ISO/IEC 80079-20-2:2016
(Main)Explosive atmospheres — Part 20-2: Material characteristics — Combustible dusts test methods
Explosive atmospheres — Part 20-2: Material characteristics — Combustible dusts test methods
ISO/IEC 80079-20-2:2016 is published as a dual logo standard and describes the test methods for the identification of combustible dust and combustible dust layers in order to permit classification of areas where such materials exist for the purpose of the proper selection and installation of electrical and mechanical equipment for use in the presence of combustible dust. The standard atmospheric conditions for determination of characteristics of combustible dusts are: - temperature -20 °C to 60 °C, - pressure 80 kPa (0,8 bar) to 110 kPa (1,1 bar) and - air with normal oxygen content, typically 21 % v/v. The test methods defined do not apply to: - recognized explosives, propellants (e.g. gunpowder, dynamite), or substances or mixtures of substances which may, under some circumstances, behave in a similar manner or - dusts of explosives and propellants that do not require atmospheric oxygen for combustion, or to pyrophoric substances. This first edition cancels and replaces the first edition of IEC 61241-2-1 published in 1994, the first edition of IEC 61241-2-2 published in 1993 and the first edition of IEC 61241-2-3 published in 1994, combining the requirements into a single document, and is considered to constitute a technical revision. Significant changes with respect to IEC 61241-2-1:1994, IEC 61241-2-2:1993 and IEC 61241-2-3:1994 can be found in the foreword of the document. Keywords: combustible dust
Atmosphères explosives — Partie 20-2: Caractéristiques des produits — Méthodes d’essai des poussières combustibles
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ISO/IEC 80079-20-2
Edition 1.0 2016-02
INTERNATIONAL
STANDARD
NORME
INTERNATIONALE
Explosive atmospheres –
Part 20-2: Material characteristics – Combustible dusts test methods
Atmosphères explosives –
Partie 20-2: Caractéristiques des produits – Méthodes d’essai des poussières
combustibles
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ISO/IEC 80079-20-2
Edition 1.0 2016-02
INTERNATIONAL
STANDARD
NORME
INTERNATIONALE
Explosive atmospheres –
Part 20-2: Material characteristics – Combustible dusts test methods
Atmosphères explosives –
Partie 20-2: Caractéristiques des produits – Méthodes d’essai des poussières
combustibles
INTERNATIONAL
ELECTROTECHNICAL
COMMISSION
COMMISSION
ELECTROTECHNIQUE
INTERNATIONALE
ICS 13.230; 29.260.20 ISBN 978-2-8322-3179-1
– 2 – ISO/IEC 80079-20-2:2016
ISO/IEC 2016
CONTENTS
FOREWORD . 5
1 Scope . 8
2 Normative references. 8
3 Terms and definitions . 8
4 Dust sample requirements . 9
4.1 Receipt of sample for testing . 9
4.2 Characterisation of sample . 9
4.3 Preparation of sample . 10
4.4 Test conditions . 10
5 Combustible dusts and combustible flyings determination . 10
5.1 Test sequence . 10
5.2 Tests to determine whether material is a combustible dust or combustible
flying . 10
5.2.1 Visual inspection . 10
5.2.2 Determine particle distribution . 11
5.2.3 Ignition test in the Hartmann tube . 11
5.2.4 Ignition test in the 20-litre sphere . 11
6 Procedure for characterisation of combustible dust or combustible flying . 11
7 Test methods for determination of whether a material is a combustible dust or a
combustible flying . 14
7.1 Modified Hartmann tube . 14
7.1.1 General . 14
7.1.2 Test equipment . 14
7.1.3 Test procedure . 15
7.2 20-litre sphere . 15
7.2.1 General . 15
7.2.2 Test equipment . 15
7.2.3 Test procedure . 16
7.3 Alternative method to 20-litre sphere for small test material quantities . 16
7.3.1 General . 16
7.3.2 Test equipment . 17
7.3.3 Test procedure . 17
8 Test methods for combustible dust determinations . 17
8.1 MIT of a dust cloud . 17
8.1.1 General . 17
8.1.2 GG furnace . 17
8.1.3 BAM furnace . 18
8.2 Test for MIT of dust layer . 19
8.2.1 General . 19
8.2.2 Heated surface . 19
8.2.3 Dust layers . 20
8.2.4 Dust layer temperature . 20
8.2.5 Ambient temperature measurements . 20
8.2.6 Dust layer temperature test method . 20
8.2.7 Recording of results . 21
8.3 Method for determining minimum ignition energy of dust/air mixtures . 22
ISO/IEC 2016
8.3.1 General . 22
8.3.2 Test equipment . 22
8.3.3 Test procedure . 23
8.3.4 Calibration for determination of minimum ignition energies (MIE) by
electrically generated high-voltage d.c. sparks . 24
8.3.5 Recording of test results . 24
8.4 Test on resistivity . 24
8.4.1 General . 24
8.4.2 Test equipment . 25
8.4.3 Test procedure . 25
8.4.4 Recording of test results . 26
9 Test report. 26
Annex A (normative) Measurement of temperature distribution on the surface of the
hot plate . 27
Annex B (informative) Godbert-Greenwald oven (GG) . 28
Annex C (informative) Examples of spark-generating systems . 29
C.1 General . 29
C.2 Triggering by auxiliary spark using three-electrode system . 30
C.3 Triggering by electrode movement . 31
C.4 Triggering by voltage increase (trickle-charging circuit) . 32
C.5 Triggering by auxiliary spark, using normal two-electrode system – Trigger
transformer in discharge circuit . 33
Annex D (normative) Vertical tube (modified Hartmann tube) apparatus . 34
Annex E (informative) 20-litre sphere . 35
Annex F (informative) BAM oven . 37
Annex G (informative) Data for dust explosion characteristics . 38
Annex H (informative) 1 m vessel . 39
H.1 Test principle . 39
H.2 Test apparatus . 39
H.3 Test conditions . 43
H.4 Test procedure . 43
Bibliography . 45
Figure 1 – Protocol for characterisation of combustible dust or combustible flying . 12
Figure 2 – Tests to define ability to form explosive dust atmosphere (combustible
dust/combustible flyings) . 13
Figure 3 – Tests to characterise combustible dust or combustible flying . 14
Figure 4 – Modified Hartmann tube . 23
Figure 5 – Measuring cell for powder resistivity . 25
Figure A.1 – Typical surface temperature distribution (method A) . 27
Figure B.1 – Vertical cross-section through the Godbert-Greenwald oven . 28
Figure C.1 – Circuit – Triggering by high-voltage relay, using a two-electrode system . 29
Figure C.2 – Apparatus for determining the minimum ignition energies of dust
(schematic) – Triggering by auxiliary spark using three-electrode system . 30
Figure C.3 – Apparatus for determining the minimum ignition energies of dust
(schematic) – Triggering by electrode movement . 31
Figure C.4 – Apparatus for determining the minimum ignition energies of dust
(schematic) – Triggering by voltage increase . 32
– 4 – ISO/IEC 80079-20-2:2016
ISO/IEC 2016
Figure C.5 – Apparatus for determining the minimum ignition energies for dust
(schematic) – Trigger transformer in discharge circuit . 33
Figure D.1 – Vertical tube apparatus (modified Hartmann tube) . 34
Figure E.1 – Test equipment 20-litre sphere (schematic) . 35
Figure E.2 – Cross-sectional view of rebound nozzle . 36
Figure E.3 – Plan view of rebound nozzle . 36
Figure E.4 – Cross-sectional view of dispersion cup . 36
Figure F.1 – Cross-sectional arrangement of BAM oven . 37
Figure H.1 – 1 m vessel (schematic) . 40
Figure H.2 – Location of the 6 mm holes in the semicircular dust dispenser . 41
Figure H.3 – Rebound nozzle . 42
Figure H.4 – Dispersion cup . 43
Table 1 – Example of ignition test report . 21
ISO/IEC 2016
INTERNATIONAL ELECTROTECHNICAL COMMISSION
____________
EXPLOSIVE ATMOSPHERES –
Part 20-2: Material characteristics –
Combustible dusts test methods
FOREWORD
1) The International Electrotechnical Commission (IEC) is a worldwide organization for standardization comprising
all national electrotechnical committees (IEC National Committees). The object of IEC is to promote
international co-operation on all questions concerning standardization in the electrical and electronic fields. To
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2) The formal decisions or agreements of IEC on technical matters express, as nearly as possible, an international
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6) All users should ensure that they have the latest edition of this publication.
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8) Attention is drawn to the Normative references cited in this publication. Use of the referenced publications is
indispensable for the correct application of this publication.
9) Attention is drawn to the possibility that some of the elements of this IEC Publication may be the subject of
patent rights. IEC shall not be held responsible for identifying any or all such patent rights.
International Standard ISO/IEC 80079-20-2 has been prepared by subcommittee 31M: Non-
electrical equipment and protective systems for explosive atmospheres, of IEC 31: Equipment
for explosive atmospheres.
It is published as a double logo standard.
This first edition cancels and replaces the first edition of IEC 61241-2-1 published in 1994, the
first edition of IEC 61241-2-2 published in 1993 and the first edition of IEC 61241-2-3
published in 1994, combining the requirements into a single document, and is considered to
constitute a technical revision.
– 6 – ISO/IEC 80079-20-2:2016
ISO/IEC 2016
The text of this standard is based on the following documents:
FDIS Report on voting
31M/102/FDIS 31M/108/RVD
Full information on the voting for the approval of this standard can be found in the report on
voting indicated in the above table. In ISO, the standard has been approved by 15 P-members
out of 21 having cast a vote.
This publication has been drafted in accordance with the ISO/IEC Directives, Part 2.
"A list of all parts in the IEC 60079 series, under the general title Explosive atmospheres, as
well as the International Standard 80079 series, can be found on the IEC website."
The committee has decided that the contents of this publication will remain unchanged until
the stability date indicated on the IEC web site under "http://webstore.iec.ch" in the data
related to the specific publication. At this date, the publication will be
• reconfirmed,
• withdrawn,
• replaced by a revised edition, or
• amended.
ISO/IEC 2016
Significant changes with respect to IEC 61241-2-1:1994, IEC 61241-2-2:1993 and
IEC 61241-2-3:1994
Type
Explanation of the significance of the Clause Minor and Extension Major technical
changes editorial changes changes
Normative references 2 X
Terms and Definitions 3 X
Dust sample Requirements 4 X
Combustible Dust Determination 5 X
Procedure for Characterisation of combustible 6 X
dust or combustible flying
Test methods for determination of a 7 X
combustible dust or a combustible flying
MIT of a dust cloud 8.1 X
MIT of a dust layer 8.2 X
MIE of a dust/air mixture 8.3 X
Tests on resistivity 8.4 X
Measurement of temperature distribution on Annex X
the surface of the hot plate A
Godbert-Greenwald oven Annex X
B
Examples of spark-generating systems Annex X
C
Vertical tube apparatus Annex X
D
20-litre sphere Annex X
E
BAM oven Annex F X
Data for dust explosion characteristics Annex X
G
1m vessel Annex X
H
– 8 – ISO/IEC 80079-20-2:2016
ISO/IEC 2016
EXPLOSIVE ATMOSPHERES –
Part 20-2: Material characteristics –
Combustible dusts test methods
1 Scope
This part of ISO/IEC 80079 describes the test methods for the identification of combustible
dust and combustible dust layers in order to permit classification of areas where such
materials exist for the purpose of the proper selection and installation of electrical and
mechanical equipment for use in the presence of combustible dust.
The standard atmospheric conditions for determination of characteristics of combustible dusts
are:
• temperature –20 °C to +60 °C,
• pressure 80 kPa (0,8 bar) to 110 kPa (1,1 bar) and
• air with normal oxygen content, typically 21 % v/v.
The test methods defined do not apply to:
• recognized explosives, propellants (e.g. gunpowder, dynamite), or substances or mixtures
of substances which may, under some circumstances, behave in a similar manner or
• dusts of explosives and propellants that do not require atmospheric oxygen for
combustion, or to pyrophoric substances.
2 Normative references
None.
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.
3.1
combustible dust
finely divided solid particles, 500 µm or less in nominal size, which may form explosive
mixtures with air at standard atmospheric pressure and temperatures
Note 1 to entry: This includes dust and grit as defined in ISO 4225.
Note 2 to entry: The term 'solid particles' is intended to address particles in the solid phase but does not preclude
a hollow particle.
3.1.1
conductive dust
combustible metal dusts and other combustible dusts with electrical resistivity equal to or less
than 1 × 10 Ω⋅m
Note 1 to entry: Metal dust is treated as conductive dust because it is assumed that surface oxidation cannot be
depended upon to always ensure electrical resistivity greater than 1 × 10 Ω⋅m
ISO/IEC 2016
3.1.2
non-conductive dust
combustible dust with electrical resistivity greater than 1 × 10 Ω⋅m
3.2
combustible flyings
solid particles, including fibres, where one dimension is greater than 500 µm in nominal size,
which may form an explosive mixture with air at standard atmospheric pressure and
temperature
Note 1 to entry: The ratio of length to width is 3 or more.
Note 2 to entry: Examples of flyings include carbon fibre, rayon, cotton (including cotton linters and cotton waste),
sisal, jute, hemp, cocoa fibre, oakum and baled waste kapok.
3.3
explosive dust atmosphere
mixture with air, under atmospheric conditions, of combustible substances in the form of dust,
fibres, or flyings which, after ignition, permits self-sustaining propagation
3.4
minimum ignition temperature of a dust layer
lowest temperature of a hot surface at which ignition occurs in a dust layer under specified
test conditions
3.5
minimum ignition temperature of a dust cloud
lowest temperature of a hot surface on which the most ignitable mixture of the dust with air is
ignited under specified test conditions
3.6
minimum ignition energy (of a combustible dust/air mixture)
lowest electrical energy stored in a capacitor which upon discharge is sufficient to effect
ignition of the most sensitive dust/air mixture under specified test conditions
4 Dust sample requirements
4.1 Receipt of sample for testing
A material safety data sheet or equivalent with the sample.
The test material shall be provided in suitable packaging, labelled according to relevant
guidelines labelled according to relevant guidelines, and appropriate transportation.
NOTE It is usual to provide a quantity of at least 0,5 kg for testing. If sample preparation is required this may be
insufficient. If only a smaller volume of material is available then the full range of testing may not be possible.
4.2 Characterisation of sample
The sample shall be representative of the material as it appears in the entire process
operated.
NOTE Many unit operations such as extract systems will separate dust into finer fractions than seen in the main
processing equipment and this is accounted for when taking the sample.
If the sample is not representative of the material as found in the process then sample
preparation shall be carried out to apply the worst case conditions.
At least the following information about the sample shall be provided:
– 10 – ISO/IEC 80079-20-2:2016
ISO/IEC 2016
– minimum particle size,
– median particle size,
– maximum particle size,
– particle distribution,
– moisture content, and
– method of determination (e.g. optical methods or sieving).
If the applicant cannot provide usable data then this shall be determined separately.
4.3 Preparation of sample
If it is not possible to test the sample as received, or if the sample is no longer representative
of the process material then it may be necessary to condition or alter the sample for testing.
This may include
– grinding/sieving,
– drying and
– humidifying.
Any apparent changes noted in the properties of the dust during preparation of the sample, for
example, by sieving or owing to temperature or humidity conditions, shall be stated in the test
report.
NOTE 1 Sample preparation such as grinding and sieving, or drying can alter the material characteristics. Where
finer fractions are present in a facility it is appropriate to take fractions of less than 63 µm to give the most easily
ignitable mixtures. When the sample is a mixture of substances, the sample preparation can result in a change to
the sample’s composition.
NOTE 2 The presence of solvents can become altered in the sample preparation process.
4.4 Test conditions
+10
The tests shall be carried out at standard atmospheric temperature of 20 °C and standard
−10
atmospheric pressure of 80 kPa to 110 kPa (0,8 bar to 1,1 bar) unless otherwise specified.
5 Combustible dusts and combustible flyings determination
5.1 Test sequence
The sequence followed for the determination of the material properties of combustible dust
and combustible flyings is given in 5.2, Clause 6 and Figure 1, Figure 2 and Figure 3.
NOTE 1 Refer also to the information referenced in Annex G.
NOTE 2 Testing in the Hartman tube is a screening method. The test procedure can be directly started with the
20 litre sphere or the GG Oven.
5.2 Tests to determine whether material is a combustible dust or combustible flying
5.2.1 Visual inspection
Make a visual inspection of the test material (by microscope if necessary) to determine
whether the material consists of combustible flyings:
• If the material consists of combustible flyings with dust then continue the test procedure in
a Hartmann tube (see 5.2.3) to determine whether the combination of the two is
combustible dust.
• If the material consists only of combustible flyings then continue the test procedure in a
Hartmann tube (see 5.2.3) to determine whether it is combustible flyings.
ISO/IEC 2016
5.2.2 Determine particle distribution
For material which does not contain combustible flyings check the particle size distribution:
• If there are no particles less than 500 µm in size then the material is not a combustible
dust.
• If there are any particles less than 500 µm in size then continue the test procedure in a
Hartmann tube to determine whether it is a combustible dust.
5.2.3 Ignition test in the Hartmann tube
5.2.3.1 Test in a Hartmann tube with a spark (see 7.1):
1) If ignition occurs, the material is a combustible dust or a combustible flying (proceed to the
procedure for characterisation of combustible dust or combustible flying (see Clause 6)).
2) If no ignition occurs:
a) proceed to a Hartmann tube with a hot coil ignition source (see 7.1);
b) it can be assumed that the minimum ignition energy is greater than 1 J and the test
material is hard to ignite.
5.2.3.2 Test in a Hartmann tube with a hot coil ignition source (see 7.1):
1) If ignition occurs, the material is a combustible dust or a combustible flying, (proceed to
the procedure for the characterisation of combustible dust or combustible flying (see
Clause 6).
2) If no ignition occurs:
a) proceed to the test in the 20-litre sphere (see 7.2);
b) it can be assumed that the minimum ignition energy is greater than 10 J.
5.2.4 Ignition test in the 20-litre sphere
Test in the 20-litre sphere (see 7.2):
• If ignition occurs the material is a combustible dust or a combustible flying (proceed to
procedure for characterisation of combustible dust or combustible flying (see Clause 6)).
• If no ignition occurs then the material is not a combustible dust or a combustible flying and
the testing procedure is completed.
NOTE Although the material does not form explosive mixtures with air, it can still ignite as a combustible dust
layer.
If there is insufficient material available for testing in a 20-litre sphere then testing in the
Godbert-Greenwald (GG) oven at 1 000 °C is an acceptable alternative (see 7.3):
• If no ignition occurs at 1 000 °C then the material is not a combustible dust or a
combustible flying.
• If there is an ignition at 1 000 °C then the material should be subject to further verification
in the 20-litre sphere before declaring it combustible or non-combustible.
6 Procedure for characterisation of combustible dust or combustible flying
The following is the procedure for the characterisation of combustible dust or combustible
flying:
– test for dust cloud minimum ignition temperature (MIT) (see Clause 8):
a) GG oven (see 8.1.2) or
b) BAM oven (see 8.1.3)
– test for dust layer MIT (see 8.2);
– 12 – ISO/IEC 80079-20-2:2016
ISO/IEC 2016
– test for minimum ignition energy (MIE) of dust cloud (see 8.3);
– test for resistivity of bulk dust (see 8.4).
IEC
Figure 1 – Protocol for characterisation of combustible dust or combustible flying
ISO/IEC 2016
IEC
Figure 2 – Tests to define ability to form explosive dust atmosphere
(combustible dust/combustible flyings)
– 14 – ISO/IEC 80079-20-2:2016
ISO/IEC 2016
IEC
Figure 3 – Tests to characterise combustible dust or combustible flying
7 Test methods for determination of whether a material is a combustible dust
or a combustible flying
7.1 Modified Hartmann tube
7.1.1 General
Dust is dispersed in a tube to form a dust cloud, and ignition trials are attempted with two
different ignition sources.
7.1.2 Test equipment
The test equipment consists of a vertical tube closed at the bottom with a dispersion cup
(volume approximately 1,2 l, internal diameter (70 ± 5) mm).
As ignition sources
ISO/IEC 2016
– a continuous induction spark (electrode gap of approximately 4 mm, with a transformer
rated approximately 15 kV, and approximately 0,2 kVA),
– a glowing coil (wire diameter approximately 1,2 mm, wire length approximately 470 mm,
coil diameter approximately 11 mm and wire temperature at least 1 000 °C)
The vertical separation between the bottom of the dispersion cup and the ignition source is
approximately 100 mm.
A detailed description of suitable equipment can be found in Annex D.
7.1.3 Test procedure
The test sample is deposited in the dispersion cup and dispersed with a blast of air (50 cm ,
700 kPa to 800 kPa gauge). The dust concentration is varied over a wide range from 250 g/m
3 3 3 3 3 3
to 1500 g/m (typically 250 g/m , 500 g/m , 750 g/m , 1 000 g/m and 1 500 g/m ) and the
behaviour is visually observed. The different quantities are each tested once, but repeated
dispersions are made for at least 3 attempts.
If a flame propagates from the ignition source, the test material is a combustible dust or
combustible flying.
If no ignitions are observed with the spark ignition source, then the coil ignition source is
used. Testing may be stopped immediately after an ignition is observed.
If it is unclear, whether ignition has been observed then the 20-litre sphere test shall be used.
NOTE 1 In the case of high density materials such as metals higher concentrations (e.g. up to 2 500 g/m ) are
used.
NOTE 2 Deposits on the coil can result in localised smouldering or burning, which is not considered as ignition.
7.2 20-litre sphere
7.2.1 General
Dust is dispersed in a pressure resistant closed apparatus (20-litre sphere) to form a dust
cloud under standard conditions of pressure and temperature. Ignition trials are attempted
with pyrotechnic igniters.
As an alternative method, the 1 m vessel can be used (see Annex H).
7.2.2 Test equipment
The standard test apparatus to determine dust cloud combustibility is a spherical explosion
pressure resistant vessel of 20 litres.
The main components of the test apparatus are:
• spherical explosion vessel;
• dust dispersion system (rebound nozzle);
• ignition source (2 × 1 000 J pyrotechnical igniters);
• control unit;
• pressure measuring system with two sensors (± 10 kPa);
• dispersion overpressure p = (2 000 ± 100) kPa;
z
• initial temperature T = (20 +/- 5) °C (water cooling).
i
A detailed description of suitable equipment can be found in Annex E.
– 16 – ISO/IEC 80079-20-2:2016
ISO/IEC 2016
NOTE 1 For flyings and very coarse materials other nozzles are typically used (see Annex E).
NOTE 2 The particle size of friable materials can be affected by the dispersing system.
7.2.3 Test procedure
Explosion tests with defined dust/air mixtures shall be carried out according to the following
procedure. The test material is dispersed in the explosion vessel by an air blast such that a
homogeneous dust cloud is created. Prior to the air blast the explosion vessel is evacuated to
a level such that immediately after dispersion the internal pressure of the vessel shall be
equal to standard atmospheric pressure.
3 3
The dust concentration is varied over a wide range from 250 g/m to 1 500 g/m (typically
3 3 3 3 3
250 g/m , 500 g/m , 750 g/m , 1 000 g/m and 1 500 g/m ) and the pressure increase is
measured. The different concentrations shall each be tested at least once.
The required amount of the dust is placed in the dust container. The bulk volume of the dust
shall not exceed ¾ of the dust container allowing proper pressurization. The amount of the
dust in the dust container has to be completely dispersed into the 20-litre-sphere. The
container is then pressurized to an overpressure of 2 000 kPa.
Before starting the test procedure the temperature inside the vessel shall be measured and
recorded.
After dispersion of dust the pressure in the 20-litre sphere shall be at atmospheric pressure.
The actual pressure in the 20-litre sphere at the moment of ignition (initial pressure p ) shall
i
be measured and recorded.
The delay between the initiation of the dust dispersion and the activation of the ignition source
) shall be 60 +/- 5 ms. The pressure is recorded as a function of time. From
(ignition delay t
v
the pressure/time curve the explosion pressure p is determined by taking the arithmetic
ex
mean of the maximum values measured by the pressure sensors (see Annex E).
If the difference in the pressures measured by the different pressure sensors is more than
10 kPa of the mean, the accuracy of the sensors shall be checked and the measurements
repeated.
An ignition of the dust (dust explosion) shall be considered to have taken place, if an
overpressure is detected which is equal to or greater than the overpressure created by the
ignition source alone in air plus 30 kPa.
If an ignition occurs, then the test material is a combustible dust or combustible flying, and
testing may be stopped.
If no ignition occurs for all concentrations it is not a combustible dust or combustible flying.
In the case of high density materials such as metals, higher concentrations (e.g. up to
2 500 g/m ) are permitted to be used.
After each test, the explosion vessel shall be cleaned.
7.3 Alternative method to 20-litre sphere for small test material quantities
7.3.1 General
Small quantities of dust are blown through a heated vertical tube (GG oven) at a temperature
of 1 000 °C and ignition is detected by visual inspection.
ISO/IEC 2016
7.3.2 Test equipment
The main components of the test apparatus are
• a furnace capable of achieving a wall temperature of 1 000 °C,
• a dust dispersion system including an air reservoir of 500 ml and
• a temperature control unit.
A detailed description of suitable equipment can be found in Annex B.
7.3.3 Test procedure
The test material is dispersed in the furnace by an air blast.
The dust quantity is varied from 0,3 g to 0,5 g.
The dust is dispersed with air at pressures varying between 10 kPa and 50 kPa.
If a burst of flame is seen below the end of the furnace tube the test material is a combustible
dust or a combustible flying.
If a burst of flame is not seen below the end of the furnace tube the test material is not a
combustible dust or combustible flying.
In case of uncertainties in the detection of flames the test material shall be considered to be a
combustible dust or combustible flying. The ultimate determination shall be from a 20-litre
sphere test as described in 7.2.
NOTE In the case of high density materials such as metals, higher quantities (e.g. up to 5,0 g) are typically used.
8 Test methods for combustible dust determinations
8.1 MIT of a dust cloud
8.1.1 General
There are two methods for measuring the MIT of the dust cloud outlined below, the GG
furnace in 8.1.2 or the BAM furnace in 8.1.3.
8.1.2 GG furnace
8.1.2.1 General
Small quantities of dust are blown vertically downward through a heated furnace and ignition
is detected by visual inspection.
8.1.2.2 Test equipment
The main components of the test apparatus are as shown in 7.3.1.
8.1.2.3 Test procedure
The test material is dispersed in the furnace by an air blast.
The dust quantity is varied over a wide range from 0,05 g to 0,5 g (typically 0,1 g, 0,2 g and
0,3 g). The dust is dispersed with air at pressures varying between 10 and 50 kPa (typically
10 kPa, 20 kPa, 30 kPa and 50 kPa).
– 18 – ISO/IEC 80079-20-2:2016
ISO/IEC 2016
In the absence of preliminary information the first test should be performed at a furnace wall
temperature of 500 °C, with a quantity of 0,3 g and an air pressure of 30 kPa.
If no ignition is observed at this temperature the temperature should be increased in steps of
50 K until 600 °C is reached.
Once ignition is obtained, vary the mass of test material and the dispersion pressure of the air
until the most vigorous ignition is apparent. Then using the same mass and dispersion
pressure carry out further tests with the temperature reduced in steps of 20 K until no ignition
is obtained after 10 attempts. If ignition still occurs at 300 °C reduce the temperature in steps
of 10 K.
When no ignition is obtained using this temperature redu
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