilicate materials, providing that uncertainty data is produced to support it. However, there might be problems in the decomposition of high-purity alumina and chrome ore samples.
The method is not suitable for reduced materials, such as silicon carbide, graphite-magnesia, etc.

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ISO 14720-1:2013 defines a method for the determination of sulfur in powdered and granular non-oxidic ceramic raw materials and materials, such as silicon carbides, silicon nitrides, graphites, carbon blacks, cokes, carbon powders. If proved by the recovery rate, this method can also be applied for other non-metallic powdered and granular materials, e.g. silicon dioxide.
ISO 14720-1:2013 is applicable for materials with mass fractions of sulfur from 0,005 % to 2 %.
ISO 14720-1:2013 can also be applied for materials with higher mass fractions of sulfur after verification of the particular case.

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This part of ISO 14720 defines a method for the determination of sulfur in powdered and granular non-oxidic ceramic raw materials and materials, which are completely oxidized at a higher temperature in an oxygen atmosphere, e.g. carbon and graphite materials.
For materials which are not completely oxidizable under these conditions, it is possible to determine sulfur that can be released under these conditions, e.g. the adherent sulfur.
This part of ISO 14720 is applicable for materials with mass fractions of sulfur ≤ 10 % and mass fractions of ash < 20 %, The defined method is limited for materials with mass fractions of barium < 10 mg/kg, because the sulfur bonded in barium sulfate is not detectable with this method.
For the lower detection limit of this method, a mass fraction of sulfur of 0,5 mg/kg in the case of inductively coupled plasma optical emission spectrometry (ICP/OES) and 5 mg/kg in the case of ion chromatography (IC) has to be considered as a recommended value.

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This part of ISO 14720 defines a method for the determination of sulfur in powdered and granular non-oxidic ceramic raw materials and materials, which are completely oxidized at a higher temperature in an oxygen atmosphere, e.g. carbon and graphite materials.
For materials which are not completely oxidizable under these conditions, it is possible to determine sulfur that can be released under these conditions, e.g. the adherent sulfur.
This part of ISO 14720 is applicable for materials with mass fractions of sulfur ≤ 10 % and mass fractions of ash < 20 %, The defined method is limited for materials with mass fractions of barium < 10 mg/kg, because the sulfur bonded in barium sulfate is not detectable with this method.
For the lower detection limit of this method, a mass fraction of sulfur of 0,5 mg/kg in the case of inductively coupled plasma optical emission spectrometry (ICP/OES) and 5 mg/kg in the case of ion chromatography (IC) has to be considered as a recommended value.

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ISO 14720-1:2013 defines a method for the determination of sulfur in powdered and granular non-oxidic ceramic raw materials and materials, such as silicon carbides, silicon nitrides, graphites, carbon blacks, cokes, carbon powders. If proved by the recovery rate, this method can also be applied for other non-metallic powdered and granular materials, e.g. silicon dioxide.
ISO 14720-1:2013 is applicable for materials with mass fractions of sulfur from 0,005 % to 2 %.
ISO 14720-1:2013 can also be applied for materials with higher mass fractions of sulfur after verification of the particular case.

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This part of ISO 14720 defines a method for the determination of sulfur in powdered and granular non-oxidic ceramic raw materials and materials, which are completely oxidized at a higher temperature in an oxygen atmosphere, e.g. carbon and graphite materials. For materials which are not completely oxidizable under these conditions, it is possible to determine sulfur that can be released under these conditions, e.g. the adherent sulfur. This part of ISO 14720 is applicable for materials with mass fractions of sulfur ≤ 10 % and mass fractions of ash For the lower detection limit of this method, a mass fraction of sulfur of 0,5 mg/kg in the case of inductively coupled plasma optical emission spectrometry (ICP/OES) and 5 mg/kg in the case of ion chromatography (IC) has to be considered as a recommended value.

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ISO 14720-1:2013 defines a method for the determination of sulfur in powdered and granular non-oxidic ceramic raw materials and materials, such as silicon carbides, silicon nitrides, graphites, carbon blacks, cokes, carbon powders. If proved by the recovery rate, this method can also be applied for other non-metallic powdered and granular materials, e.g. silicon dioxide. ISO 14720-1:2013 is applicable for materials with mass fractions of sulfur from 0,005 % to 2 %. ISO 14720-1:2013 can also be applied for materials with higher mass fractions of sulfur after verification of the particular case.

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This part of EN 12698 describes the methods for the analysis of all refractory products containing nitride bonded silicon carbide, irrespective of the Silicon carbide level.  It includes details of sample preparation, general principles of chemical analysis and detailed methods for the determination of carbon, silicon carbide, free aluminium, free silicon, total nitrogen and oxygen.  
Silicon nitride, silicon oxynitride, silicon, free silica and silicon aluminium oxynitride (sialon) can be determined by XRD.

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This European Standard defines a method for the determination of the trace element concentrations of Al, Ca, Cr, Cu, Fe, Mg, Ni, Ti, V and Zr in powdered and granular silicon carbide.
Dependent on element, wavelength, plasma conditions and weight, this test method is applicable for mass contents of the above trace contaminations from about 0,1 mg/kg to about 1 000 mg/kg, after evaluation also from 0,001 mg/kg to about 5 000 mg/kg.
NOTE 1   Generally for optical emission spectrometry using inductively coupled plasma (ICP OES) and electrothermal vaporization (ETV) there is a linear working range of up to four orders of magnitude. This range can be expanded for the respective elements by variation of the weight or by choosing lines with different sensitivity.
After adequate verification, the standard is also applicable to further metallic elements (excepting Rb and Cs) and some non-metallic contaminations (like P and S) and other allied non-metallic powdered or granular materials like carbides, nitrides, graphite, soot, coke, coal, and some other oxidic materials (see [1], [4], [5], [6], [7], [8], [9] and [10]).
NOTE 2   There is positive experience with materials like, for example, graphite, B4C, Si3N4, BN and several metal oxides as well as with the determination of P and S in some of these materials.

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This European Standard describes the method for the analysis of mass fractions of the impurities Al, B, Ca, Cr, Cu, Fe, Mg, Ni, Ti, V and Zr in powder  and grain-shaped silicon carbide of ceramic raw and basic materials. This application can also be extended to other metallic elements and other similar non-metallic powder  and grain-shaped materials such as carbides, nitrides, graphite, carbon blacks, cokes, carbon, as well as a number of further oxidic raw and basic materials after appropriate testing.
NOTE   There are positive interferences for materials such as e.g. graphite, B4C, BN, WC and several refractory metal oxides.
This testing procedure is applicable to mass fractions of the impurities mentioned above from approximately
1 mg/kg up to approximately 3 000 mg/kg, after verification. In some cases it may be possible to extend the range up to 5 000 mg/kg depending on element, wavelength, arc parameter, and sample weight.

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This European Standard defines a method for the determination of the trace element concentrations of Al, Ca, Cr, Cu, Fe, Mg, Ni, Ti, V and Zr in powdered and granular silicon carbide.
Dependent on element, wavelength, plasma conditions and weight, this test method is applicable for mass contents of the above trace contaminations from about 0,1 mg/kg to about 1 000 mg/kg, after evaluation also from 0,001 mg/kg to about 5 000 mg/kg.
NOTE 1   Generally for optical emission spectrometry using inductively coupled plasma (ICP OES) and electrothermal vaporization (ETV) there is a linear working range of up to four orders of magnitude. This range can be expanded for the respective elements by variation of the weight or by choosing lines with different sensitivity.
After adequate verification, the standard is also applicable to further metallic elements (excepting Rb and Cs) and some non-metallic contaminations (like P and S) and other allied non-metallic powdered or granular materials like carbides, nitrides, graphite, soot, coke, coal, and some other oxidic materials (see [1], [4], [5], [6], [7], [8], [9] and [10]).
NOTE 2   There is positive experience with materials like, for example, graphite, B4C, Si3N4, BN and several metal oxides as well as with the determination of P and S in some of these materials.

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This European Standard describes the method for the analysis of mass fractions of the impurities Al, B, Ca, Cr, Cu, Fe, Mg, Ni, Ti, V and Zr in powder  and grain-shaped silicon carbide of ceramic raw and basic materials. This application can also be extended to other metallic elements and other similar non-metallic powder  and grain-shaped materials such as carbides, nitrides, graphite, carbon blacks, cokes, carbon, as well as a number of further oxidic raw and basic materials after appropriate testing.
NOTE   There are positive interferences for materials such as e.g. graphite, B4C, BN, WC and several refractory metal oxides.
This testing procedure is applicable to mass fractions of the impurities mentioned above from approximately
1 mg/kg up to approximately 3 000 mg/kg, after verification. In some cases it may be possible to extend the range up to 5 000 mg/kg depending on element, wavelength, arc parameter, and sample weight.

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This European Standard defines a method for the determination of the trace element concentrations of Al, Ca, Cr, Cu, Fe, Mg, Ni, Ti, V and Zr in powdered and granular silicon carbide.
Dependent on element, wavelength, plasma conditions and weight, this test method is applicable for mass contents of the above trace contaminations from about 0,1 mg/kg to about 1 000 mg/kg, after evaluation also from 0,001 mg/kg to about 5 000 mg/kg.
NOTE 1   Generally for optical emission spectrometry using inductively coupled plasma (ICP OES) and electrothermal vaporisation (ETV) there is a linear working range of up to four orders of magnitude. This range can be expanded for the respective elements by variation of the weight or by choosing lines with different sensitivity.
After adequate verification, the standard is also applicable to further metallic elements (excepting Rb and Cs) and some non-metallic contaminations (like P and S) and other allied non-metallic powdered or granular materials like carbides, nitrides, graphite, soot, coke, coal, and some other oxidic materials (see [1], [4], [5], [6], [7], [8], [9] and [10]).
NOTE 2   There is positive experience with materials like for example graphite, B4C, Si3N4, BN and several metal oxides as well as with the determination of P and S in some of these materials.

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This European Standard defines a method for the determination of the trace element concentrations of Al, Ca, Cr, Cu, Fe, Mg, Ni, Ti, V and Zr in powdered and granular silicon carbide.
Dependent on element, wavelength, plasma conditions and weight, this test method is applicable for mass contents of the above trace contaminations from about 0,1 mg/kg to about 1 000 mg/kg, after evaluation also from 0,001 mg/kg to about 5 000 mg/kg.
NOTE 1   Generally for optical emission spectrometry using inductively coupled plasma (ICP OES) and electrothermal vaporisation (ETV) there is a linear working range of up to four orders of magnitude. This range can be expanded for the respective elements by variation of the weight or by choosing lines with different sensitivity.
After adequate verification, the standard is also applicable to further metallic elements (excepting Rb and Cs) and some non-metallic contaminations (like P and S) and other allied non-metallic powdered or granular materials like carbides, nitrides, graphite, soot, coke, coal, and some other oxidic materials (see [1], [4], [5], [6], [7], [8], [9] and [10]).
NOTE 2   There is positive experience with materials like for example graphite, B4C, Si3N4, BN and several metal oxides as well as with the determination of P and S in some of these materials.

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SCOPE
1.1 This method covers the quantitative determination of the distribution of particle sizes in kaolins and ball clays in the size range 44 to 0.1 [mu]m by the sedimentation process. Particles are allowed to settle under normal gravitational forces and concentrations of particles in the size range 44 to 2 [mu]m are measured using a hydrometer. Centrifuging is used to cause the smaller particles to settle more rapidly so that concentrations of particles in the size range 2 to 0.1 [mu]m may be measured using a pipet.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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SCOPE
1.1 This test method covers the determination of the biaxial flexure strength (modulus of rupture) of thin ceramic substrates.  
1.2 This test method is applicable to specimens in the as-fired condition or to test pieces prepared to have a certain thickness or surface finish.  
1.3 This test method may be used with specimens of various thicknesses and having warpage; no limits are placed on the latter, except those mutually imposed by the specifications agreed upon between the manufacturer and the purchaser of the substrates.  
1.4 The values stated in inch-pound units are to be regarded as the standard. The metric equivalents of inch-pound units may be approximate.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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1.1 This practice describes a safe manner in which to handle ceramic clays and slips in order to minimize respiratory exposure to dust.
1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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