EN 15002:2015
(Main)Characterization of waste - Preparation of test portions from the laboratory sample
Characterization of waste - Preparation of test portions from the laboratory sample
This European Standard is applicable for the preparation of representative test portions from the laboratory sample that has been taken according to the sampling plan (EN 14899), prior to physical and/or chemical analysis (e.g. preparation of eluates, extractions, digestion and/or analytical determinations) of solid (including monolithic material) and liquid samples and sludge. It is also applicable for the preparation of test portions from digests and eluates for the subsequent analyses.
This European Standard is intended to find the correct sequence of operations and treatments to be applied to the laboratory sample in order to obtain suitable test portions in compliance with the specific requirements defined in the corresponding analytical procedures.
Charakterisierung von Abfällen - Herstellung von Prüfmengen aus der Laborprobe
Diese Europäische Norm ist anwendbar bei der Aufbereitung von repräsentativen Prüfmengen aus der Laborprobe, die nach dem Probenahmeplan (EN 14899) entnommen wurde; vor der physikalischen und/oder chemischen Analyse (z. B. Herstellung von Eluaten, Extraktionen, Aufschlüsse und/oder analytische Bestimmungen) von festen (inklusive monolithischem Material) und flüssigen Proben sowie von Schlamm. Sie gilt auch für die Vorbereitung von Prüfmengen aus Aufschlüssen und Eluaten für die anschließende Analyse.
Diese Europäische Norm ist dafür vorgesehen, die richtige Reihenfolge von Arbeitsschritten und Behandlungen herauszufinden, die auf die Laborproben anzuwenden sind, um geeignete Prüfmengen unter Beachtung der in den entsprechenden Analysenverfahren festgelegten spezifischen Anforderungen zu erhalten.
Caractérisation des déchets - Préparation de prises d'essai à partir de l'échantillon pour laboratoire
La présente Norme européenne s'applique pour la préparation de prises d'essai représentatives à partir de l'échantillon pour laboratoire qui a été prélevé conformément au plan d'échantillonnage (EN 14899), avant analyse physique et/ou chimique (par exemple, préparation d'éluats, extractions, digestion et/ou déterminations analytiques) de boues et d'échantillons solides (y compris des matériaux monolithiques) et liquides. Elle est également applicable pour la préparation de prises d'essai à partir de digestats et d'éluats, en vue d'analyses ultérieures.
La présente Norme européenne a pour objet de déterminer la séquence correcte d'opérations et de traitements à appliquer à l'échantillon pour laboratoire afin d'obtenir des prises d'essai convenables conformément aux exigences spécifiques définies dans les modes opératoires d'analyse correspondants.
Karakterizacija odpadkov - Priprava preskusnih vzorcev iz laboratorijskega vzorca
General Information
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Standards Content (Sample)
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Karakterizacija odpadkov - Priprava preskusnih vzorcev iz laboratorijskega vzorcaCharaktersierung von Abfällen - Herstellung von Prüfmengen aus der LaboratoriumsprobeCaractérisation des déchets - Préparation de prises d'essai à partir de l'échantillon pour laboratoireCharacterization of waste - Preparation of test portions from the laboratory sample13.030.01Odpadki na splošnoWastes in generalICS:Ta slovenski standard je istoveten z:EN 15002:2015SIST EN 15002:2015en,fr,de01-julij-2015SIST EN 15002:2015SLOVENSKI
STANDARDSIST EN 15002:20061DGRPHãþD
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 15002
April 2015 ICS 13.030.01 Supersedes EN 15002:2006English Version
Characterization of waste - Preparation of test portions from the laboratory sample
Caractérisation des déchets - Préparation de prises d'essai à partir de l'échantillon pour laboratoire
Charakterisierung von Abfällen - Herstellung von Prüfmengen aus der Laborprobe This European Standard was approved by CEN on 7 February 2015.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2015 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 15002:2015 ESIST EN 15002:2015
Guideline for choosing sample treatment techniques . 13 A.1 General . 13 A.2 Homogenization . 13 A.2.1 General information . 13 A.2.2 Solid samples . 13 A.2.3 Liquid samples . 14 A.2.4 Homogenization in case of volatile compounds . 15 A.3 Phase/fraction separation . 15 A.3.1 General information . 15 A.3.2 Solid – liquid separation . 15 A.3.3 Liquid – liquid separation . 17 A.3.4 Solid – solid separation; separation into different fractions . 18 A.4 Drying . 19 A.4.1 General information . 19 A.4.2 Procedures . 19 A.5 Particle size reduction . 21 A.5.1 General information . 21 A.5.2 Procedures . 22 A.6 Sub-sampling . 24 A.6.1 General information . 24 A.6.2 Manual division of solid samples by coning and quartering . 24 A.6.3 Dry cutting . 25 A.6.4 Mechanical division of solid samples . 25 A.6.5 Sub-sampling for volatile compounds . 26 A.6.6 Sub-sampling for moderately volatile organic compounds . 26 SIST EN 15002:2015
Relationship between minimum amount of (sub-)sample and particle size. 28 B.1 Formula for the estimation of the minimum amount of (sub-)sample: . 28 B.2 Empirical rule . 29 Annex C (informative)
Sample treatment equipment . 30 Annex D (informative)
Examples for analytical methods . 31 Annex E (informative)
Examples for preparation of test samples . 37 E.1 Example 1 . 37 E.2 Example 2 . 41 Bibliography . 49
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