Standard Terminology Relating to Nonsieving Methods of Powder Characterization

SIGNIFICANCE AND USE
3.1 Interpretation and use of data generated by particle characterization methods is highly dependent on the definitions of terms describing that data. It is extremely important that those terms be defined in precisely the same way both when comparing data from different characterization techniques and even when correlating data from the same technique.  
3.2 It is likewise important that users of particle characterization methods and the data generated therefrom understand the principles of the methods, so that differences and similarities in the data can be interpreted in relation to those principles. That understanding can help to avoid disagreements when data from different characterization methods are compared.  
3.3 The definitions contained in this terminology will aid in the interpretation of particle characterization data with respect to the method(s) used to produce that data.
SCOPE
1.1 This terminology covers the definitions of terms used in the description and procedures of analysis of particulate materials not ordinarily analyzed using test sieves. The terms relate directly to the equipment used in analysis, the physical forms of the materials to be analyzed, and selected descriptive data reduction and analysis formats.  
1.2 Committee E29 on Particle and Spray Characterization believes that it is essential to include terms and definitions explicit to the committee’s scope, regardless of whether the terms appear in existing ASTM standards. Terms that are in common usage and appear in common-language dictionaries are generally not included, unless they have specific meanings in the context of particle characterization different from the common-language definitions.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Aug-2023
Drafting Committee
E29.02 - Non-Sieving Methods

Relations

Effective Date
01-Sep-2023
Effective Date
01-Sep-2023
Effective Date
01-Sep-2023
Effective Date
01-Sep-2023
Effective Date
01-Sep-2023
Effective Date
01-Sep-2023
Effective Date
01-Sep-2023

Overview

ASTM E2589-23a: Standard Terminology Relating to Nonsieving Methods of Powder Characterization is a key international standard developed by ASTM International. This standard defines essential terminology for the analysis and description of particulate materials by nonsieving methods. As nonsieving powder characterization is widely applied in industries such as pharmaceuticals, materials science, chemicals, and manufacturing, standardizing language is critical for consistent interpretation of data across different laboratories, equipment, and methods.

The standard is maintained by ASTM Committee E29 on Particle and Spray Characterization, and it aligns with international best practices set forth by the World Trade Organization (WTO) Technical Barriers to Trade (TBT) Committee.

Key Topics

ASTM E2589-23a covers a broad range of terms and concepts related to nonsieving particle size analysis and measurement techniques, emphasizing:

  • Definitions of Key Terms: Clear, precise definitions for common and specialized terms in powder characterization, such as particle size, particle size distribution, mean and median particle size, cumulative distribution, mode, roundness, and sphericity.
  • Methods and Technologies: Terminology surrounding analytical methods which do not use sieves, including dynamic image analysis, static light scattering, sedimentation analysis, and electrical sensing zone analysis.
  • Descriptive Formats and Calculations: Terms defining data reduction, analysis formats, as well as specific measurements like Feret diameter, equivalent diameter, and others.
  • Image Analysis: Definitions specific to digital image analysis, such as area, aspect ratio, binarization, binary object, and perimeter.
  • Powder and Particle Attributes: Terms describing physical characteristics like dispersion, emulsion, porosity, open pore, blind pore, and primary particle.

These well-established definitions reduce ambiguity and enhance inter-laboratory, inter-instrument, and intra-organization data comparisons.

Applications

The precise terminology of ASTM E2589-23a provides practical value across multiple industries and research fields, including:

  • Pharmaceuticals: For quality control and regulatory compliance, understanding particle size and distribution affects drug dissolution rates, bioavailability, and stability.
  • Materials Science: Accurate powder analysis is essential in ceramics, metallurgy, additive manufacturing, and composites, where powder characteristics influence final product performance.
  • Chemicals and Catalysts: Particle size and surface area directly impact reactivity and process efficiency.
  • Industrial Manufacturing: Ensures uniformity and repeatability in products where powders or dispersions are key components.
  • Academic Research: Supplies a common scientific language, facilitating publication, collaboration, and peer review.

Adopting ASTM E2589-23a terminology avoids misunderstandings, supports method validation, and enables coherent reporting, especially when different nonsieving methods yield slightly different results.

Related Standards

ASTM E2589-23a is part of a larger body of standards on particle characterization. Key related standards include:

  • ASTM E2578 - Practice for Calculation of Mean Sizes/Diameters and Standard Deviations of Particle Size Distributions.
  • Other ASTM E29 Standards - Cover procedures and best practices in particle and spray characterization.

These standards are available through ASTM International and are regularly reviewed and updated. Users are encouraged to combine ASTM E2589-23a with related standards for a comprehensive approach to powder characterization.


Keywords: nonsieving methods, powder characterization, particle size, particle analysis, image analysis, ASTM E2589, powder measurement, surface area, ASTM International, particle measurement.

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Frequently Asked Questions

ASTM E2589-23a is a standard published by ASTM International. Its full title is "Standard Terminology Relating to Nonsieving Methods of Powder Characterization". This standard covers: SIGNIFICANCE AND USE 3.1 Interpretation and use of data generated by particle characterization methods is highly dependent on the definitions of terms describing that data. It is extremely important that those terms be defined in precisely the same way both when comparing data from different characterization techniques and even when correlating data from the same technique. 3.2 It is likewise important that users of particle characterization methods and the data generated therefrom understand the principles of the methods, so that differences and similarities in the data can be interpreted in relation to those principles. That understanding can help to avoid disagreements when data from different characterization methods are compared. 3.3 The definitions contained in this terminology will aid in the interpretation of particle characterization data with respect to the method(s) used to produce that data. SCOPE 1.1 This terminology covers the definitions of terms used in the description and procedures of analysis of particulate materials not ordinarily analyzed using test sieves. The terms relate directly to the equipment used in analysis, the physical forms of the materials to be analyzed, and selected descriptive data reduction and analysis formats. 1.2 Committee E29 on Particle and Spray Characterization believes that it is essential to include terms and definitions explicit to the committee’s scope, regardless of whether the terms appear in existing ASTM standards. Terms that are in common usage and appear in common-language dictionaries are generally not included, unless they have specific meanings in the context of particle characterization different from the common-language definitions. 1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE 3.1 Interpretation and use of data generated by particle characterization methods is highly dependent on the definitions of terms describing that data. It is extremely important that those terms be defined in precisely the same way both when comparing data from different characterization techniques and even when correlating data from the same technique. 3.2 It is likewise important that users of particle characterization methods and the data generated therefrom understand the principles of the methods, so that differences and similarities in the data can be interpreted in relation to those principles. That understanding can help to avoid disagreements when data from different characterization methods are compared. 3.3 The definitions contained in this terminology will aid in the interpretation of particle characterization data with respect to the method(s) used to produce that data. SCOPE 1.1 This terminology covers the definitions of terms used in the description and procedures of analysis of particulate materials not ordinarily analyzed using test sieves. The terms relate directly to the equipment used in analysis, the physical forms of the materials to be analyzed, and selected descriptive data reduction and analysis formats. 1.2 Committee E29 on Particle and Spray Characterization believes that it is essential to include terms and definitions explicit to the committee’s scope, regardless of whether the terms appear in existing ASTM standards. Terms that are in common usage and appear in common-language dictionaries are generally not included, unless they have specific meanings in the context of particle characterization different from the common-language definitions. 1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM E2589-23a is classified under the following ICS (International Classification for Standards) categories: 19.120 - Particle size analysis. Sieving. The ICS classification helps identify the subject area and facilitates finding related standards.

ASTM E2589-23a has the following relationships with other standards: It is inter standard links to ASTM E2589-23, ASTM E2980-20, ASTM E3060-23, ASTM E2651-19, ASTM D8392-22, ASTM E3338-22, ASTM E1638-22. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

ASTM E2589-23a is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.

Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E2589 − 23a
Standard Terminology Relating to
Nonsieving Methods of Powder Characterization
This standard is issued under the fixed designation E2589; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
Particle size distribution, surface area, and other forms of particle analysis have been commonly
adopted methods of verifying compliance with desired particle specifications for some time. Greater
emphasis is now being placed on inter- and intralaboratory correlation of all particle measurement
systems.
To ensure a better understanding of the comparison of testing results from particle measurement
systems, terminology relating to the measurements must be clearly defined and documented so that
both the recipient and generator of the data are in full agreement as to the meaning of the data. Every
effort has been made here to ensure accuracy, precision, and clarity for the terms included in this
terminology document. For Committee E29, this is an ongoing process with new terms being
developed and defined for future inclusion. Suggestions and comments for additions, corrections, and
revisions are welcomed.
1. Scope 2. Referenced Documents
2.1 ASTM Standards:
1.1 This terminology covers the definitions of terms used in
E2578 Practice for Calculation of Mean Sizes/Diameters and
the description and procedures of analysis of particulate
Standard Deviations of Particle Size Distributions
materials not ordinarily analyzed using test sieves. The terms
relate directly to the equipment used in analysis, the physical
3. Significance and Use
forms of the materials to be analyzed, and selected descriptive
3.1 Interpretation and use of data generated by particle
data reduction and analysis formats.
characterization methods is highly dependent on the definitions
1.2 Committee E29 on Particle and Spray Characterization of terms describing that data. It is extremely important that
those terms be defined in precisely the same way both when
believes that it is essential to include terms and definitions
comparing data from different characterization techniques and
explicit to the committee’s scope, regardless of whether the
even when correlating data from the same technique.
terms appear in existing ASTM standards. Terms that are in
common usage and appear in common-language dictionaries
3.2 It is likewise important that users of particle character-
are generally not included, unless they have specific meanings
ization methods and the data generated therefrom understand
in the context of particle characterization different from the
the principles of the methods, so that differences and similari-
common-language definitions.
ties in the data can be interpreted in relation to those principles.
That understanding can help to avoid disagreements when data
1.3 This international standard was developed in accor-
from different characterization methods are compared.
dance with internationally recognized principles on standard-
3.3 The definitions contained in this terminology will aid in
ization established in the Decision on Principles for the
the interpretation of particle characterization data with respect
Development of International Standards, Guides and Recom-
to the method(s) used to produce that data.
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
4. Terminology
area, A, n—in image analysis, sum of pixels representing a
binary object.
This terminology is under the jurisdiction of ASTM Committee E29 on Particle
and Spray Characterization and is the direct responsibility of Subcommittee E29.02
on Non-Sieving Methods. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Sept. 1, 2023. Published October 2023. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 2007. Last previous edition approved in 2023 as E2589 – 23. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/E2589-23A. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
E2589 − 23a
aspect ratio, n—in image analysis, ratio of the maximum to equivalent spherical diameter, n—diameter of a sphere that
the minimum dimensions as determined by the technique. has the same geometrical characteristics (projected area,
volume, etc.) or the same behavior (settling, light scattering,
binarization, n—in image analysis, process of reducing a
etc.) as the particle under analysis.
digital image to a binary image.
equivalent Stokes diameter, n—the diameter of a sphere of
binary object, n—in image analysis, set of connected binary
the same density as the particle under analysis, undergoing
pixels representing the two dimensional projection of a
the same limiting velocity when moving in the same medium
particle.
under laminar flow conditions.
binary image, n—in image analysis, image formed by an array
equivalent surface area diameter, n—the diameter of a sphere
of pixels having only two possible values, representing
that has the same surface area as the particle under analysis.
objects and background, as a result of binarization. Synony-
mous with binary plane and bitplane. equivalent volume diameter, n—diameter of a sphere that has
the same volume as the particle under analysis.
blind pore, n—open pore having only a single connection with
an external surface. Feret diameter, F, n—distance between two parallel tangents
on opposite side of a binary object. Synonymous with Feret
circularity, C, n—in image analysis, a measure of the similar-
dimension.
ity of a particle’s image to the shape of a circle and defined
as C = √(4πA/P ), where A is the area of the particle’s image frequency distribution, n—the representation of the relative
and P is the perimeter of the particle’s image. fractions of a particle size distribution represented by (or
associated with) discrete size values (recognizing that an
convex perimeter, P , n—in image analysis, total length of
C
individual value may represent a range of values).
line segments connecting the Feret tangent points around a
binary object. maximum Feret diameter, F , n—longest Feret dimension
max
DISCUSSION—This is the perimeter that would be obtained if a rubber
found for a binary object. Synonymous with maximum Feret
band was stretched around the object.
dimension.
DISCUSSION—Refer to Fig. 1 for clarity.
cumulative distribution, n—the representation of the total
fraction of the population, expressed as either mass-,
mean particle size, n—a measure of the central tendency of a
volume-, area-, or number-based, that is greater than or less
particle size distribution, according to the Moment-Ratio
than discrete size val
...


This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E2589 − 23 E2589 − 23a
Standard Terminology Relating to
Nonsieving Methods of Powder Characterization
This standard is issued under the fixed designation E2589; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
Particle size distribution, surface area, and other forms of particle analysis have been commonly
adopted methods of verifying compliance with desired particle specifications for some time. Greater
emphasis is now being placed on inter- and intralaboratory correlation of all particle measurement
systems.
To ensure a better understanding of the comparison of testing results from particle measurement
systems, terminology relating to the measurements must be clearly defined and documented so that
both the recipient and generator of the data are in full agreement as to the meaning of the data. Every
effort has been made here to ensure accuracy, precision, and clarity for the terms included in this
terminology document. For Committee E29, this is an ongoing process with new terms being
developed and defined for future inclusion. Suggestions and comments for additions, corrections, and
revisions are welcomed.
1. Scope
1.1 This terminology covers the definitions of terms used in the description and procedures of analysis of particulate materials not
ordinarily analyzed using test sieves. The terms relate directly to the equipment used in analysis, the physical forms of the materials
to be analyzed, and selected descriptive data reduction and analysis formats.
1.2 Committee E29 on Particle and Spray Characterization believes that it is essential to include terms and definitions explicit to
the committee’s scope, regardless of whether the terms appear in existing ASTM standards. Terms that are in common usage and
appear in common-language dictionaries are generally not included, unless they have specific meanings in the context of particle
characterization different from the common-language definitions.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2.1 ASTM Standards:
E2578 Practice for Calculation of Mean Sizes/Diameters and Standard Deviations of Particle Size Distributions
This terminology is under the jurisdiction of ASTM Committee E29 on Particle and Spray Characterization and is the direct responsibility of Subcommittee E29.02 on
Non-Sieving Methods.
Current edition approved Feb. 15, 2023Sept. 1, 2023. Published March 2023October 2023. Originally approved in 2007. Last previous edition approved in 20222023 as
E2589 – 22.E2589 – 23. DOI: 10.1520/E2589-23.10.1520/E2589-23A.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
E2589 − 23a
3. Significance and Use
3.1 Interpretation and use of data generated by particle characterization methods is highly dependent on the definitions of terms
describing that data. It is extremely important that those terms be defined in precisely the same way both when comparing data
from different characterization techniques and even when correlating data from the same technique.
3.2 It is likewise important that users of particle characterization methods and the data generated therefrom understand the
principles of the methods, so that differences and similarities in the data can be interpreted in relation to those principles. That
understanding can help to avoid disagreements when data from different characterization methods are compared.
3.3 The definitions contained in this terminology will aid in the interpretation of particle characterization data with respect to the
method(s) used to produce that data.
4. Terminology
area, A,n—in image analysis, sum of pixels representing a binary object.
aspect ratio, n—in image analysis, ratio of the maximum to the minimum dimensions as determined by the technique.
binarization, n—in image analysis, process of reducing a digital image to a binary image.
binary object, n—in image analysis, set of connected binary pixels representing the two dimensional projection of a particle.
binary image, n—in image analysis, image formed by an array of pixels having only two possible values, representing objects
and background, as a result of binarization. Synonymous with binary plane and bitplane.
blind pore, n—open pore having only a single connection with an external surface.
circularity, C,n—in image analysis, a measure of the similarity of a particle’s image to the shape of a circle and defined as C
= √(4πA/P ), where A is the area of the particle’s image and P is the perimeter of the particle’s image.
convex perimeter, P ,n—in image analysis, total length of line segments connecting the Feret tangent points around a binary
C
object.
DISCUSSION—
This is the perimeter that would be obtained if a rubber band was stretched around the object.
cumulative distribution, n—the representation of the total fraction of the population, expressed as either mass-, volume-, area-,
or number-based, that is greater than or less than discrete size values.
dispersion, n—system consisting of particles distributed in a solid, liquid, or gas.
dynamic image analysis, n—particle size and shape analysis using computer image analysis techniques on instantaneously-
captured still-frame projected images of particles in motion.
DISCUSSION—
Some instruments use a moving measurement apparatus on static particles.
electrical sensing zone analysis, n—particle size analysis in which particles suspended in a conductive liquid medium pass
through a narrow orifice in an insulating material separating two electrodes. Each traversing particle generates an electrical
signal proportional to its volume.
electrical sensing zone equivalent spherical diameter, n—diameter of a hypothetical spherical particle that when suspended
in a conducting fluid would yield the same electrical signal as the particle under analysis.
E2589 − 23a
emulsion, n—a system that consists of one liquid dispersed in another.
equivalent aerodynamic diameter, n—the diameter of a unit density sphere that has the same inertial properties as the particle
under analysis, under the same conditions
equivalent area diameter, D,n—in image analysis, diameter of a circle having the same area as the binary object. Syno
...

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