19.120 - Particle size analysis. Sieving
ICS 19.120 Details
Particle size analysis. Sieving
Korngro?enbestimmung. Siebtechnik
Analyse dimensionnelle des particules. Tamisage
Analiza velikosti delcev. Sejanje
General Information
Frequently Asked Questions
ICS 19.120 is a classification code in the International Classification for Standards (ICS) system. It covers "Particle size analysis. Sieving". The ICS is a hierarchical classification system used to organize international, regional, and national standards, facilitating the search and identification of standards across different fields.
There are 391 standards classified under ICS 19.120 (Particle size analysis. Sieving). These standards are published by international and regional standardization bodies including ISO, IEC, CEN, CENELEC, and ETSI.
The International Classification for Standards (ICS) is a hierarchical classification system maintained by ISO to organize standards and related documents. It uses a three-level structure with field (2 digits), group (3 digits), and sub-group (2 digits) codes. The ICS helps users find standards by subject area and enables statistical analysis of standards development activities.
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This document specifies characteristics of a light scattering aerosol spectrometer (LSAS) which is used for measuring the size, number concentration and number-based size distribution of particles suspended in a gas. This document provide the calibration procedure and the validation method for aerosol spectrometers. This document applies to: - characterization of metered dose inhalers (MDI), dry powder inhalers (DPI) and nebulizers in pharmacy; - production control of active agents; - cut-off determination: impactors, cyclones and impingers; - atmospheric aerosols: bio-aerosols, stables or composting facilities, nebulized droplets, measurements in street tunnels; - fractional separation efficiency determination of filters.
- Standard37 pagesEnglish languagesale 15% off
This document specifies guidelines and instructions for the graphical representation of particle size analysis data in histograms, distribution densities and cumulative distributions. It also establishes a standard nomenclature to obtain the histograms, distribution densities and cumulative distributions from measured particle size data. This document applies to the graphical representation of particle size distributions (PSDs) of solid particles, droplets or gas bubbles covering all size ranges.
- Standard27 pagesEnglish languagesale 15% off
This document specifies the application of dynamic light scattering (DLS) to the following: - measurement of average hydrodynamic particle size; - measurement of the size distribution of mainly sub micrometre-sized particles, emulsions or fine bubbles dispersed in liquids. This document is applicable to the measurement of a broad range of dilute and concentrated suspensions.
- Standard64 pagesEnglish languagesale 15% off
This document specifies two methods of measurement of the electrophoretic mobility of particles suspended in a liquid: video microscopy and electrophoretic light-scattering. NOTE Estimation of surface charge and determination of zeta-potential can be achieved from measured electrophoretic mobility using proper theoretical models, which are described in detail in ISO 13099-1.
- Standard21 pagesEnglish languagesale 15% off
This document specifies principles and methods for the use of gravitational photosedimentation techniques for the characterization of dispersed phases of suspensions and emulsions. These techniques monitor the gravity-induced phase separation of particulate materials dispersed in liquids by recording photometric signals (i.e. intensity of transmitted or scattered light) as a function of either vertical position or measurement time, or both. This document does not cover particle migration by centrifugal, electric or magnetic forces, or sedimentation at high particle concentrations (e.g. zone sedimentation). Moreover, it does not cover the determination of properties other than sedimentation velocity and particle size (i.e. it does not cover particle concentration, particle shape, particle density, zeta-potential or apparent viscosity). Additionally, this document does not cover alternative techniques for gravitational sedimentation including balance based and X-ray based techniques. NOTE This document does not purport to address all the safety problems associated with its use.
- Standard54 pagesEnglish languagesale 15% off
This document specifies requirements and provides guidance for the use of charge conditioners for aerosol particles, especially for particle characterization and for the generation of calibration and test aerosols. This document provides a methodology to specify the performance of charge conditioners and for adequate quality control, with respect to their application in: — particle size and concentration measurement with differential mobility analysing systems (DMAS); —particle size classification with differential electrical mobility classifiers (DEMC). For these applications, this document covers particle charge conditioning for particle sizes ranging from approximately 1 nm to 1 µm and for particle number concentrations at the inlet of the charge conditioner up to approximately 107 cm-3. This document does not address specific charge conditioner designs or other applications besides those specified in Clause 1. Radiation safety for charge conditioners with radioactive sources or x-ray tubes is not covered by this document.
- Standard58 pagesEnglish languagesale 15% off
This document specifies the principles of particle size analysis by centrifugal liquid sedimentation (CLS). It also: - defines the relevant terms; - describes the various measurement techniques; - gives guidance for sample preparation, conducting measurements as well as data analysis; - establishes rules for method validation, determination of the uncertainty budget as well as representation of results. An important part of this document deals with the derivation of particle size distributions from CLS data, including discussions on: - the impact of Brownian motion; - the parallel determination of particle concentrations; - the working range with respect to size and concentration; -the handling of non-spherical and porous particles. This document applies to samples composed of dispersions of low particle concentration, so that the particles’ motion can be considered as that of fully isolated particles. This document does not cover particle migration by gravity, electric or magnetic forces. It also does not cover deriving particle properties other than size, sedimentation velocity and sedimentation coefficient. NOTE This document can involve hazardous materials, operations and equipment. It does not purport to address all the safety problems associated with its use. Regulations regarding explosion-proof analysers can apply when examining volatile liquids with a low flash point. It is the responsibility of the user of this document to establish appropriate safety and health practices and to determine the applicability of the regulatory limitations prior to its use.
- Standard81 pagesEnglish languagesale 15% off
This document specifies the particle tracking analysis (PTA) method under static (no flow) conditions for the determination of the number–based particle size distribution and the number concentration in liquid dispersions (solid particles, liquid droplets or bubbles suspended in liquids). This document covers two tracking regimes. — Brownian motion tracking for smaller particles. — Gravitational fall tracking for larger particles. This document outlines the theory and basic principles of the PTA method along with its limitations and advantages for both size evaluation and number concentration measurements. It also describes commonly used instrument configurations and measurement procedures as well as system qualifications and data reporting.
- Standard42 pagesEnglish languagesale 15% off
This document gives guidance on the determination criteria for when laser diffraction is the most appropriate method for the analysis of samples, the appropriate preparation of samples, the verification of the correct functioning of instruments, the interpretation of data, and the assessment of data quality. This document focuses on the practical steps needed to obtain results of good quality, rather than on theoretical considerations, and covers not only the measurement of solid particles (in wet and dry measurement configurations), but also emulsions and bubbles. Result variation expectations of real samples are also considered in this document.
- Technical specification23 pagesEnglish languagesale 15% off
This document specifies the principles of particle size analysis by gravitational sedimentation, the principal types of measurement techniques as well as the general rules for conducting measurements, method validation, determination of the uncertainty budget and representation of results. This document covers neither particle migration by centrifugal, electric or magnetic forces nor sedimentation at high particle concentrations (e.g. zone sedimentation). Moreover, this document does not deal with the determination of properties other than sedimentation velocity and particle size (i.e. neither particle concentration, particle shape, particle density, zeta-potential nor apparent viscosity). NOTE This document can involve hazardous materials, operations and equipment. This document does not purport to address all the safety problems associated with its use. Explosion proof analysers are required when examining volatile liquids with a low flash point.
- Standard70 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
5.1 The test can be used to evaluate the following:
5.1.1 Classification or Comparison of Powders—There are several parameters that can be used to classify powders relative to each other, the most useful being the measured shear stresses, cohesion, flow function and angle of internal friction.
5.1.2 Sensitivity Analysis—The shear cell can be used to evaluate the relative effects of a range of powder properties or environmental parameters, or both, such as (but not limited to) humidity, particle size and size distribution, particle shape and shape distribution, water content and temperature.
5.2 Quality Control—The test can, in some circumstances, be used to assess the flow properties of a raw material, intermediate or product against pre-determined acceptance criteria.
5.3 Storage Vessel Design—Mathematical models exist for the determination of storage vessel design parameters which are based on the flow properties of powders as generated by shear cell testing, requiring shear testing at a range of consolidating stresses as well as the measurement of the wall friction angle with respect to the material of construction of the storage vessel. The methods are detailed in Refs. (1-3).3
Note 1: The quality of the result produced by this test method is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this test method are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors (4).
Practice D3740 was developed for agencies engaged in the testing and/or inspection of soil and rock. As such it is not totally applicable to agencies performing this test method. However, users of this test method shoul...
SCOPE
1.1 This method covers the apparatus and procedures for quantifying the incipient failure properties of a powder as a function of the normal stress for a given level of consolidation. The method also allows the further determination of the unconfined yield strength, internal friction angles, cohesion, flow function, major principal stress and wall friction angle (with the appropriate wall coupon fitted to the correct accessory).
1.2 These parameters are most commonly used to assist with the design of storage hoppers and bins using industry standard calculations and procedures. They can also provide relative classification or comparison of the flow behavior of different powders or different batches of the same powder if similar stress and shear regimes are encountered within the processing equipment.
1.3 The apparatus is appropriate for measuring the properties of powders with a maximum particle size of 1 mm. It is practicable to test powders that have a small proportion of particles of 1 mm or greater, but it is recommended they represent no more than 5 % of the total mass in samples with a normal (Gaussian) size distribution.
1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.
1.4.1 The procedures used to specify how data are collected/recorded or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.
1.5 Un...
- Standard12 pagesEnglish languagesale 15% off
- Standard12 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
4.1 This test method can be used to determine particle size distributions for material specifications, manufacturing control, and research and development work in the particle size range usually encountered in fluidizable cracking catalysts.
SCOPE
1.1 This test method covers the determination of particle size distribution of catalyst and catalyst carrier (see Terminology D3766) particles using an electroconductive sensing method and is one of several valuable methods for the measurement of particle size.
1.2 The range of particle sizes investigated was 20 μm to 150 μm (see IEEE/ASTM SI 10) equivalent spherical diameter. The technique is capable of measuring particles above and below this range. The instrument used for this method is an electric current path of small dimensions that is modulated by individual particle passage through an aperture, and produces individual pulses of amplitude proportional to the particle volume.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard4 pagesEnglish languagesale 15% off
- Standard4 pagesEnglish languagesale 15% off
This document specifies methods for the zeta potential determination in porous materials that are saturated with a liquid where the pores are readily accessible. There is no restriction on the value of the zeta potential or on the porosity of the porous material. A pore is assumed to be on the scale of hundreds of micrometres or smaller without any restriction on pore geometry. This document covers the applications of alternating current (AC) and direct current (DC) methods using aqueous media as wetting liquids. This document is restricted to linear electrokinetic effects.
- Standard29 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
3.1 When evaluating the particle size information, if the procedures of the data processing are not available, the user of the data must make assumptions concerning the reported data in the event of analytical inconsistencies. In order for different data sets to be compared it is crucial that the parties report the analytical techniques and methods or procedures for evaluating, calculating, compiling or otherwise processing the data to be reported.
3.2 Particle size characterization information can be reported in three levels of detail in order to satisfy user's needs.
3.2.1 Level 1 applies when only basic information about the material is required, and shall be provided with each shipment. This level represents the minimum information that shall be reported. Level 1 information may be sufficient in such cases as identifying a certain grade of a material or when detailed knowledge of analytical methodology is not needed.
3.2.2 Level 2 presumes the need for knowledge of methodology on the user's part and allows the user to make a more informed judgment about the information provided in Level 1.
3.2.3 Level 3 provides detailed written procedures to allow duplication of the measurement.
3.2.4 Information provided through Levels 2 and 3 will allow users to perform comparative material evaluations among several suppliers, set specifications or define a purchase agreement, perform inter-laboratory studies and most importantly resolve disputes among suppliers and users.
3.3 Reported particle size measurement is a function of both the actual particle dimension and shape factor as well as the particular physical or chemical properties of the particle being measured. Caution is required when comparing data from instruments operating on different physical or chemical parameters or with different particle size measurement ranges. Sample acquisition, handling and preparation can also affect the reported particle size results.
SCOPE
1.1 This practice covers reporting particle size measurement data.
1.2 This practice applies to particle size measurement methods, devices, detail levels, and data formats for dry powders, and wet suspensions of solids, gels, or emulsion droplets. This practice does not pertain to liquid particles.
Note 1: For information on reporting liquid particle measurement data, refer to Practice E799.
1.3 This practice does not concern particle concentration information.
1.4 This practice uses SI (Système International) units as standard. State all numerical values in terms of SI units unless specific instrumentation software reports particle size information, including percentiles, indices, and distributions as tabulations and graphs using alternate units. In this case, present both reported and equivalent SI units in the final written report. Refer to Practice E380 for proper usage of SI units.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard7 pagesEnglish languagesale 15% off
This document specifies the measurements of particle size distribution and concentration of suspended particles, ranging from 40 nm to 100 µm, using tunable resistive pulse sensing (TRPS). This document provides a comprehensive overview of the methodologies that are applied to achieve reproducible and accurate TRPS measurement results. This document also includes best practice considerations, possible pitfalls and information on how to alleviate or avoid these pitfalls.
- Standard22 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
3.1 Interpretation and use of data generated by particle characterization methods is highly dependent on the definitions of terms describing that data. It is extremely important that those terms be defined in precisely the same way both when comparing data from different characterization techniques and even when correlating data from the same technique.
3.2 It is likewise important that users of particle characterization methods and the data generated therefrom understand the principles of the methods, so that differences and similarities in the data can be interpreted in relation to those principles. That understanding can help to avoid disagreements when data from different characterization methods are compared.
3.3 The definitions contained in this terminology will aid in the interpretation of particle characterization data with respect to the method(s) used to produce that data.
SCOPE
1.1 This terminology covers the definitions of terms used in the description and procedures of analysis of particulate materials not ordinarily analyzed using test sieves. The terms relate directly to the equipment used in analysis, the physical forms of the materials to be analyzed, and selected descriptive data reduction and analysis formats.
1.2 Committee E29 on Particle and Spray Characterization believes that it is essential to include terms and definitions explicit to the committee’s scope, regardless of whether the terms appear in existing ASTM standards. Terms that are in common usage and appear in common-language dictionaries are generally not included, unless they have specific meanings in the context of particle characterization different from the common-language definitions.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard4 pagesEnglish languagesale 15% off
- Standard4 pagesEnglish languagesale 15% off
This document deals with the application of small-angle X-ray scattering (SAXS) for the measurement of the particle concentration in suspensions. In this document, only the concentration of sufficiently monodisperse spherical particles is treated, which means that the width of the size distribution is typically below about 50 % of the mean diameter. Here, the differential scattering cross section can be calculated based on the form factor, which depends only on the momentum transfer q and the particle radius r. Furthermore, this document is limited to dilute systems. A dilute system in the sense of SAXS means that particle interactions are absent. In case of long-range interactions (Coulomb forces between the particles), special care needs to be taken and a reduction of the concentration can be necessary.
- Standard14 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
3.1 This test method assures that the particle size of soaps and detergents conforms to specifications having to do with density and packaging, among others. It also offers a means of controlling the amount of potentially hazardous very low particle size material.
SCOPE
1.1 This test method covers the determination of the particle size of soaps and other detergents by hand sieving and machine sieving methods.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Material Safety Data Sheets are available for reagents and materials. Review them for hazards prior to usage.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard2 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
3.1 This test method is used to determine the grading of aggregates extracted from asphalt mixtures. The results are used to determine compliance of the particle size distribution with applicable specifications requirements, and to provide necessary data for control of the production of various aggregates to be used in asphalt mixtures.
Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
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1.1 This test method covers a procedure for determination of the particle size distribution of fine and coarse aggregates extracted from asphalt mixtures using sieves with square openings.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard3 pagesEnglish languagesale 15% off
- Standard3 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
5.1 The particle size of fine mesh and powdered activated carbon is sometimes used to evaluate filter cake filtration rates and the filter penetration in filtering applications.
5.2 The selection and handling of fine mesh or powdered activated carbon, and operation of processes using fine mesh or powdered activated carbon, requires the knowledge of the particle size.
5.3 This test method is intended for single sieve testing only. For determination of particle size distribution of a sample, the test must be repeated using sieves with different openings.
Note 1: Relative humidity (RH) can affect the repeatability and accuracy of this test. Activated carbon not at equilibrium with the RH of the ambient air may lose or gain weight accordingly, dependent upon whether the carbon picks up or loses moisture.
SCOPE
1.1 This test method covers the determination of the particle size of powdered activated carbons using an air-jet sieve device. For purposes of this test method, powdered activated carbon is defined as activated carbon in particle sizes predominantly in a range of 80 mesh (0.180 mm) through 500 mesh (0.025 mm).
1.2 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard4 pagesEnglish languagesale 15% off
- Standard4 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
4.1 The method of powder dispersion in a liquid has a significant effect on the results of a particle size distribution analysis. The analysis will show a too-coarse, unstable, or nonrepeatable distribution if the powder has not been dispersed adequately. It is therefore important that parties wishing to compare their analyses use the same dispersion technique.
4.2 This guide provides ways of deriving dispersion techniques for a range of metal powders and compounds. It should be used by all parties performing liquid-dispersed particle size analysis of all of the materials covered by this guide (see 1.1, 1.2, and 4.1).
4.3 Table 1 provides some dispersion procedures that have been found useful and consistent for the particular materials listed there. These are only suggested dispersion procedures; the procedures and dispersion checks of 7.1.2 – 7.1.4, or the more detailed method development procedures of Guide E3340, should still be used to verify adequate dispersion for each particular material and particle size range. (A) Stated ultrasonic power and duration times are given as an indication only. Specific conditions should be sought for the particular system in question during the method development phase.(B) Tween 21, chemically known as polyoxyethylene6 sorbitan monolaurate, is manufactured by Croda International PLC, and is available from various chemical suppliers.(C) Three to five drops Tween 21 in 30 to 50 mL water.
4.4 This guide should be used in the preparation of powders for use in Test Methods B761 and B822 and other procedures that analyze metal powder particle size distributions in liquid-dispersed systems.
SCOPE
1.1 This guide covers the dispersion in liquids of metal powders and related compounds for subsequent use in particle size analysis instruments. This guide describes a general procedure for achieving and determining dispersion; it also lists procedures that have been found useful for certain materials.
1.2 This guide does not include specific procedures for dry dispersion of particulate materials. It only indicates when liquid dispersion is not appropriate and dry dispersion must be utilized (see 7.1.2.1). For guidance on development of methods of dry dispersion, see Guide E3340.
1.3 This guide is limited to metal powders and related metal compounds. However, the general procedure described herein may be used, with caution as to its significance, for other particulate materials, such as ceramics, pigments, minerals, etc.
1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Guide4 pagesEnglish languagesale 15% off
- Guide4 pagesEnglish languagesale 15% off
This document specifies the determination of the overall specific external and internal surface area of either disperse (e.g. nano-powders) or porous, solids by measuring the amount of physically adsorbed gas according to the method of Brunauer, Emmett and Teller method,[1] based on the 2015 International Union for Pure and Applied Chemistry (IUPAC) recommendations[3]. NOTE For solids exhibiting a chemically heterogeneous surface, for example, metal-carrying catalyst, the BET method gives the overall surface area, whereas the metallic portion of the surface area can be measured by chemisorption methods.
- Standard22 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
5.1 The ability to correlate results of analyzers to sieve sets enables the use of non-sieve methods to be employed that give comparable results to each other.
5.2 The use of analyzers for proppant measurement has the benefit of providing particle shape characteristics which are important in the performance of these materials. Shape analysis is currently done by operator’s determination based on a visual observation of a small number of particles per API 19C. Available information from imaging analysis of many particles can be used to assess the proppant shape characteristics as opposed to just a small number.
SCOPE
1.1 This practice describes procedural steps to create a correlation that can be used to compare results of proppant size distributions between dynamic imaging analyzers (analyzers) and prescribed sieve sets.
1.2 The proppant size and distribution specifications that are included in this practice are listed in API Standard 19C (API 19C) and shown in Table 1, however as industry evolves additional specifications may come into use and this practice can be used with those as well.
1.3 This practice may not be applicable to all proppant types and designations. The acceptability of the correlations determined are judged by the operator.
1.4 The values stated in SI units are to be regarded as the standard, except sieve designations are typically identified using the ‘alternative’ system in accordance with Practice E11, such as 3 in. and No. 200 instead of the ‘standard’ system of 75 mm and 75 µm, respectively.
1.5 Observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this standard.
1.5.1 The procedures used to specify how data are collected/recorded and calculated in Practice D6026 are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of these test methods to consider significant digits used in analysis methods for engineering data.
1.6 This practice offers a set of instructions for performing one or more specific operations. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this practice may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project’s many unique aspects. The word “Standard” in the title means only that the document has been approved through the ASTM consensus process.
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard7 pagesEnglish languagesale 15% off
SCOPE
1.1 This terminology includes all those terms used in all of the standards under the jurisdiction of Subcommittee E29.01. Terms are defined that are related to the manufacture of standard test sieves and screening media, as well as terms related to the methods, analysis, procedures, and equipment for sizing and separating particles.
1.2 Committee E29 on Particle and Spray Characterization feels that it is essential to include terms and definitions explicit to the scope, regardless of whether the terms appear in existing ASTM standards. Terms that are in common usage and appear in common-language dictionaries are generally not included.
1.3 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard6 pagesEnglish languagesale 15% off
- Standard6 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
4.1 This test method can be used to determine particle size distributions of catalysts and supports for materials specifications, manufacturing control, and research and development work.
SCOPE
1.1 This test method covers the determination of particle size distribution of catalytic powder material using a sieving instrument and is one of several found valuable for the measurement of particle size. This test method is particularly suitable for particles in the 20 to 420 μm range. (See Terminology D3766.)
1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.2.1 Exception—In 5.2, mesh size is the standard unit of measure.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard3 pagesEnglish languagesale 15% off
- Standard3 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
5.1 This practice is primarily used in the horticulture industry to separates peat material into arbitrary fractions based on particle size. Physical separation of peat material according to particle size provides a useful indicator of the properties of a peat specimen such as pore space and degree of decomposition for unprocessed peat. It also provides a means of determining the amount of foreign matter not in a divided state such as sticks, stones, and glass.
Note 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 Peat materials consist of particles with various sizes. This practice covers the separation of peat particles into coarse, medium, and fine size fractions using the 2.36 mm (No. 8) and 0.850 mm (No. 20) sieves equipped with cover and bottom pan. This practice is applicable for peat materials used in the horticultural industry and can be used to verify the degree of decomposition of peat and to determine the foreign matter content.
1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.
1.2.1 It is common practice in the engineering/construction profession to concurrently use pounds to represent both a unit of mass (lbm) and of force (lbf). This practice implicitly combines two separate systems of units; the absolute and the gravitational systems. It is scientifically undesirable to combine the use of two separate sets of inch-pound units within a single standard. As stated, this standard includes the gravitational system of inch-pound units and does not use/present the slug unit of mass. However, the use of balances and scales recording pounds of mass (lbm) or recording density in lbm/ft3 shall not be regarded as nonconformance with this standard.
1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.
1.3.1 The procedures used to specify how data are collected/recorded or calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.
1.4 This practice offers a set of instructions for performing one or more specific operations. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this practice may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project’s many unique aspects. The word “Standard” in the title of this document means only that the document has been approved through the ASTM consensus process.
1.5 This standard does not purport to address all of the safety concerns, if any...
- Standard3 pagesEnglish languagesale 15% off
- Standard3 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
5.1 Mean particle diameters defined according to the Moment-Ratio (M-R) system are derived from ratios between two moments of a particle size distribution.
SCOPE
1.1 The purpose of this practice is to present procedures for calculating mean sizes and standard deviations of size distributions given as histogram data (see Practice E1617). The particle size is assumed to be the diameter of an equivalent sphere, for example, equivalent (area/surface/volume/perimeter) diameter.
1.2 The mean sizes/diameters are defined according to the Moment-Ratio (M-R) definition system.2,3,4
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 It is necessary to know the distribution of particle sizes of granular activated carbon in order to provide proper contact of gases or liquid in a packed bed of the material. Changes in particle size distribution can affect the pressure drop across the bed and the rate of adsorption in a bed of a given size.
4.2 Mean particle diameter is a property of activated carbons that influences pressure drop.
4.3 Effective size and uniformity coefficient are two properties of activated carbons often of interest in municipal water treatment applications where control of particle size is of interest.
SCOPE
1.1 This test method covers the determination of the particle size distribution of granular activated carbon. For the purposes of this test, granular activated carbon is defined as a minimum of 90 % of the sample weight being retained on a 180 μm Standard sieve. A U.S. mesh 80 sieve is equivalent to a 180 μm Standard sieve.
Note 1: For extruded carbons, as the length/diameter ratio of the particles increases, the validity of the test results might be affected.
1.2 The data obtained may also be used to calculate mean particle diameter (MPD), effective size, and uniformity coefficient.
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3.1 Exception—All mass measurements are in SI units only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard6 pagesEnglish languagesale 15% off
This document specifies requirements for ultrasonic attenuation spectroscopy methods for determining the size distributions of a particulate phase dispersed in a liquid at dilute concentrations, where the ultrasonic attenuation spectrum is a linear function of the particle volume fraction. In this regime particle-particle interactions are negligible. Colloids, dilute dispersions, and emulsions are within the scope of this document. The typical particle size for such analysis ranges from 10 nm to 3 mm, although particles outside this range have also been successfully measured. For solid particles in suspension, size measurements can be made at concentrations typically ranging from 0,1 % by volume up to 5 % by volume, depending on the density contrast between the solid and liquid phases, the particle size, and the frequency range[9],[10]. For emulsions, measurements can be made at much higher concentrations. These ultrasonic methods can be used to monitor dynamic changes in the size distribution.
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This document defines terms that are relevant to the characterization of particles and particulate systems. This document includes such fields as the representation of results of particle size analysis, the descriptive and quantitative representation of particle shape and morphology, sample preparation, specific surface area and porosity characterization and such measurement methods as sedimentation, classification, acoustic methods, laser diffraction, dynamic light scattering, single particle light interaction methods, differential electrical mobility analysis, image analysis and others in a size scale from nanometre to millimetre.
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SIGNIFICANCE AND USE
5.1 Particle size and shape are important in predicting the performance of catalytic materials. They influence the bulk density of the final product and thereby the effectiveness of performance.
5.2 Establishing a verification reference for the analyzer that is commercially available and dimensionally reliable to close tolerances enables different analyzers to be easily checked to equivalent standards.
5.3 This practice may also be followed to analyze catalytic materials for quality manufacturing purposes. Sections 9 and 10 instruct on sample count determination as well as sampling recommendations. Test Method D6299 may be utilized to monitor performance of the analyzer in measuring the size and shape of catalytic materials.
SCOPE
1.1 This practice covers the calibration and verification of Dynamic Imaging Analyzers (analyzers) using catalytic and non-catalytic reference materials. The measurement range of analyzers covers from 500 µm to 20 000 µm.
1.2 This practice may also be used to analyze catalytic materials once the analyzer has been calibrated and verified.
1.3 Units—The values stated in SI units are to be regarded as standard; however, English and mesh units are also acceptable with conversions provided in Appendix X3.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard10 pagesEnglish languagesale 15% off
This document is intended to support users of reference materials (RMs) for particle size analysis to identify suitable RMs (certified or not) for their needs. In line with the focus on users, questions on sample preparation that go beyond preparation of the sample as received by the user will not be covered by this document. This document describes the fundamental requirements that RMs (certified or not) for the determination of particle size shall fulfil in order to be fit for a given purpose. The document is limited to a description of the fundamental principles – the discussion whether a certain numerical value is fit for purpose is beyond the scope of this document. The scope of this document is limited to RMs (certified or not) in the form of particles. This document does not deal with any other form of RMs, like calibration grids.
- Technical specification24 pagesEnglish languagesale 15% off
This document specifies the application of small-angle X-ray scattering (SAXS) for the determination of specific surface area. Both the mass specific surface area in the order of 1 m2g-1 to 2 000 m2g-1 and the volume specific surface areas in the range from 0,01 m2cm-3 to 1 000 m2cm-3 can be obtained. The method described is applicable to dilute and concentrated systems. NOTE: In ISO 17867:2020, the determination of the particle size by SAXS is limited to dilute systems. The determination of surfaces with SAXS is straightforward for two-phase systems only. Surface determination in systems with more than two phases is beyond the scope of this document. The term ‘surface’ refers to any interface between domains of different density (more precisely: electron density) and is not restricted to the external surface of particles. As any interfaces between areas with different electron density, not only to air or vacuum, can be probed, the method can be applied to any heterogeneous system. SAXS measures not only the specific surface area of open pores but also of inaccessible, closed pores or inclusions. NOTE: This is in contrast to gas sorption methods which are described in ISO 9277:2010. In addition to porous systems, there can be contributions of internal interfaces to the measured specific surface area of any heterogeneous compact solid system, such as between crystalline and amorphous phases, provided there is an electron density contrast. Although materials comprising micropores (pore width
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SIGNIFICANCE AND USE
5.1 This guide provides an alternative way to measure the porosity of catalytic materials without the use of mercury porosimetry. It is useful for research and development as well as quality control purposes. (See Test Methods D4284 and D6761.)
SCOPE
1.1 This guide describes how to measure the pore volume of catalytic materials by water immersion with the excess water removed with a centrifuge. The measured pore volume is converted to the dry pore volume by using the loss on ignition (LOI) of the material. It is generally applicable to both powdered materials and particles greater than about 1 mm.
1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Guide4 pagesEnglish languagesale 15% off
- Guide4 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
5.1 The technique of laser diffraction for particle size distribution analysis is extensively used in industry and academia both for on-line control and laboratory needs. Guidance is obviously useful in this regard.
5.2 This guide can be used to develop methods of particle size analysis where well-established analysis procedures do not already exist. See Guide B821 for similar guidance and useful procedures for wet dispersion of metal powders and related compounds.
SCOPE
1.1 This guide sets out the general approach to the particle size distribution measurement of powders, suspensions, or slurries using an appropriate wet or dry methodology by the laser diffraction technique. It is recommended for use in measurements of broad particle size distributions.
1.2 The guide provides guidelines to the parameters that should be specified and a generalized guideline to reasonable and acceptable tolerances for points in the volume-based distribution curve such as x10 (Dv10), x50 (Dv50), x90 (Dv90), and D[4, 3] (volume moment mean). It is noted that ISO prefers the term x for particle size as opposed to other usage of d or D (implying diameter).
1.3 This guide provides guidance on the verification of instrument performance in conjunction with the internal quality control (QC) audit functions of the instrument owner. Results should be reported in the format indicated by Practice E1617 and ISO 13320.
1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Guide9 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
4.1 This guide is intended to inform those who have need for particle analysis data of their product or process, how imaging technology, in the form of a DIA, can be employed to provide the required information for a wide range of processes and material types. It expands on dynamic imaging information provided in Guide E2651 which is a broad view of particle analysis methods.
4.2 This guide can be used to assess the suitability of the technology to particular applications as well as any limitations that may be encountered. It is also intended to help the user make an informed decision on how to best use the technology to make the measurement(s) most important in providing data that best describes the process or product.
4.3 Determining particle shape of materials such as proppants, catalysts, additive manufacturing powders, and many more materials, is critical to their performance. Imaging technology can provide a consistent assessment of shape factors based on objective criteria and a statistically significant number of particles analyzed. Human visual methods generally compare a small number of particles to a standard leaving room for subjective interpretation.
4.4 Determining particle count, size and shape are important in assessing contamination of fluids such as fuels, lubricating oils, water, injectables, and other liquids where particle contamination can affect their performance. Particle shape can point to the type and source of these particles which can help analysts improve process control.
4.5 Shape information is also advantageous in categorizing particles detected so as to not skew particle analysis results. For instance, if a flowing mixture of solid particles in liquid also contains gas bubbles or water droplets, it is important to be able to identify the bubbles and droplets and not count them as solid particles.
SCOPE
1.1 This guide provides information for determining particle size and shape using Dynamic Imaging Analyzers (DIA) in multiple application points including in-line, at-line and stand alone, lab based or portable, configurations. This guide focuses on concepts and strategies for applying imaging techniques to process applications in a way that improves the knowledge of the particles contained in dynamic flows, dry and wet, which can lead to more improved control of manufacturing processes.
1.2 Analyzers may be configured for open, dry or wet analysis, or enclosed, dry or wet analysis, as appropriate for analysis of the process or test specimen. Particles in liquid borne flows can be analyzed at least up to 1000 µm and dry particle flows can be analyzed up to several cm if equipment is appropriate for the size. Limitations will be discussed in Section 6.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
Standard ASTM E11 was completely revised with the -09 revision, and further in subsequent years to apply tolerances in conformance with truncated Gaussian normal distribution statistics. It covers the requirements for the sieve cloth itself, and for the design and construction of test sieves that use sieve cloth as a particle sizing medium to classify materials. This specification incorporates a maximum standard deviation value (where applicable) for the sieve cloth and for the Test Sieves. The maximum standard deviation values in Table 1 have been corrected by a K factor so as to increase the confidence level of the sieve cloth and the Test Sieve. Three (3) different inspection confidence levels are applied for Compliance, Inspection and Calibration Test Sieves; with Calibration Test Sieves having at least twice as many openings measured as Inspection Sieves. Similar to previous ASTM E11 revisions the specification covers the Test Sieve and its construction; standard frame sizes, non-standard frames, dimensional information, characteristics of the sieve frame, materials of construction for the sieve frame, attachment of the sieve cloth to the sieve frame, and specifies how test sieves should be labeled. Lastly, the specification Annex discusses in detail the proper procedure for inspection of the sieve cloth and the test sieve, to ensure that it complies with the requirements as shown in Table 1 of the specification.
SCOPE
1.1 This document specifies the technical requirements for; the woven wire test sieve cloth (sieve cloth) used in test sieves, the construction of test sieves, standard and non-standard test sieve frame sizes, and test procedures used to inspect sieve cloth and the test sieves. This specification applies to test sieves manufactured with sieve cloth having a nominal aperture size ranging from 125 millimetres (mm) down to 20 micrometres (μm).
1.2 Additional reference information can be found in Specifications E161, E323, E2016, and in Test Methods C430 and E2427.
1.3 The values stated in SI units shall be considered standard for the dimensions of the sieve cloth openings and the wire diameters used in the sieve cloth. The values stated in inch-pound units shall be considered standard with regard to the sieve frames, pans, and covers.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Technical specification12 pagesEnglish languagesale 15% off
- Technical specification12 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
4.1 This test method may be used by producers, users, and general interest parties for research and development or production quality control work, and is useful for the comparison of test sieves.
4.2 Because the reference material’s particle size distribution will affect the acceptance tolerance, the user should determine an acceptance tolerance based on their specific reference material.
SCOPE
1.1 This test method is a performance test for acceptance of test sieves.
1.2 This test method compares the performance of an E11 test sieve against an inspection or calibration test sieve using a known quantity of reference material such that the long-term stability of test sieves can be measured.
1.3 This is a test method for checking the accuracy and long-term reliability of test sieves. Since it is not possible to adjust the measuring capability of a test sieve, the test method is designed to offer a verification procedure based on sieving performance by comparison to a standard reference. This test method is not proposed as an alternative to the inspection methods in accordance with Specification E11 or the procedures in MNL 32.
1.4 Units—The values stated in SI units are to be regarded as standard. The additional values given are included for information only and are not considered standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard4 pagesEnglish languagesale 15% off
- Standard4 pagesEnglish languagesale 15% off
ABSTRACT
This specification covers the special grade of industrial woven wire cloth, referred to as filter cloth (also known as, Dutch weave or Hollander weave), for general filtration including the separation of solids from fluids (liquids or gases), based on a desired particle size retention. Filter cloth can be made of any primary metal or metal alloy wire that is suitable for weaving, and is woven with a greater number of wires in one direction than the other, and utilizing two different wire diameters. E2814 introduces standard terms and definitions, observes common technical considerations that a user should be aware of, and presents alternative acceptance criteria based on a desired pore size, or micron retention filtration rating.
SCOPE
1.1 This specification covers the special grade of industrial woven wire cloth, referred to as filter cloth, for general filtration including the separation of solids from fluids (liquids or gases), based on a desired particle size retention. Filter cloth can be made of any primary metal or metal alloy wire that is suitable for weaving.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Technical specification15 pagesEnglish languagesale 15% off
- Technical specification15 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
4.1 This test method permits a user to compare the performance of an instrument to the tolerance limit specifications stated by a manufacturer and to verify that an instrument is suitable for continued routine use. It also provides for generation of calibration data on a periodic basis, forming a database from which any changes in the performance of the instrument will be evident.
4.2 This test method for the calibration verification of laser diffraction particle sizing instruments is suitable for acceptance testing of laser diffraction instruments so long as current estimates of the bias (see Section 11) and the between-laboratory precision of the test method (see Section 10) are acceptably small relative to typical laser diffraction instrument accuracy specifications; see Practice D3244.
SCOPE
1.1 This test method describes a procedure necessary to permit a user to easily verify that a laser diffraction particle sizing instrument is operating within tolerance limit specifications, for example, such that the instrument accuracy is as stated by the manufacturer. The recommended calibration verification method provides a decisive indication of the overall performance of the instrument at the calibration point or points, but it is specifically not to be inferred that all factors in instrument performance are verified. In effect, use of this test method will verify the instrument performance for applications involving spherical particles of known refractive index where the near-forward light scattering properties are accurately modeled by the instrument data processing and data reduction software. The precision and bias limits presented herein are, therefore, estimates of the instrument performance under ideal conditions. Nonideal factors that could be present in actual applications and that could significantly increase the bias errors of laser diffraction instruments include vignetting4 (that is, where light scattered at large angles by particles far away from the receiving lens does not pass through the receiving lens and therefore does not reach the detector plane), the presence of nonspherical particles, the presence of particles of unknown refractive index, and multiple scattering.
1.2 This test method shall be used as a significant test of the instrument performance. While the procedure is not designed for extensive calibration adjustment of an instrument, it shall be used to verify quantitative performance on an ongoing basis, to compare one instrument performance with that of another, and to provide error limits for instruments tested.
1.3 This test method provides an indirect measurement of some of the important parameters controlling the results in particle sizing by laser diffraction. A determination of all parameters affecting instrument performance would come under a calibration adjustment procedure.
1.4 This test method shall be performed on a periodic and regular basis, the frequency of which depends on the physical environment in which the instrumentation is used. Thus, units handled roughly or used under adverse conditions (for example, exposed to dust, chemical vapors, vibration, or combinations thereof) shall undergo a calibration verification more frequently than those not exposed to such conditions. This procedure shall be performed after any significant repairs are made on an instrument, such as those involving the optics, detector, or electronics.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally rec...
- Standard12 pagesEnglish languagesale 15% off
This document describes a method for the evaluation of porosity and pore size distribution by physical adsorption (or physisorption). The method is limited to the determination of the quantity of a gas adsorbed per unit mass of sample as a function of pressure at a controlled, constant temperature[1]-[9]. Commonly used adsorptive gases for physical adsorption characterization include nitrogen, argon, krypton at the temperatures of liquid nitrogen and argon (77 K and 87 K respectively) as well as CO2 (at 273 K). Traditionally, nitrogen and argon adsorption at 77 K and 87 K, respectively, allows one to assess pores in the approximate range of widths 0,45 nm to 50 nm, although improvements in temperature control and pressure measurement allow larger pore widths to be evaluated. CO2 adsorption at 273 K – 293 K can be applied for the microporous carbon materials exhibiting ultramicropores. Krypton adsorption at 77 K and 87 K is used to determine the surface area or porosity of materials with small surface area or for the analysis of thin porous films. The method described is suitable for a wide range of porous materials. This document focuses on the determination of pore size distribution from as low as 0,4 nm up to approximately 100 nm. The determination of surface area is described in ISO 9277. The procedures which have been devised for the determination of the amount of gas adsorbed may be divided into two groups: - those which depend on the measurement of the amount of gas removed from the gas phase, i.e. manometric (volumetric) methods; - those which involve the measurement of the uptake of the gas by the adsorbent (i.e. direct determination of increase in mass by gravimetric methods). In practice, static or dynamic techniques can be used to determine the amount of gas adsorbed. However, the static manometric method is generally considered the most suitable technique for undertaking physisorption measurements with nitrogen, argon and krypton at cryogenic temperatures (i.e. 77 K and 87 K, the boiling temperature of nitrogen and argon, respectively) with the goal of obtaining pore volume and pore size information. This document focuses only on the application of the manometric method.
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SIGNIFICANCE AND USE
5.1 Using a geohazard netting as a medium to retain rock particles necessitates compatibility between it and the adjacent rock. These test methods measure the opening size of a geohazard netting which may be used to estimate the largest size of rocks or other objects that may pass through the geohazard netting without transferring load to the wire mesh or wire net.
5.2 These test methods may be applied to other components of the geohazard netting, such as regularly spaced reinforcement elements or secondary mesh openings.
5.3 These test methods may also be used for quality control during the manufacturing process and quality assurance that materials supplied conform to project or material specifications.
Note 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 These test methods are index tests to measure the opening size of a geohazard netting, or its components, or both, as it has been manufactured. They can be used for estimating the largest size of rock or other object that may pass through an individual opening in the geohazard netting without transferring load to the wire mesh or wire net and may also be used for quality control purposes. These test methods are not used to determine the maximum size rock or other object that the geohazard netting may contain through mobilization of the netting’s strength. These test methods do not apply to the measurement of the opening size of a geosynthetic, such as a turf reinforcement mat or geotextile, that may be manufactured as a composite system with the geohazard netting.
1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.
1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.
1.3.1 For purposes of comparing a measured or calculated value(s) with specified limits, the measured or calculated value(s) shall be rounded to the nearest decimal of significant digits in the specified limit.
1.3.2 The procedures used to specify how data are collected/recorded or calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objective; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT...
- Standard4 pagesEnglish languagesale 15% off
This document describes a method to transfer the images from particles having relative motion to binary images within practical systems, in which the particles in the images are individually separated. Images of moving particles are created by an optical image capture device. Effects of particle movement on the images are either minimized by the instrumentation or corrected by software procedures. This method is applicable to the particle images that are clearly distinguishable from static background. Further processing of the binary image, which is then considered as static, is described in ISO 13322-1. A dynamic image analysis system is capable of measuring a higher number of particles compared to static image analysis systems. This document provides guidance on instrument qualification for particle size distribution measurements by using particulate reference materials. This document addresses the relative movement of the particles with respect to each other, the effect of particle movement on the image (motion blur), the movement and position along the optical axis (depth of field), and the orientation of the particles with respect to the camera.
- Standard53 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
5.1 This test method is intended to be used for compliance with compositional specifications for particle size distribution. It is assumed that all who use this procedure will be trained analysts capable of performing common laboratory practices skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Follow appropriate quality control practices such as those described in Guide E882.
SCOPE
1.1 This test method covers the determination of the particle size distribution by screen analysis, dry or wet, of metal-bearing ores and related materials at 4.75 mm (No. 4) sieve and finer.
1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard4 pagesEnglish languagesale 15% off
- Standard4 pagesEnglish languagesale 15% off
This document establishes a generally applicable (i.e. not application specific) definition for dispersibility. It identifies significant characteristics for evaluating dispersibility and lists examples of methods used to characterize dispersibility in various applications. This document applies to processes that disperse powders into a liquid continuous phase while reducing the size of agglomerates or flocs down to the intended level, that homogenize an existing dispersed solid phase of a suspension or the mixture of two suspensions, or that exchange the original continuous phase in a suspension for another. Specific methods to disperse particles and to characterize the state of dispersion and/or homogeneity are only referenced, if necessary, for context. This document is applicable to nano- and micro-sized particles across a range of product applications.
- Technical specification22 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
4.1 This procedure was designed principally for clay, corncob, nut shell, paper, or sand granular carriers and granular pesticide products, but need not be limited to these materials. There may be more appropriate test methods for other types of granular carriers and products.
SCOPE
1.1 This test method is used to determine the particle size distribution of granular carriers and granular pesticides.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 6.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 The particle size distribution of RDF-5 strongly influences the storage and handling characteristics of the fuel. Small particles tend to block flow through storage bins and feed hoppers, although correct bin and hopper designs will alleviate this blockage problem.
4.2 This test method for measuring size manually allows for accurate description of RDF-5 particle size distribution. Manual measurement is superior to sieving techniques, wherein particles may be broken by the size separation technique itself. However, hand measurement is more time consuming than sieving techniques.
SCOPE
1.1 This test method is used to determine the size distribution of a RDF-5 sample. Size is defined as the maximum length of the particle, where length is determined by the RDF-5 manufacturing process. That is, a pellet, cubette, or briquette all have a recognizable length. Fig. 1 displays the sizes and shapes of some RDF-5 particles.
FIG. 1 RDF-5 Sizes
1.2 An air-dried RDF-5 sample is separated into categories of differing particle sizes. The size distribution is measured as the weight percentage of each size category. A graph of a function of the cumulative fraction of material by weight finer than particle size versus particle size is plotted. From this plot are taken values which describe the size distribution—the uniformity constant and the characteristic particle size.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method is intended to be used for compliance with compositional specifications for particle size distribution. It is assumed that all who use this procedure will be trained analysts capable of performing common laboratory practices skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Follow appropriate quality control practices such as those described in Guide E882.
SCOPE
1.1 This test method covers the determination of the particle size distribution by screen analysis of metal-bearing ores and related materials at 4.75 mm (No. 4) sieve and coarser.
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification covers perforated-plate sieves with either round or square apertures, normally mounted in a frame for use in precision testing in the classification of materials according to designated nominal particle size. The materials used in the manufacture of these sieves shall be steel, stainless steel, brass, bronze, or other rigid material. Each plate of specified sieve designation and aperture size shall conform to individually allocated dimensional requirements.
SCOPE
1.1 This specification covers perforated plate with either round or square apertures, normally mounted in a frame for use as sieves in precision testing in the classification of materials according to designated nominal particle size. A method for checking the accuracy of perforated sieve plates is included as information in Appendix X1.
Note 1: The perforated-plate sieves covered by this specification are intended for general precision testing. Some industries may require more restricted specifications for sieves for special testing purposes.
Note 2: For other types of sieves see Specifications E11 and E161.
Note 3: Complete instructions and procedures on the use of test sieves are contained in ASTM STP 447, Manual on Test Sieving Methods. This manual also contains a list of all ASTM published standards on sieve analysis procedures for specific materials or industries.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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