ASTM E2230-22
(Practice)Standard Practice for Thermal Qualification of Type B Packages for Radioactive Material
Standard Practice for Thermal Qualification of Type B Packages for Radioactive Material
SIGNIFICANCE AND USE
5.1 The major objective of this practice is to provide a common reference document for both applicants and certification authorities on the accepted practices for accomplishing package thermal qualification. Details and methods for accomplishing qualification are described in this document in more specific detail than available in the regulations. Methods that have been shown by experience to lead to successful qualification are emphasized. Possible problems and pitfalls that lead to unsatisfactory results are also described.
5.2 The work described in this standard practice shall be done under a quality assurance program that is accepted by the regulatory authority that certifies the package for use. For packages certified in the United States, 10 CFR 71 Subpart H shall be used as the basis for the quality assurance (QA) program, while for international certification, ISO 9000 usually defines the appropriate program. The quality assurance program shall be in place and functioning prior to the initiation of any physical or analytical testing activities and prior to submittal of any information to the certifying authority.
SCOPE
1.1 This practice defines detailed methods for thermal qualification of “Type B” radioactive materials packages under Title 10, Code of Federal Regulations, Part 71 (10CFR71) in the United States or, under International Atomic Energy Agency Regulation SSR-6. Under these regulations, packages transporting what are designated to be Type B quantities of radioactive material shall be demonstrated to be capable of withstanding a sequence of hypothetical accidents without significant release of contents.
1.2 The unit system (SI metric or English) used for thermal qualification shall be agreed upon prior to submission of information to the certification authority. If SI units are to be standard, then use IEEE/ASTM SI-10. Additional units given in parentheses are for information purposes only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.
1.5 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
General Information
- Status
- Published
- Publication Date
- 31-Dec-2021
- Technical Committee
- C26 - Nuclear Fuel Cycle
- Drafting Committee
- C26.13 - Spent Fuel and High Level Waste
Relations
- Effective Date
- 01-Jan-2024
- Effective Date
- 15-Dec-2018
- Effective Date
- 01-Mar-2018
- Effective Date
- 01-Aug-2015
- Effective Date
- 01-Aug-2015
- Effective Date
- 01-Feb-2015
- Effective Date
- 01-Oct-2014
- Effective Date
- 15-Aug-2014
- Effective Date
- 01-Aug-2014
- Effective Date
- 01-Jul-2014
- Effective Date
- 01-Apr-2013
- Effective Date
- 15-Dec-2012
- Effective Date
- 01-Nov-2012
- Effective Date
- 01-Oct-2012
- Effective Date
- 01-Aug-2010
Overview
ASTM E2230-22 is the internationally recognized standard practice for the thermal qualification of Type B packages intended for the transport of radioactive material. Developed by ASTM International, this standard establishes widely accepted methods and quality assurance requirements for demonstrating that Type B packages can safely withstand severe thermal environments, such as those that may occur during hypothetical accident conditions. It provides detailed guidance beyond basic regulatory requirements to help package designers, applicants, and certification authorities achieve robust and reliable thermal qualification.
Key Topics
- Thermal Qualification Methods: ASTM E2230-22 outlines four primary approaches for qualifying packages: qualification by analysis, pool fire testing, furnace testing, and radiant heat testing. The selection of method is influenced by package design, regulatory requirements, and environmental considerations.
- Regulatory Compliance: This standard addresses compliance with both U.S. regulations (Title 10, Code of Federal Regulations, Part 71) and international requirements (International Atomic Energy Agency SSR-6). Type B packages must be proven capable of surviving a sequence of hypothetical accident scenarios, particularly a 30-minute engulfing hydrocarbon fire at 800°C.
- Quality Assurance: Implementation of a quality assurance (QA) program is mandatory and must be accepted by the relevant regulatory authority prior to testing. U.S. certifications require compliance with 10 CFR 71 Subpart H, while international certifications usually reference ISO 9000 standards.
- Modeling and Simulation: The practice includes detailed recommendations on creating and using analytical models for steady-state and transient thermal analysis. It emphasizes proper material properties, model validation, and benchmarking of thermal codes for reliable results.
- Safety Considerations: ASTM E2230-22 highlights the importance of health, safety, and environmental safeguards due to the inherent hazards of fire testing and the handling of radioactive materials.
Applications
- Design and Certification of Nuclear Transport Packages: Package vendors and regulatory applicants use this standard to demonstrate that their designs meet stringent thermal endurance requirements during the transport of radioactive material.
- Approval Submissions: The methods described are used to prepare supporting documentation (such as Safety Analysis Reports for Packages, or SARP) for submission to certifying agencies.
- Performance Validation: Laboratory testing and advanced computational analysis performed as per ASTM E2230-22 underpin the validation of packages for domestic and international radioactive materials transport, covering all common transport modes.
- Risk Assessment: By thoroughly assessing the thermal response of Type B packages under extreme accidental fire conditions, organizations can minimize the risk of radioactive release during transport.
- Quality Management: The integration of robust QA standards ensures consistency, credibility, and traceability throughout the qualification, testing, and certification process.
Related Standards
- Title 10 CFR 71: U.S. regulations governing the packaging and transportation of radioactive material.
- IAEA SSR-6: International regulations for the safe transport of radioactive material.
- IEEE/ASTM SI-10: Standard for the use of the International System of Units (SI) in scientific and engineering work.
- ASME NQA-1: Quality Assurance Requirements for Nuclear Facility Applications.
- ISO 9000: Fundamental quality management systems standard.
- ASTM E176: Terminology of fire standards.
- NRC Regulatory Guide 7.9: Guidance for preparing and reviewing applications for packaging approval.
- ISO 13943: Fire safety - vocabulary.
By following the practices outlined in ASTM E2230-22, stakeholders ensure compliance with regulatory standards, promote the safe transport of radioactive materials, and support global nuclear safety and security initiatives. This standard is an indispensable reference for nuclear engineers, certification authorities, quality managers, and all professionals involved in the design, evaluation, and approval of Type B radioactive material transport packages.
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Frequently Asked Questions
ASTM E2230-22 is a standard published by ASTM International. Its full title is "Standard Practice for Thermal Qualification of Type B Packages for Radioactive Material". This standard covers: SIGNIFICANCE AND USE 5.1 The major objective of this practice is to provide a common reference document for both applicants and certification authorities on the accepted practices for accomplishing package thermal qualification. Details and methods for accomplishing qualification are described in this document in more specific detail than available in the regulations. Methods that have been shown by experience to lead to successful qualification are emphasized. Possible problems and pitfalls that lead to unsatisfactory results are also described. 5.2 The work described in this standard practice shall be done under a quality assurance program that is accepted by the regulatory authority that certifies the package for use. For packages certified in the United States, 10 CFR 71 Subpart H shall be used as the basis for the quality assurance (QA) program, while for international certification, ISO 9000 usually defines the appropriate program. The quality assurance program shall be in place and functioning prior to the initiation of any physical or analytical testing activities and prior to submittal of any information to the certifying authority. SCOPE 1.1 This practice defines detailed methods for thermal qualification of “Type B” radioactive materials packages under Title 10, Code of Federal Regulations, Part 71 (10CFR71) in the United States or, under International Atomic Energy Agency Regulation SSR-6. Under these regulations, packages transporting what are designated to be Type B quantities of radioactive material shall be demonstrated to be capable of withstanding a sequence of hypothetical accidents without significant release of contents. 1.2 The unit system (SI metric or English) used for thermal qualification shall be agreed upon prior to submission of information to the certification authority. If SI units are to be standard, then use IEEE/ASTM SI-10. Additional units given in parentheses are for information purposes only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions. 1.5 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
SIGNIFICANCE AND USE 5.1 The major objective of this practice is to provide a common reference document for both applicants and certification authorities on the accepted practices for accomplishing package thermal qualification. Details and methods for accomplishing qualification are described in this document in more specific detail than available in the regulations. Methods that have been shown by experience to lead to successful qualification are emphasized. Possible problems and pitfalls that lead to unsatisfactory results are also described. 5.2 The work described in this standard practice shall be done under a quality assurance program that is accepted by the regulatory authority that certifies the package for use. For packages certified in the United States, 10 CFR 71 Subpart H shall be used as the basis for the quality assurance (QA) program, while for international certification, ISO 9000 usually defines the appropriate program. The quality assurance program shall be in place and functioning prior to the initiation of any physical or analytical testing activities and prior to submittal of any information to the certifying authority. SCOPE 1.1 This practice defines detailed methods for thermal qualification of “Type B” radioactive materials packages under Title 10, Code of Federal Regulations, Part 71 (10CFR71) in the United States or, under International Atomic Energy Agency Regulation SSR-6. Under these regulations, packages transporting what are designated to be Type B quantities of radioactive material shall be demonstrated to be capable of withstanding a sequence of hypothetical accidents without significant release of contents. 1.2 The unit system (SI metric or English) used for thermal qualification shall be agreed upon prior to submission of information to the certification authority. If SI units are to be standard, then use IEEE/ASTM SI-10. Additional units given in parentheses are for information purposes only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions. 1.5 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM E2230-22 is classified under the following ICS (International Classification for Standards) categories: 13.300 - Protection against dangerous goods; 55.040 - Packaging materials and accessories. The ICS classification helps identify the subject area and facilitates finding related standards.
ASTM E2230-22 has the following relationships with other standards: It is inter standard links to ASTM E176-24, ASTM E176-18a, ASTM E176-18, ASTM E176-15a, ASTM E176-15ae1, ASTM E176-15, ASTM E176-14c, ASTM E176-14b, ASTM E176-14a, ASTM E176-14, ASTM E176-13, ASTM E176-12b, ASTM E176-12a, ASTM E176-12, ASTM E176-10a. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
ASTM E2230-22 is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.
Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation:E2230 −22
Standard Practice for
Thermal Qualification of Type B Packages for Radioactive
Material
This standard is issued under the fixed designation E2230; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
1.1 This practice defines detailed methods for thermal
2.1 ASTM Standards:
qualificationof“TypeB”radioactivematerialspackagesunder E176Terminology of Fire Standards
Title 10, Code of Federal Regulations, Part 71 (10CFR71) in
IEEE/ASTMSI-10International System of Units (SI) The
the United States or, under International Atomic Energy Modernized Metric System
Agency Regulation SSR-6. Under these regulations, packages
2.2 Federal Standard:
transporting what are designated to be Type B quantities of
Title 10, Code of Federal Regulations, Part 71
radioactive material shall be demonstrated to be capable of
(10CFR71), PackagingandTransportationofRadioactive
withstanding a sequence of hypothetical accidents without
Material, United States Government Printing Office, Oc-
significant release of contents.
tober 1, 2004
1.2 The unit system (SI metric or English) used for thermal
2.3 Nuclear Regulatory Commission Standards:
qualification shall be agreed upon prior to submission of
Standard Format and Content of Part 71 Applications for
information to the certification authority. If SI units are to be
Approval of Packaging of Type B Large Quantity and
standard, then use IEEE/ASTMSI-10. Additional units given
Fissile Radioactive Material, Regulatory Guide
in parentheses are for information purposes only.
7.9, United States Nuclear Regulatory Commission,
1.3 This standard does not purport to address all of the
United States Government Printing Office, 1986
safety concerns, if any, associated with its use. It is the
2.4 International Atomic Energy Agency Standards:
responsibility of the user of this standard to establish appro-
Regulations for the Safe Transport of Radioactive Material,
priate safety, health, and environmental practices and deter-
No. SSR-6 (IAEA SSR-6 Revised)International Atomic
mine the applicability of regulatory limitations prior to use.
Energy Agency, Vienna, Austria, 2018
1.4 This standard is used to measure and describe the
Advisory Material for the IAEA Regulations for the Safe
response of materials, products, or assemblies to heat and
Transport of Radioactive Material (2012 Edition), No.
flame under controlled conditions, but does not by itself
SSG-26, (IAEA SSG-26)International Atomic Energy
incorporate all factors required for fire hazard or fire risk
Agency, Vienna, Austria, 2014
assessment of the materials, products, or assemblies under
2.5 American Society of Mechanical Engineers Standard:
actual fire conditions.
Quality Assurance Program Requirements for Nuclear
1.5 Fire testing is inherently hazardous. Adequate safe-
Facilities, NQA-1, American Society of Mechanical
guards for personnel and property shall be employed in
Engineers, New York, 2001
conducting these tests.
1.6 This international standard was developed in accor- 2.6 International Organization for Standards (ISO) Stan-
dance with internationally recognized principles on standard- dard:
ISO 9000:2000, Quality Management Systems—
ization established in the Decision on Principles for the
Development of International Standards, Guides and Recom- Fundamentals and Vocabulary, International Organization
for Standards (ISO), Geneva, Switzerland, 2000
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee. ISO 13943Fire Safety – Vocabulary, International Organi-
zation for Standards (ISO), Geneva, Switzerland, 2017
This practice is under the jurisdiction of ASTM Committee C26 on Nuclear
Fuel Cycle and is the direct responsibility of Subcommittee C26.13 on Spent Fuel
and High Level Waste. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Jan. 1, 2022. Published April 2022. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 2002. Last previous edition approved in 2013 as E2230–13. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/E2230-22. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
E2230−22
3. Terminology 4.3 The regulatory thermal test is intended to simulate a
30-min exposure to a fully engulfing pool fire that occurs if a
3.1 Definitions—For definitions of terms used in this test
transportation accident involves the spill of large quantities of
method refer to the terminology contained in Terminology
hydrocarbon fuels from a tank truck or similar vehicle. The
E176 and ISO 13943 (Fire Safety – Vocabulary). In case of
regulations are “mode independent” meaning that they are
conflict between Terminology E176 and ISO 13943, the
intended to cover packages for a wide range of transportation
definitions given in Terminology E176 shall prevail.
modes such as truck and rail.
3.2 Definitions of Terms Specific to This Standard:
3.2.1 hypothetical accident conditions, n—a series of acci-
5. Significance and Use
dent environments, defined by regulation, that a Type B
5.1 The major objective of this practice is to provide a
package must survive without significant loss of contents.
common reference document for both applicants and certifica-
3.2.2 insolation, n—solar energy incident on the surface of
tion authorities on the accepted practices for accomplishing
a package.
package thermal qualification. Details and methods for accom-
3.2.3 normal conditions of transport, n—a range of
plishing qualification are described in this document in more
conditions, defined by regulation, that a package must with-
specific detail than available in the regulations. Methods that
stand during normal usage.
have been shown by experience to lead to successful qualifi-
cation are emphasized. Possible problems and pitfalls that lead
3.2.4 regulatory hydrocarbon fire, n—a fire environment,
to unsatisfactory results are also described.
one of the hypothetical accident conditions, defined by
regulation, that a package shall survive for 30 min without
5.2 The work described in this standard practice shall be
significant release of contents.
doneunderaqualityassuranceprogramthatisacceptedbythe
3.2.5 thermal qualification, n—the portion of the certifica- regulatory authority that certifies the package for use. For
tion process for a radioactive materials transportation package packages certified in the United States, 10 CFR 71 Subpart H
that includes the submittal, review, and approval of a Safety shall be used as the basis for the quality assurance (QA)
Analysis Report for Packages (SARP) through an appropriate
program,whileforinternationalcertification,ISO9000usually
regulatory authority, and which demonstrates that the package defines the appropriate program. The quality assurance pro-
meets the thermal requirements stated in the regulations.
gram shall be in place and functioning prior to the initiation of
any physical or analytical testing activities and prior to
3.2.6 Type B package, n—a transportation package that is
submittal of any information to the certifying authority.
licensed to carry what the regulations define to be a Type B
quantity of a specific radioactive material or materials.
TEST METHODS
4. Summary of Practice
6. General Information
4.1 This document outlines four methods for meeting the
6.1 In preparing a Safety Analysis Report for Packaging
thermal qualification requirements: qualification by analysis,
(SARP), the normal transport and accident thermal conditions
pool fire testing, furnace testing, and radiant heat testing. The
specified in 10CFR71 or IAEASSR-6 shall be addressed. For
choice of the certification method for a particular package is
based on discussions between the package suppliers and the approval in the United States, reports addressing the thermal
issues shall be included in a SARP prepared according to the
appropriate regulatory authorities prior to the start of the
qualification process. Factors that influence the choice of format described in Nuclear Regulatory Commission (NRC)
Regulatory Guide 7.9. Upon review, a package is considered
method are package size, construction and cost, as well as
hazards associated with certification process. Environmental qualified if material temperatures are within acceptable limits,
temperature gradients lead to acceptable thermal stresses, the
factorssuchasairandwaterpollutionareincreasinglyafactor
cavity gas pressure is within design limits, and safety features
in choice of qualification method. Specific benefits and limi-
continue to function over the entire temperature range. Test
tations for each method are discussed in the sections covering
initial conditions vary with regulation, but are intended to give
the particular methods.
the most unfavorable normal ambient temperature for the
4.2 The complete hypothetical accident condition sequence
feature under consideration, and corresponding internal pres-
consists of a drop test, a puncture test, and a 30-min hydro-
suresareusuallyatthemaximumnormalvaluesunlessalower
carbon fire test, commonly called a pool fire test, on the
pressure is shown to be more unfavorable. Depending on the
package. Submersion tests on undamaged packages are also
regulation used, the ambient air temperature is in the –29°C
required, and smaller packages are also required to survive
(–20°F) to 38°C (100°F) range. Normal transport require-
crushteststhatsimulatehandlingaccidents.Detailsofthetests
ments include a maximum air temperature of 38°C (100°F),
and test sequences are given in the regulations cited. This
insolation, and a cold temperature of –40°C (–40°F). Regu-
document focuses on thermal qualification, which is similar in
lations also include a maximum package surface temperatures
both the U.S. and IAEA regulations. A summary of important
for personnel protection of 50°C (122°F). See Appendix X3
differences is included as Appendix X3 to this document. The
for clarification of differences between U.S. and international
overall thermal test requirements are described generally in
regulations.
Part 71.73 of 10CFR71 and in Section VII of SSR-6. Addi-
tional guidance on thermal tests is also included in IAEA 6.2 Hypothetical accident thermal requirements stated in
SSG-26. Part 71.73 or IAEA SSR-6, Section VII call for a 30 min
E2230−22
exposure of the entire container to a radiation environment of 6.6 While 10CFR71 or SSR-6 values represent typical
800°C (1475°F) with a flame emissivity of 0.9. The surface package average heat fluxes in pool fires, large variations in
heat flux depending on both time and location have been
emissivity of the package shall be 0.8 or the package surface
observed in actual pool fires. Local heat fluxes as high as 150
value,whicheverisgreater.Withtemperaturesandemissivities
stated in the specification, the basic laws of radiation heat kW/m under low wind conditions are routinely observed for
low package surface temperatures. For high winds, heat fluxes
transfer permit direct calculation of the resulting radiant heat
as high as 400 kW/m are observed locally. Local flux values
flux to a package surface.This means that what appears at first
areafunctionofseveralparameters,includingheightabovethe
glance to be a flame or furnace temperature specification is in
pool. Thus the size, shape, and construction of the package
reality a heat flux specification for testing. Testing shall be
affects local heat flux conditions. Designers shall keep the
conducted with this point in mind.
possible differences between the hypothetical accident and
6.3 Two definitions of flame emissivity exist, and this
actual test conditions in mind during the design and testing
causes confusion during the qualification process. Siegel and
process. These differences explain some unpleasant surprises
Howell,2001,providethetextbookdefinitionforacloudofhot
such as localized high seal or cargo temperatures that have
soot particles representing a typical flame zone in open pool
occurred during the testing process.
fires. In this definition the black body emissive power of the
4 6.7 For proper testing, good simulations of both the regula-
flame, σT , is multiplied by the flame emissivity, ε, in order to
tory hydrocarbon fire heat flux transient and resulting material
accountforthefactthatsootcloudsinflamesbehaveasifthey
temperatures shall be achieved. Unless both the heat flux and
were weak black body emitters. A second definition of flame
material surface temperature transients are simultaneously
emissivity, often used for package analysis, assumes that the
reproduced, then the thermal stresses resulting from material
flame emissivity, ε, is the surface emissivity of a large,
temperature gradients and the final container temperature are
high-temperature, gray-body surface that both emits and re-
reported to be erroneously high or low. Some test methods are
flects energy and completely surrounds the package under
better suited to meeting these required transient conditions for
analysis. The second definition leads to slightly higher (con-
a particular package than others. The relative benefits and
servative) heat fluxes to the package surface, and also leads to
limitations of the various methods in simulating the pool fire
a zero heat flux as the package surface reaches the fire
environment are discussed in the following sections.
temperature. For the first definition, the heat flux falls to zero
whilethepackagesurfaceissomewhatbelowthefiretempera-
7. Procedure
ture. For package qualification, use of the second definition is
7.1 Qualification by Analysis
often more convenient, especially with computer codes that
model surface-to-surface thermal radiation, and is usually 7.1.1 Benefits, Limitations:
permitted by regulatory authorities.
7.1.1.1 The objective of thermal qualification of radioactive
material transportation packages by analysis is to ensure that
6.4 Convectiveheattransferfrommovingairat800°Cshall
containment of the contents, shielding of radiation from the
also be included in the analysis of the hypothetical accident
contents, and the sub-criticality of the contents is maintained
condition. Convection correlations shall be chosen to conform
per the regulations. The analysis determines the thermal
to the configuration (vertical or horizontal, flat or curved
behavior in response to the thermal conditions specified in the
surface) that is used for package transport. Typical flow
regulations for normal conditions of transport and for hypo-
velocities for combustion gases measured in large fires range
thetical accident conditions by calculating the maximum tem-
are in the 1 to 10 m/s range with mean velocities near the
peratures and temperature gradients for the various compo-
middle of that range (see Schneider and Kent, 1989, Gregory,
nentsofthepackagebeingqualified.RefertoAppendixX3for
et al, 1987, and Koski, et al, 1996). No external non-natural
specific requirements of the regulations.
coolingofthepackageafterheatinputispermittedafterthefire
7.1.1.2 Temperaturesthataretypicallydeterminedbyanaly-
event,, and combustion shall proceed until it stops naturally.
sis are package surface temperatures and the temperature
Duringthefire,effectsofsolarradiationareoftenneglectedfor
distribution throughout the package during normal conditions
analysis and test purposes.
of transport and during thermal accident conditions. In
6.5 For purposes of analysis, the hypothetical accident addition, maximum pressure inside the package is determined
thermalconditionsarespecifiedbythesurfaceheatfluxvalues. for both normal and accident conditions.
Peak regulatory heat fluxes for low surface temperatures
7.1.1.3 While an analysis cannot fully take place of an
typicallyrangefrom55to65kW/m .Convectiveheattransfer
actual test, performing the thermal analysis on a radioactive
from air is estimated from convective heat transfer
material transportation package allows the applicant to
correlations, and contributes of 15 to 20% of the total heat
estimate, with relatively high accuracy, the anticipated thermal
flux. The value of 15 to 20% value is consistent with
behavior of the package during both normal and accident
experimental estimates. Recent versions of the regulations
conditions without actually exposing a package to the extreme
specify moving, hot air for convection calculations, and an
conditions of the thermal qualification tests described in
appropriateforcedconvectioncorrelationshallbeusedinplace Section 6. Qualification by analysis is also a necessity in those
oftheolderpracticethatassumedstillairconvection.Afurther
cases where only a design is being qualified and an actual
discussion of heat flux values is provided in 7.2. specimen for a radioactive materials package does not exist.
E2230−22
7.1.1.4 Whiletoday’sthermalcodesprovideausefultoolto conduction and radiation. Natural convection in the gap is
perform the thermal qualification by analysis producing reli- usually neglected. Drum type packages usually have an inte-
gral thermal shield.
ableresults,thelimitationofanymethodliesintheexperience
of the user, the completeness of the model and accuracy of the
7.1.2.5 Thepackagecontentsandtheirheatgenerationshall
input data. Since in these analyses the heat transfer is the main
beconsideredinthemodelpreparation.Theimpactlimiterand
phenomenon being modeled and since it is mostly nonlinear,
the thermal shield insulation properties will result in slightly
thethermalcodeusedshallbeverifiedagainstavailabledataor
elevated temperatures during normal conditions of transport
benchmarked against other codes that have been verified. In
due to the resistance to heat flow from the package. Thus the
addition, limitations of analyses for determining the thermal
package interior has higher temperatures than the surrounding
behavior of a package include as-built package geometry, real
ambient temperature.
material properties including phase changes and destruction of
7.1.2.6 When creating the model and selecting the nodes, it
insulation, and real fire characteristics, including actual con-
is important to represent all materials of construction and
vection. Code software used shall be managed in a manner
components essential to containment in the model. Fig. 1
consistent with the appropriate QA methodology outlined in
shows a typical nodal network/finite difference model with
NQA-1 or ISO 9000 as appropriate.
node selection for temperature information on a package with
7.1.2 Model Preparation—This section describes the vari- animpactlimiter.Additionalnodeswillneedtobecreatedand
ousaspectsathermalmodelshallincludeandthemethodology utilized for an accurate Finite Element Analysis or Finite
of preparing a representative model. Difference Analysis model.
7.1.2.1 A common approach to analyzing a package is to 7.1.2.7 The mesh selected in the model for temperature
model the package as a drum or in a cylindrical configuration. profile analysis in the thermal portion of the hypothetical
This approach considers the package as an axisymmetric accident analysis shall be varied depending on the temperature
gradients. The finest mesh is located near the outer surface of
circular cylinder (outer shell) with a constant internal heat
source.Anothercommonapproachistomodelthepackagesas the package where the steepest temperature gradients occur.
The mesh size is increased as temperature gradients decrease,
a finite length right circular cylinder with an impact limiter
which usually occurs as the distance from the surface in-
(which also acts as a thermal insulator to the package). The
creases.Atestforpropermeshsizeistorefinethemeshfurther
outer shell will surround a cylindrical structure that contains
and demonstrate that no significant change in calculated
the content heat source.
temperatures results from the refinement.
7.1.2.2 Thermalprotectionofatypicalradioactivematerials
7.1.2.8 Thermo-physical Properties of Typical Materials:
package includes the impact limiters placed at the ends of the
(1)The thermal properties of the materials of construction
package and the thermal shield surrounding the cylindrical
need to be defined and documented as they are critical to
section of the package. The impact limiters consist of a
achieving meaningful results from the analysis. Properties of
low-density material, such as polyurethane foam, wood, or
the various components involved are often obtained from
other organic material enclosed in a steel shell, hollow steel
reference materials but all sources are to be verified for
structures or aluminum honeycomb design structure. The
reliability by determining that the properties were measured in
low-density configuration impact limiter usually has a low
accordance with accepted standards (that is,ASTM) and under
effective thermal conductivity.
an accepted quality assurance program (that is, NQA-1 or ISO
7.1.2.3 Thelowthermalconductivityimpactlimiterreduces
9000).
the heat transfer from the ends of the cask during normal
(2)Thematerialpropertiesusedneedtocoverthetempera-
conditions of transport, and into the ends of the cask during
ture range of the conditions being analyzed. If materials have
hypotheticalaccidentconditions.Analysisoftenshowsthatfor
propertiesthatchangewithtemperature,theyshallbemodeled
polyurethane foam impact limiters, the foam burns during a
withtheappropriatevariableproperties.Notethatuncertainties
hypotheticalaccidentandoff-gasescreatingpressurewithinthe
in the temperature dependence of material property data
impact limiter structure. This, along with the thermal expan-
increase with the variation of temperature from “room tem-
sion of the materials is to be considered in order to provide for
perature.”Additional testing is necessary for any material that
the worst case conduction/insulating properties. Credit for the
does not have well defined material properties.
insulating properties of the impact limiters shall be taken only
(3)Parts that are small or thin, or both, and do not have a
when structural analyses can demonstrate that the limiter
measurable affect on the overall heat transfer rates are often
remains in place under hypothetical accident conditions.
omitted from the model. Typical examples for this are thin
7.1.2.4 The thermal shield of radioactive waste and spent
partsthathavehighthermalconductivityandarenotseparated
fuelpackagestypicallyisastainlesssteelshellsurroundingthe
by air gaps from other components of the package being
cylindrical structural shell of the package. A gap is created
analyzed.Thinpartsseparatedbygaps,however,actasthermal
between the thermal shield and the structural shell of the
radiationshieldsthatgreatlyaffecttheoverallheattransferrate
package. Because of the low conductivity of air contained in
and shall be considered.
the gap, the heat resistance of the gap greatly reduces the heat
(4)When a material phase change or decomposition is
transfer rate during both normal conditions of transport and expected to occur, the analysis shall consider replacing the
hypothetical accident conditions. Heat transfer across the gap
material properties with conservative values. For example,
betweenthethermalshieldandstructuralshellismodeledwith polyurethane begins to decompose at 200°C (400°F), and the
E2230−22
FIG. 1Example of Node Selection When Modeling a Package
analyst often considers replacing the polyurethane properties (which is equivalent to the total insolation specified in
withthoseofairatthesametemperature.Notethatthethermal 10CFR71.71(c)(1) of 800 g-cal/cm for a 12-h period), 96.92
2 2
properties of polyurethane are similar to those of air and W/m (200 g-cal/cm for a 12-h period) for non-horizontal flat
2 2
actually the polyurethane properties are not critical since the surfaces, and 193.83 W/m (400 g-cal/cm for a 12-h period)
use of polyurethane results in a nearly adiabatic, that is, well for curved surfaces. Ambient temperature shall be 38°C
insulated, surface during hypothetical accident conditions. (100°F). Note that insolation depends on the shape and
(5)Radiation heat transfer occurs at the outer surfaces of a orientation of the package surface. A transient analysis of the
packageandalsointhegapbetweenthethermalshieldandthe normal conditions of transport can be performed instead of a
structural shell. Therefore, the consideration of the surface steady-stateanalysis.Thermalloadsforatransientanalysisare
emittance of these surfaces is critical to the model. Emittance different from those discussed in this paragraph.
values of the package exterior surface for the fire are specified (2)Inaddition,representativeinternalheatgenerationshall
in the regulations. be considered when preparing the model to determine the
(6)The analyst shall be familiar with the how the code temperature distribution of the package.
models radiation and, in specific, surface emissivity or absorp- (3)The model shall address external natural convection
tivity (also treated by some codes as reflectivity or albedo). In and radiation boundary conditions and temperature property
general,conservativesurfaceemittancevaluesaretobeusedin variations.
the analysis, that is, emittance value of 0.9 or unity (black (4)The temperature distribution of the package is assumed
body) for fire conditions, and an emittance of 0.8 shall be symmetric about the vertical axis and its horizontal mid-plane.
assumed for the outer surfaces in accordance with regulations. The heat transfer model needs to be defined, for example,
Package interior gap surfaces might be assumed as manufac- two-dimensional axisymmetric heat transfer (radial and axial).
tured for pre-fire conditions. Use of other than conservative The model shall address insolation on the package surfaces.
values shall be justified. Radiation heat exchange at the package interior surfaces shall
7.1.2.9 Model Preparation for Normal Conditions of Trans- be addressed.
port Thermal Evaluation: (5)Heattransferwithinthecontentsofthepackageisoften
(1)A steady-state analysis for normal conditions of trans- omitted in the special case where the heat generated in the
portthatfollows10CFR71.71shallassumeconstantinsolation contents is uniformly applied to the interior surfaces of the
of 387.67 W/m on horizontal flat surfaces exposed to the sun package. It is possible to use the package symmetry in the
E2230−22
modeltofacilitateevenheattransferconsiderations.Spentfuel pletelylost.Thisassumptionprovidesaconservativeapproach.
packages require special consideration as the bulk of the heat These two cases envelop the best and worst case scenarios
during the hypothetical accident thermal evaluation.
generated by the contents is transferred radially to the packag-
ing due to the large aspect ratio and the impact limiters on the (5)Underlying assumptions shall be documented and in-
clude:
ends of the package.
(6)The inside containment vessel temperature causes the
Enclosure radiation
External radiation
internal pressure to be elevated above atmospheric pressure.
Natural convection
Theinternalpressureatsteadystateareestimatedbyassuming
Insolation
the atmosphere contains dry air at an appropriate pressure and Internal heat dissipation
Internal convection
temperature when the package is closed. If the package
containswater,assumethatatsteady-statetransportconditions
7.1.3 Example of Package Model:
the air is saturated with water vapor. The internal pressure is
7.1.3.1 For demonstration purposes, consider that the ex-
equal to the sum of the dry air and the vapor pressure of water
ample package (see Safety Analysis Report for the 10-135
at the temperature of the environment within the containment
RadwasteShippingCask,1999)isasteelencasedleadshielded
vessel for normal conditions of transport. The stresses due to
cask intended for solid radioactive material (see Fig. 2).
pressurization of the package need to be addressed as part of
Overall dimensions are 2.85 m (112 in.) diameter by 3.3 m
the structural analysis.
(130 in.) height. It consists of two (2) concentric carbon steel
cylindrical shells surrounding a 89 mm (3.5 in.) thick lead
7.1.2.10 Model Preparation for Hypothetical Accident
shield. The 13 mm (0.5 in.) thick inner shell has a 1.67 m (66
Thermal Qualification:
in.) internal diameter and the 25 mm (1 in.) thick outer shell
(1)The effects of the hypothetical accident thermal condi-
has a 1.93 m (76 in.) outside diameter. The base is welded to
tions on the package need to be evaluated. The hypothetical
theshells.Thetopofthepackageisprovidedwithprimaryand
accident thermal conditions are defined in the regulations. The
secondarylidsofasteppeddowndesignconstructedoftwo75
various test conditions shall be applied sequentially, which
mm(3in.)thickplatesjoinedtogethertoforma150mm(6in.)
means that the thermal test follows the drop and the puncture
thick lid. The lids are secured with bolts. Lid interfaces are
tests.The reduction of the insulating capabilities of the impact
provided with high temperature silicone gaskets.
limiter caused by the free drop and puncture test shall be
7.1.3.2 The initial temperatures are determined from the
consideredintheanalysisofpackages.Incaseswheredropand
normal conditions of transport assuming a 38°C (100°F)
puncture damage to the impact limiters cannot be modeled in
ambient temperature with insolation. Fig. 3 shows typical
sufficient detail, two cases are analyzed to envelope the
steady-state temperatures under these conditions and an as-
performance of the impact limiters during a fire.
sumed 400W heat generation from the contents of a typical
(2)Theinitialtemperaturedistributioninthepackageprior
package. For packages with large thermal mass, or fully
to the fire shall be that determined for either the normal
enclosed by a thick insulating medium, such as polyurethane
conditionsoftransport(38°Cwithinsolation)[SSR-6,§728]or
foam, a 24-h average insolation value is often used to deter-
that determined for the case of defining the type of shipment
mine temperatures of interior components.
(exclusive or nonexclusive) from 10 CFR 71.43 (g) [10 CFR
71.73 (b)]. Usually, undamaged packages lead to higher 7.1.3.3 Two impact limiters are located at the top and
bottom of the package. The impact limiters are 10-gauge
pre-fire temperatures because package insulation is undam-
stainless steel shells filled with rigid polyurethane. The inner
aged. However in cases where damaged conditions lead to
surfaces of the body and the lid are clad with 12-gauge
higher pre-fire temperatures, those temperatures shall be used
stainless steel. The exposed portion of the cask body is
instead.
provided with a 10-gauge stainless steel thermal shield. A 6.4
(3)The thermal conditions imposed on the package during
mm (0.25 in.) gap between the cask body and the thermal
hypothetical accident conditions are that the package, with the
shield is maintained by spacers. A potential issue during
initial temperature distribution as determined above, is sub-
thermal qualification is the manufacturer’s ability to maintain
jectedtoafireof800°C(1475°F)foraperiodof30min.After
uniform gap width and potential effect of gap variation on the
the 30-min period, the source fire is assumed extinguished and
thermal results. The effect of gap widths in the as-
the ambient temperature reduced to 38°C (100°F). Any
manufacturedpackageshallbeconsideredanddiscussedbythe
ongoing combustion that continues after the fire shall be
analyst.
accounted for in the analysis. Flames of the ongoing combus-
7.1.3.4 Fig. 4 shows the predicted temperatures of a typical
tion are not allowed to be extinguished. In addition to the
package after 30 min following the initiation of the flame
natural convection to the ambient air and radiation to the
environment for the cask with the impact limiter attached.The
environment, the package shall be subject to insolation during
model was created using TAS of Harvard Thermal.
the post-fire cool-down.
(4)To determine the effect of the reduced insulating
7.1.3.5 After 30 min, the ambient temperature is reduced
capabilities of the impact limiter, two cases are analyzed. The from 800°C (1475°F) to 38°C (100°F) and, consequently,
first one assumes that the free drop and puncture tests had
the package begins to lose heat to the environment by natural
minor effects in thermal performance of the package during a convection to the still air and radiation to the environment.
hypothetical accident. The second case assumes that the However, the temperature in some regions of the package
insulating capabilities of the impact limiter have been com- continues to increase for some time due to heat conduction
E2230−22
FIG. 2Typical Package With Impact Limiters at Steady State (Using TAS)
NOTE 1—Temperatures are in °F. Note that in the original figure, colors were used to represent temperature variations.
FIG. 3Initial Temperatures for Transient Analysis for a Typical Package With Impact Limiters (Using TAS)
from surrounding regions of higher temperatures. These local partially, for the lack of pre-fire insolation. For packages to be
temperatures will continue to increase until the content tem-
qualified under both U. S. and international regulations, this
perature exceeds the temperature of the surrounding package
effect shall be addressed and quantified for the regulator.
components. The rate at which the package cools will be
7.1.4 Additional Information to be Reported:
reduced as insolation is applied during the cool-down time. If,
7.1.4.1 The results of the analysis shall be tabulated to
aspermittedintheU.S.(10CFR71.73(b)),pre-fireconditions
summarize the maximum temperatures resulting from the
are determined without the insolation specified in 10 CFR
hypothetical accident condition for each material of construc-
71.71, then initial package surface and contents temperatures
tion. In addition, graph(s) shall be included showing tempera-
will often be lower than the steady state temperatures reached
ture as a function of time for representative and critical/unique
with insolation after the fire. If package temperatures without
locations on the container during a hypothetical accident. The
insolationareloweratthestartofthefire,initialfireheatfluxes
to the package surface will be higher, compensating, at least
E2230−22
NOTE 1—Temperatures are in °F. Note that in the original figure, colors were used to represent temperature variations.
FIG. 4Temperatures After the 30-Min Fire on a Typical Package With Impact Limiters Attached (Using TAS)
interval selected shall be long enough to show all component data and retrieve results through a number of menu driven
temperatures descending with time. An example is shown choices. Some older codes require entry of data in the form of
below in Fig. 5. an input file, without the benefit of a GUI, and rely on a
7.1.4.2 Changes in the internal pressure shall be addressed. third-party graphics program to plot results of an analysis.
The internal pressure typically increases during the hypotheti- Some heat transfer codes require the use of a separate code to
cal accident due to heating of contents. Chemical decomposi- determine radiation form factors, which are then used by the
tion of the packaging materials and package contents shall be thermal code to treat enclosure radiation. The results of the
considered and appropriately addressed. thermal analysis are often used by the structural analyst to
7.1.4.3 Considerationofthermalstressesduetobothnormal perform thermal or pressure-induced stress analyses.
conditions of transport and hypothetical accident conditions 7.1.5.4 Thermal codes shall be qualified for package evalu-
shall also be included in the analysis. ation by verification, benchmarking, or validation. A code is
7.1.4.4 Post-firesteadystatetemperaturesshallbeanalyzed. verified by comparison of the results with the results of
Any resultant damage (for example, smoldering or melting of appropriate closed form solutions.
aneutronorgammashield,orboth)orchangeintheemissivity 7.1.5.5 Sample Problem Manual for Benchmarking of Cask
ofthesurfaceofthepackageshallbeevaluatedwithrespectto Analysis Codes (Glass, et al, 1988) describes a series of
the impact on the post-accident “normal” temperatures. problems, which have been defined to evaluate structural and
7.1.5 Analysis Conduct: thermalcodes.Theseproblemsweredevelopedtosimulatethe
7.1.5.1 General-purpose heat transfer codes exist for per- hypothetical accident conditions given in the regulations while
forming the thermal analysis of packages for the transport of retaining simple geometries. The intent of the manual is to
radioactive materials. These codes model heat transfer phe- provide code users with a set of structural and thermal
nomena (conduction, convection and radiation) for multidi- problems and solutions which are used to evaluate individual
mensionalgeometrieswithlinearandnon-linearsteady-stateor codes.
transientbehavior.Theymodelvariousmaterialswithtempera- 7.1.5.6 Acodeisbenchmarkedbycomparisonoftheresults
ture dependent isotropic and orthotropic thermal and other with the results of other qualified codes. An alternative code
physical properties, including phase change. validationmethodistocomparethecoderesultstoresultsfrom
7.1.5.2 These general-purpose codes treat constant or time- package design-based test data or hand calculations performed
dependent spatially-distributed heat-generation sources, enclo- under qualified QA programs.
sure radiation and boundary conditions including temperature 7.1.5.7 Any code selected to perform the thermal design
and heat flux. analysis of a radioactive material transportation package shall
7.1.5.3 Most commercial FEA codes have thermal solvers be subject to the QA program requirements for nuclear
and provide pre- and post-processors. The pre-processor is facilities as prescribed in ASME NQA-1 or software require-
used to create package geometry and generate a mesh for the ments of ISO 9000 as required by the certifying authority.
package, while the post-processor provides results in a graphi- 7.1.5.8 Several thermal analysis codes are available to
cal format. Pre- and post-processors are often in the form of a licensees of radioactive packages to perform the qualification
graphical user interface (GUI) which allows the user to enter analyses.Thisdocumentisnotintendedtodescribethevarious
E2230−22
FIG. 5Example for Temperature as a Function of Time for Selected Locations on a Sample Container
During a Hypothetical Thermal Accident
thermal codes in detail, but a few are mentioned and briefly surfaceisheavierthanair,andsubjecttodisplacementbyvery
described in Appendix X4 for the reader’s benefit. Codes not low velocity air currents. The effect of wind is minimized by
mentioned in Appendix X4 are often equally adequate to enclosing the pool within a ring of 6 m high wind fencing.
perform thermal qualification of packages to regulatory re-
7.2.1.3 The intention of a pool fire test is to subject the
quirements. No comparison or evaluation of codes is provided
prototype package to an environment that is representative of
in this document.
conditionsfoundinatransportationaccidentfire.Notethattwo
differentenvironmentsareunderconsiderationhere.Thereisa
7.2 Pool Fire Testing
hypothetical accident condition or regulatory hydrocarbon fire
7.2.1 Benefits, Limitations:
environment, described in the regulations, and an actual pool
7.2.1.1 Pool fire testing has been the traditional testing
fire environment, which is created at 1 m above a pool of
methodbywhichapackageisqualifiedtothethermalaccident
burning liquid hydrocarbon fuel in calm wind conditions.
environment set forth in the regulations. In the test, the
Packages that are designed to withstand the regulatory hydro-
prototype package is placed 1 m over a pool of fuel whose
carbonfireareconsideredtofunctionsafelyinatransportation
lateral dimensions relative to the package meet the require-
accident. The actual pool fire environment is a convenient
ments stated in the regulation. When atmospheric conditions
means for testing packages and is usually very different from
arequiescent,thefuelisignitedandthepackageisengulfedin
the hypothetical accident conditions as discussed below.
thefireplume.After30min,thefuelisconsumed,thefiregoes
7.2.1.4 The hypothetical accident condition environment
out, and the prototype package is left to cool down naturally.
specified in the regulations is usually reduced to a schedule of
7.2.1.2 Aconvenient method for forming a pool consists of
heatfluxabsorbedthroughthepackagesurfaceasafunctionof
floating a layer of jet fuel (JP-8) on water in a deep steel tub
the package surface temperature.Aheat balance at any instant
(see Fig. 6). The water provides a flat surface for the fuel,
in time on the surface of a package subjected to the regulatory
which ensures the fire burns out evenly over the whole pool
hydrocarbon fire gives:
area when the fuel is completely consumed. A deep tub (~0.7
4 4
m)providesenoughwatertomaintainaconstantfuelsubstrate
q 50.9·0.8·σ·T 20.8·σ·T (1)
absorbed environment surface
temperature which helps to maintain a constant fuel consump-
where:
tion rate during the fire. The packages are held at the required
q = heat flux passing through the surface of the
height above the pool surface with a stainless steel grill.
absorbed
package, kW/m ,
Structures are placed throughout the pool to support fire
-11
σ = Stefan-Boltzmann constant, 5.67 × 10 kW/
instrumentation that might include thermocouples,
2 4
(m K ),
calorimeters, heat flux gages, and gas velocity probes. The
T = temperature specified in 10CFR71, 800 + 273
environment
response of this instrumentation is used to provide evidence
= 1073 K,
that the required thermal environment has been met. Sheet
T = surface temperature of the package at any
surface
metal side ramps on the outside of the tub, and sheet metal
instant, K,
skirts on the grill provide fire plume stability. These are
0.9 = specified emissivity of flames, and
necessary because the fuel vapor immediately above the fuel
E2230−22
NOTE 1—Some features are to meet geometrical requirements, some stabilize the plume, and others provide evidence of supplying the required
environment.
FIG. 6A Pool Fire Test and Setup That Meets the Regulatory Requirements
support structures. In terms of flexibility and cost, there are
0.8 = absorptivity of package surface (minimum
obvious benefits over those associated with an oven or radiant
value).
heat facility.
7.2.1.5 This description of the hypothetical accident condi-
7.2.1.8 A second benefit is that the pool fire environment
tion environment is shown in Fig. 7. Note that in the equation
oftensurpassestherequirements,providingaconservativetest.
above, the “text book” definition of flame emissivity (see 6.3)
Fig.7showsthatthefluxfromapoolfiretoanengulfedobject
has been used to generate the plot. The regulatory heat fluxes
often exceeds the criteria by a factor approaching four.
are compared to a description of the actual pool fire environ-
Furthermore, the fact that the environment is a real fire shall
ment that has been determined from the response of thick wall
not be overlooked. The so-called second order characteristics,
passive calorimeters from which data have been gathered over
such as fire plume chemistry or non-uniform spatial and
the last 20 years in pool fires of sizes ranging from 1 to 20 m
temporalheatfluxes,affectpackageperformanceinunforeseen
in diameter.The wide range is due to minor variations in wind
ways; and subjecting a prototype package to a pool fire brings
conditions and calorimeter surface orientation with respect to
out deficiencies due to features that weren’t considered in the
the pool geometry.
design. Examples of this that have occurred in the past with
7.2.1.6 Note that in general, the pool fire provides an
packages in pool fires include unexpected seal response due to
environment that is more intense than that o
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E2230 − 13 E2230 − 22
Standard Practice for
Thermal Qualification of Type B Packages for Radioactive
Material
This standard is issued under the fixed designation E2230; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This practice defines detailed methods for thermal qualification of “Type B” radioactive materials packages under Title 10,
Code of Federal Regulations, Part 71 (10CFR71) in the United States or, under International Atomic Energy Agency Regulation
TS-R-1.SSR-6. Under these regulations, packages transporting what are designated to be Type B quantities of radioactive material
shall be demonstrated to be capable of withstanding a sequence of hypothetical accidents without significant release of contents.
1.2 The unit system (SI metric or English) used for thermal qualification shall be agreed upon prior to submission of information
to the certification authority. If SI units are to be standard, then use IEEE/ASTM SI-10. Additional units given in parentheses are
for information purposes only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.4 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under
controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials,
products, or assemblies under actual fire conditions.
1.5 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these
tests.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2.1 ASTM Standards:
E176 Terminology of Fire Standards
IEEE/ASTM SI-10 International System of Units (SI) The Modernized Metric System
2.2 Federal Standard:
Title 10, Code of Federal Regulations, Part 71 (10CFR71), Packaging and Transportation of Radioactive Material, United States
Government Printing Office, October 1, 2004
This practice is under the jurisdiction of ASTM Committee C26 on Nuclear Fuel Cycle and is the direct responsibility of Subcommittee C26.13 on Spent Fuel and High
Level Waste.
Current edition approved April 1, 2013Jan. 1, 2022. Published April 2013April 2022. Originally approved in 2002. Last previous edition approved in 20082013 as
E2230E2230 – 13.–08. DOI: 10.1520/E2230-13.10.1520/E2230-22.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
E2230 − 22
2.3 Nuclear Regulatory Commission Standards:
Standard Format and Content of Part 71 Applications for Approval of Packaging of Type B Large Quantity and Fissile
Radioactive Material, Regulatory Guide 7.9, United States Nuclear Regulatory Commission, United States Government
Printing Office, 1986
Standard Review Plan for Transportation of Radioactive Materials, NUREG-1609, United States Nuclear Regulatory
Commission, United States Government Printing Office, May 1999
2.4 International Atomic Energy Agency Standards:
Regulations for the Safe Transport of Radioactive Material, No. TS-R-1,SSR-6 (IAEA ST-1SSR-6 Revised) International Atomic
Energy Agency, Vienna, Austria, 19962018
Advisory Material for the IAEA Regulations for the Safe Transport of Radioactive Material, No. ST-2, (IAEA ST-2)Material
(2012 Edition), No. SSG-26, (IAEA SSG-26) International Atomic Energy Agency, Vienna, Austria, 19962014
2.5 American Society of Mechanical Engineers Standard:
Quality Assurance Program Requirements for Nuclear Facilities, NQA-1, American Society of Mechanical Engineers, New
York, 2001
2.6 International Organization for Standards (ISO) Standard:
ISO 9000:2000, Quality Management Systems—Fundamentals and Vocabulary, International Organization for Standards (ISO),
Geneva, Switzerland, 2000
ISO 13943 Fire Safety – Vocabulary, International Organization for Standards (ISO), Geneva, Switzerland, 2017
3. Terminology
3.1 Definitions—For definitions of terms used in this test method refer to the terminology contained in Terminology E176 and ISO
13943. 13943 (Fire Safety – Vocabulary). In case of conflict, conflict between Terminology E176 and ISO 13943, the definitions
given in Terminology E176 shall prevail.
3.2 Definitions of Terms Specific to This Standard:
3.2.1 hypothetical accident conditions, n—a series of accident environments, defined by regulation, that a Type B package must
survive without significant loss of contents.
3.2.2 insolation, n—solar energy incident on the surface of a package.
3.2.3 normal conditions of transport, n—a range of conditions, defined by regulation, that a package must withstand during normal
usage.
3.2.4 regulatory hydrocarbon fire, n—a fire environment, one of the hypothetical accident conditions, defined by regulation, that
a package shall survive for 30 min without significant release of contents.
3.2.5 thermal qualification, n—the portion of the certification process for a radioactive materials transportation package that
includes the submittal, review, and approval of a Safety Analysis Report for Packages (SARP) through an appropriate regulatory
authority, and which demonstrates that the package meets the thermal requirements stated in the regulations.
3.2.6 Type B package, n—a transportation package that is licensed to carry what the regulations define to be a Type B quantity
of a specific radioactive material or materials.
4. Summary of Practice
4.1 This document outlines four methods for meeting the thermal qualification requirements: qualification by analysis, pool fire
testing, furnace testing, and radiant heat testing. The choice of the certification method for a particular package is based on
discussions between the package suppliers and the appropriate regulatory authorities prior to the start of the qualification process.
Factors that influence the choice of method are package size, construction and cost, as well as hazards associated with certification
process. Environmental factors such as air and water pollution are increasingly a factor in choice of qualification method. Specific
benefits and limitations for each method are discussed in the sections covering the particular methods.
4.2 The complete hypothetical accident condition sequence consists of a drop test, a puncture test, and a 30-min hydrocarbon fire
test, commonly called a pool fire test, on the package. Submersion tests on undamaged packages are also required, and smaller
packages are also required to survive crush tests that simulate handling accidents. Details of the tests and test sequences are given
E2230 − 22
in the regulations cited. This document focuses on thermal qualification, which is similar in both the U.S. and IAEA regulations.
A summary of important differences is included as Appendix X3 to this document. The overall thermal test requirements are
described generally in Part 71.73 of 10CFR71 and in Section VII of TS-R-1.SSR-6. Additional guidance on thermal tests is also
included in IAEA ST-2.SSG-26.
4.3 The regulatory thermal test is intended to simulate a 30-min exposure to a fully engulfing pool fire that occurs if a
transportation accident involves the spill of large quantities of hydrocarbon fuels from a tank truck or similar vehicle. The
regulations are “mode independent” meaning that they are intended to cover packages for a wide range of transportation modes
such as truck and rail.
5. Significance and Use
5.1 The major objective of this practice is to provide a common reference document for both applicants and certification
authorities on the accepted practices for accomplishing package thermal qualification. Details and methods for accomplishing
qualification are described in this document in more specific detail than available in the regulations. Methods that have been shown
by experience to lead to successful qualification are emphasized. Possible problems and pitfalls that lead to unsatisfactory results
are also described.
5.2 The work described in this standard practice shall be done under a quality assurance program that is accepted by the regulatory
authority that certifies the package for use. For packages certified in the United States, 10 CFR 71 Subpart H shall be used as the
basis for the quality assurance (QA) program, while for international certification, ISO 9000 usually defines the appropriate
program. The quality assurance program shall be in place and functioning prior to the initiation of any physical or analytical testing
activities and prior to submittal of any information to the certifying authority.
5.3 The unit system (SI metric or English) used for thermal qualification shall be agreed upon prior to submission of information
to the certification authority. If SI units are to be standard, then use IEEE/ASTM SI-10. Additional units given in parentheses are
for information purposes only.
TEST METHODS
6. General Information
6.1 In preparing a Safety Analysis Report for Packaging (SARP), the normal transport and accident thermal conditions specified
in 10CFR71 or IAEA TS-R-1SSR-6 shall be addressed. For approval in the United States, reports addressing the thermal issues
shall be included in a SARP prepared according to the format described in Nuclear Regulatory Commission (NRC) Regulatory
Guide 7.9. Upon review, a package is considered qualified if material temperatures are within acceptable limits, temperature
gradients lead to acceptable thermal stresses, the cavity gas pressure is within design limits, and safety features continue to function
over the entire temperature range. Test initial conditions vary with regulation, but are intended to give the most unfavorable normal
ambient temperature for the feature under consideration, and corresponding internal pressures are usually at the maximum normal
values unless a lower pressure is shown to be more unfavorable. Depending on the regulation used, the ambient air temperature
is in the -29°C (-20°F) to 38°C (100°F)–29 °C (–20 °F) to 38 °C (100 °F) range. Normal transport requirements include a
maximum air temperature of 38°C (100°F), insolation, and a cold temperature of -40°C (-40°F).–40 °C (–40 °F). Regulations also
include a maximum package surface temperatures for personnel protection of 50°C (122°F).50 °C (122 °F). See Appendix X3 for
clarification of differences between U.S. and international regulations.
6.2 Hypothetical accident thermal requirements stated in Part 71.73 or IAEA TS-R-1,SSR-6, Section VII call for a 30 min
exposure of the entire container to a radiation environment of 800°C (1475°F)800 °C (1475 °F) with a flame emissivity of 0.9. The
surface emissivity of the package shall be 0.8 or the package surface value, whichever is greater. With temperatures and
emissivities stated in the specification, the basic laws of radiation heat transfer permit direct calculation of the resulting radiant heat
flux to a package surface. This means that what appears at first glance to be a flame or furnace temperature specification is in reality
a heat flux specification for testing. Testing shall be conducted with this point in mind.
6.3 Two definitions of flame emissivity exist, and this causes confusion during the qualification process. Siegel and Howell, 2001,
provide the textbook definition for a cloud of hot soot particles representing a typical flame zone in open pool fires. In this
definition the black body emissive power of the flame, σT , is multiplied by the flame emissivity, ε, in order to account for the fact
that soot clouds in flames behave as if they were weak black body emitters. A second definition of flame emissivity, often used
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for package analysis, assumes that the flame emissivity, ε, is the surface emissivity of a large, high-temperature, gray-body surface
that both emits and reflects energy and completely surrounds the package under analysis. The second definition leads to slightly
higher (conservative) heat fluxes to the package surface, and also leads to a zero heat flux as the package surface reaches the fire
temperature. For the first definition, the heat flux falls to zero while the package surface is somewhat below the fire temperature.
For package qualification, use of the second definition is often more convenient, especially with computer codes that model
surface-to-surface thermal radiation, and is usually permitted by regulatory authorities.
6.4 Convective heat transfer from moving air at 800°C shall also be included in the analysis of the hypothetical accident condition.
Convection correlations shall be chosen to conform to the configuration (vertical or horizontal, flat or curved surface) that is used
for package transport. Typical flow velocities for combustion gases measured in large fires range are in the 1 to 10 m/s range with
mean velocities near the middle of that range (see Schneider and Kent, 1989, Gregory, et al, 1987, and Koski, et al, 1996). No
external non-natural cooling of the package after heat input is permitted after the fire event,, and combustion shall proceed until
it stops naturally. During the fire, effects of solar radiation are often neglected for analysis and test purposes.
6.5 For purposes of analysis, the hypothetical accident thermal conditions are specified by the surface heat flux values. Peak
regulatory heat fluxes for low surface temperatures typically range from 55 to 65 kW/m . Convective heat transfer from air is
estimated from convective heat transfer correlations, and contributes of 15 to 20 % of the total heat flux. The value of 15 to 20 %
value is consistent with experimental estimates. Recent versions of the regulations specify moving, hot air for convection
calculations, and an appropriate forced convection correlation shall be used in place of the older practice that assumed still air
convection. A further discussion of heat flux values is provided in 7.2.
6.6 While 10CFR71 or TS-R-1SSR-6 values represent typical package average heat fluxes in pool fires, large variations in heat
flux depending on both time and location have been observed in actual pool fires. Local heat fluxes as high as 150 kW/m under
low wind conditions are routinely observed for low package surface temperatures. For high winds, heat fluxes as high as 400
kW/m are observed locally. Local flux values are a function of several parameters, including height above the pool. Thus the size,
shape, and construction of the package affects local heat flux conditions. Designers shall keep the possible differences between the
hypothetical accident and actual test conditions in mind during the design and testing process. These differences explain some
unpleasant surprises such as localized high seal or cargo temperatures that have occurred during the testing process.
6.7 For proper testing, good simulations of both the regulatory hydrocarbon fire heat flux transient and resulting material
temperatures shall be achieved. Unless both the heat flux and material surface temperature transients are simultaneously
reproduced, then the thermal stresses resulting from material temperature gradients and the final container temperature are reported
to be erroneously high or low. Some test methods are better suited to meeting these required transient conditions for a particular
package than others. The relative benefits and limitations of the various methods in simulating the pool fire environment are
discussed in the following sections.
7. Procedure
7.1 Qualification by Analysis
7.1.1 Benefits, Limitations:
7.1.1.1 The objective of thermal qualification of radioactive material transportation packages by analysis is to ensure that
containment of the contents, shielding of radiation from the contents, and the sub-criticality of the contents is maintained per the
regulations. The analysis determines the thermal behavior in response to the thermal conditions specified in the regulations for
normal conditions of transport and for hypothetical accident conditions by calculating the maximum temperatures and temperature
gradients for the various components of the package being qualified. Refer to Appendix X3 for specific requirements of the
regulations.
7.1.1.2 Temperatures that are typically determined by analysis are package surface temperatures and the temperature distribution
throughout the package during normal conditions of transport and during thermal accident conditions. In addition, maximum
pressure inside the package is determined for both normal and accident conditions.
7.1.1.3 While an analysis cannot fully take place of an actual test, performing the thermal analysis on a radioactive material
transportation package allows the applicant to estimate, with relatively high accuracy, the anticipated thermal behavior of the
package during both normal and accident conditions without actually exposing a package to the extreme conditions of the thermal
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qualification tests described in Section 6. Qualification by analysis is also a necessity in those cases where only a design is being
qualified and an actual specimen for a radioactive materials package does not exist.
7.1.1.4 While today’s thermal codes provide a useful tool to perform the thermal qualification by analysis producing reliable
results, the limitation of any method lies in the experience of the user, the completeness of the model and accuracy of the input
data. Since in these analyses the heat transfer is the main phenomenon being modeled and since it is mostly nonlinear, the thermal
code used shall be verified against available data or benchmarked against other codes that have been verified. In addition,
limitations of analyses for determining the thermal behavior of a package include as-built package geometry, real material
properties including phase changes and destruction of insulation, and real fire characteristics, including actual convection. Code
software used shall be managed in a manner consistent with the appropriate QA methodology outlined in NQA-1 or ISO 9000 as
appropriate.
7.1.2 Model Preparation—This section describes the various aspects a thermal model shall include and the methodology of
preparing a representative model.
7.1.2.1 A common approach to analyzing a package is to model the package as a drum or in a cylindrical configuration. This
approach considers the package as an axisymmetric circular cylinder (outer shell) with a constant internal heat source. Another
common approach is to model the packages as a finite length right circular cylinder with an impact limiter (which also acts as a
thermal insulator to the package). The outer shell will surround a lead shieldcylindrical structure that contains the content heat
source.
7.1.2.2 Thermal protection of a typical radioactive materials package includes the impact limiters placed at the ends of the package
and the thermal shield surrounding the cylindrical section of the package. The impact limiters consist of a low-density material,
such as polyurethane foam, wood, or other organic material enclosed in a steel shell, hollow steel structures or aluminum
honeycomb design structure. The low-density configuration impact limiter usually has a low effective thermal conductivity.
7.1.2.3 The low thermal conductivity impact limiter reduces the heat transfer from the ends of the cask during normal conditions
of transport, and into the ends of the cask during hypothetical accident conditions. Analysis often shows that for polyurethane foam
impact limiters, the foam burns during a hypothetical accident and off-gases creating pressure within the impact limiter structure.
This, along with the thermal expansion of the materials is to be considered in order to provide for the worst case
conduction/insulating properties. Credit for the insulating properties of the impact limiters shall be taken only when structural
analyses can demonstrate that the limiter remains in place under hypothetical accident conditions.
7.1.2.4 The thermal shield of radioactive waste and spent fuel packages typically is a stainless steel shell surrounding the
cylindrical structural shell of the package. A gap is created between the thermal shield and the structural shell of the package.
Because of the low conductivity of air contained in the gap, the heat resistance of the gap greatly reduces the heat transfer rate
during both normal conditions of transport and hypothetical accident conditions. Heat transfer across the gap between the thermal
shield and structural shell is modeled with conduction and radiation. Natural convection in the gap is usually neglected. Drum type
packages usually have an integral thermal shield.
7.1.2.5 The package contents and their heat generation shall be considered in the model preparation. The impact limiter and the
thermal shield insulation properties will result in slightly elevated temperatures during normal conditions of transport due to the
resistance to heat flow from the package. Thus the package interior has higher temperatures than the surrounding ambient
temperature.
7.1.2.6 When creating the model and selecting the nodes, it is important to represent all materials of construction and components
essential to containment in the model. Fig. 1 shows a typical nodal network/finite difference model with node selection for
temperature information on a package with an impact limiter. Additional nodes will need to be created and utilized for an accurate
Finite Element Analysis or Finite Difference Analysis model.
7.1.2.7 The mesh selected in the model for temperature profile analysis in the thermal portion of the hypothetical accident analysis
shall be varied depending on the temperature gradients. The finest mesh is located near the outer surface of the package where the
steepest temperature gradients occur. The mesh size is increased as temperature gradients decrease, which usually occurs as the
distance from the surface increases. A test for proper mesh size is to refine the mesh further and demonstrate that no significant
change in calculated temperatures results from the refinement.
7.1.2.8 Thermo-physical Properties of Typical Materials:
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FIG. 1 Example of Node Selection When Modeling a Package
(1) The thermal properties of the materials of construction need to be defined and documented as they are critical to achieving
meaningful results from the analysis. Properties of the various components involved are often obtained from reference materials
but all sources are to be verified for reliability by determining that the properties were measured in accordance with accepted
standards (that is, ASTM) and under an accepted quality assurance program (that is, NQA-1 or ISO 9000).
(2) The material properties used need to cover the temperature range of the conditions being analyzed. If materials have
properties that change with temperature, they shall be modeled with the appropriate variable properties. Note that uncertainties in
the temperature dependence of material property data increase with the variation of temperature from “room temperature.”
Additional testing is necessary for any material that does not have well defined material properties.
(3) Parts that are small or thin, or both, and do not have a measurable affect on the overall heat transfer rates are often omitted
from the model. Typical examples for this are thin parts that have high thermal conductivity and are not separated by air gaps from
other components of the package being analyzed. Thin parts separated by gaps, however, act as thermal radiation shields that
greatly affect the overall heat transfer rate and shall be considered.
(4) When a material phase change or decomposition is expected to occur, the analysis shall consider replacing the material
properties with conservative values. For example, polyurethane begins to decompose at 200°C (400°F),200 °C (400 °F), and the
analyst often considers replacing the polyurethane properties with those of air at the same temperature. Note that the thermal
properties of polyurethane are similar to those of air and actually the polyurethane properties are not critical since the use of
polyurethane results in a nearly adiabatic, that is, well insulated, surface during hypothetical accident conditions.
(5) Radiation heat transfer occurs at the outer surfaces of a package and also in the gap between the thermal shield and the
structural shell. Therefore, the consideration of the surface emittance of these surfaces is critical to the model. Emittance values
of the package exterior surface for the fire are specified in the regulations.
(6) The analyst shall be familiar with the how the code models radiation and, in specific, surface emissivity or absorptivity (also
treated by some codes as reflectivity or albedo). In general, conservative surface emittance values are to be used in the analysis,
that is, emittance value of 0.9 or unity (black body) for fire conditions, and an emittance of 0.8 shall be assumed for the outer
surfaces in accordance with regulations. Package interior gap surfaces might be assumed machined as manufactured for pre-fire
conditions. Use of other than conservative values shall be justified.
7.1.2.9 Model Preparation for Normal Conditions of Transport Thermal Evaluation:
(1) A steady-state analysis for normal conditions of transport that follows 10CFR71.71 shall assume constant insolation of
387.67 W/m on horizontal flat surfaces exposed to the sun (which is equivalent to the total insolation specified in
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2 2 2
10CFR71.71(c)(1) of 800 g-cal/cm for a 12-h period), 96.92 W/m (200 g-cal/cm for a 12-h period) for non-horizontal flat
2 2
surfaces, and 193.83 W/m (400 g-cal/cm for a 12-h period) for curved surfaces. Ambient temperature shall be 38°C
(100°F).38 °C (100 °F). Note that insolation depends on the shape and orientation of the package surface. A transient analysis of
the normal conditions of transport can be performed instead of a steady-state analysis. Thermal loads for a transient analysis are
different from those discussed in this paragraph.
(2) In addition, representative internal heat generation shall be considered when preparing the model to determine the
temperature distribution of the package.
(3) The model shall address external natural convection and radiation boundary conditions and temperature property variations.
(4) The temperature distribution of the package is assumed symmetric about the vertical axis and its horizontal mid-plane. The
heat transfer model needs to be defined, for example, two-dimensional axisymmetric heat transfer (radial and axial). The model
shall address insolation on the package surfaces. Radiation heat exchange at the package interior surfaces shall be addressed.
(5) Heat transfer within the contents of the package is often omitted in the special case where the heat generated in the contents
is uniformly applied to the interior surfaces of the package. It is possible to use the package symmetry in the model to facilitate
even heat transfer considerations. Spent fuel packages require special consideration as the bulk of the heat generated by the
contents is transferred radially to the packaging due to the large aspect ratio and the impact limiters on the ends of the package.
(6) The inside containment vessel temperature causes the internal pressure to be elevated above atmospheric pressure. The
internal pressure at steady state are estimated by assuming the atmosphere contains dry air at an appropriate pressure and
temperature when the package is closed. If the package contains water, assume that at steady-state transport conditions the air is
saturated with water vapor. The internal pressure is equal to the sum of the dry air and the vapor pressure of water at the
temperature of the environment within the containment vessel for normal conditions of transport. The stresses due to pressurization
of the package need to be addressed as part of the structural analysis.
7.1.2.10 Model Preparation for Hypothetical Accident Thermal Qualification:
(1) The effects of the hypothetical accident thermal conditions on the package need to be evaluated. The hypothetical accident
thermal conditions are defined in the regulations. The various test conditions shall be applied sequentially, which means that the
thermal test follows the drop and the puncture tests. The reduction of the insulating capabilities of the impact limiter caused by
the free drop and puncture test shall be considered in the analysis of packages. In cases where drop and puncture damage to the
impact limiters cannot be modeled in sufficient detail, two cases are analyzed to envelope the performance of the impact limiters
during a fire.
(2) The initial temperature distribution in the package prior to the fire shall be that determined for either the normal conditions
of transport (38°C with insolation) [TS-R-1,[SSR-6, §728] or that determined for the case of defining the type of shipment
(exclusive or nonexclusive) from 10 CFR 71.43 (g) [10 CFR 71.73 (b)]. Usually, undamaged packages lead to higher pre-fire
temperatures because package insulation is undamaged. However in cases where damaged conditions lead to higher pre-fire
temperatures, those temperatures shall be used instead.
(3) The thermal conditions imposed on the package during hypothetical accident conditions are that the package, with the
initial temperature distribution as determined above, is subjected to a fire of 800°C (1475°F)800 °C (1475 °F) for a period of 30
min. After the 30-min period, the source fire is assumed extinguished and the ambient temperature reduced to 38°C (100°F).38 °C
(100 °F). Any ongoing combustion that continues after the fire shall be accounted for in the analysis. Flames of the ongoing
combustion are not allowed to be extinguished. In addition to the natural convection to the ambient air and radiation to the
environment, the package shall be subject to insolation during the post-fire cool-down.
(4) To determine the effect of the reduced insulating capabilities of the impact limiter, two cases are analyzed. The first one
assumes that the free drop and puncture tests had minor effects in thermal performance of the package during a hypothetical
accident. The second case assumes that the insulating capabilities of the impact limiter have been completely lost. This assumption
provides a conservative approach. These two cases envelop the best and worst case scenarios during the hypothetical accident
thermal evaluation.
(5) Underlying assumptions shall be documented and include:
Enclosure radiation
External radiation
Natural convection
Insolation
Internal heat dissipation
Internal convection
7.1.3 Example of Package Model:
7.1.3.1 For demonstration purposes, consider that the typicalexample package (see Safety Analysis Report for the 10-135
Radwaste Shipping Cask, 1999) is a steel encased lead shielded cask intended for solid radioactive material (see Fig. 2). Overall
dimensions are 2.85 m (112 in.) diameter by 3.3 m (130 in.) height. It consists of two (2) concentric carbon steel cylindrical shells
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FIG. 2 Typical Package With Impact Limiters at Steady State (Using TAS)
surrounding a 89 mm (3.5 in.) thick lead shield. The 13 mm (0.5 in.) thick inner shell has a 1.67 m (66 in.) internal diameter and
the 25 mm (1 in.) thick outer shell has a 1.93 m (76 in.) outside diameter. The base is welded to the shells. The top of the package
is provided with primary and secondary lids of a stepped down design constructed of two 75 mm (3 in.) thick plates joined together
to form a 150 mm (6 in.) thick lid. The lids are secured with bolts. Lid interfaces are provided with high temperature silicone
gaskets.
7.1.3.2 The initial temperatures are determined from the normal conditions of transport assuming a 38°C (100°F)38 °C (100 °F)
ambient temperature with insolation. Fig. 3 shows typical steady-state temperatures under these conditions and an assumed 400W
heat generation from the contents of a typical package. For packages with large thermal mass, or fully enclosed by a thick
insulating medium, such as polyurethane foam, a 24-h average insolation value is often used to determine temperatures of interior
components.
7.1.3.3 Two impact limiters are located at the top and bottom of the package. The impact limiters are 10-gage10-gauge stainless
steel shells filled with rigid polyurethane. The inner surfaces of the body and the lid are clad with 12-gage12-gauge stainless steel.
The exposed portion of the cask body is provided with a 10-gage10-gauge stainless steel thermal shield. A 6.4 mm (0.25 in.) gap
between the cask body and the thermal shield is maintained by spacers. A potential issue during thermal qualification is the
manufacturer’s ability to maintain uniform gap width and potential effect of gap variation on the thermal results. The effect of gap
widths in the as-manufactured package shall be considered and discussed by the analyst.
7.1.3.4 Fig. 4 shows the predicted temperatures of a typical package after 30 min following the initiation of the flame environment
for the cask with the impact limiter attached. The model was created using TAS of Harvard Thermal.
7.1.3.5 After 30 min, the ambient temperature is reduced from 800°C (1475°F) to 38°C (100°F)800 °C (1475 °F) to 38 °C (100 °F)
and, consequently, the package begins to lose heat to the environment by natural convection to the still air and radiation to the
environment. However, the temperature in some regions of the package continues to increase for some time due to heat conduction
from surrounding regions of higher temperatures. These local temperatures will continue to increase until the content temperature
exceeds the temperature of the surrounding package components. The rate at which the package cools will be reduced as insolation
is applied during the cool-down time. If, as permitted in the U. S. (10 CFR 71.73(b)), pre-fire conditions are determined without
the insolation specified in 10 CFR 71.71, then initial package surface and contents temperatures will often be lower than the steady
state temperatures reached with insolation after the fire. If package temperatures without insolation are lower at the start of the fire,
initial fire heat fluxes to the package surface will be higher, compensating, at least partially, for the lack of pre-fire insolation. For
packages to be qualified under both U. S. and international regulations, this effect shall be addressed and quantified for the
regulator.
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NOTE 1—Temperatures are in °F. Note that in the original figure, colors were used to represent temperature variations.
FIG. 3 Initial Temperatures for Transient Analysis for a Typical Package With Impact Limiters (Using TAS)
NOTE 1—Temperatures are in °F. Note that in the original figure, colors were used to represent temperature variations.
FIG. 4 Temperatures After the 30-Min.30-Min Fire on a Typical Package With Impact Limiters Attached (Using TAS)
7.1.4 Additional Information to be Reported:
7.1.4.1 The results of the analysis shall be tabulated to summarize the maximum temperatures resulting from the hypothetical
accident condition for each material of construction. In addition, graph(s) shall be included showing temperature as a function of
time for representative and critical/unique locations on the container during a hypothetical accident. The interval selected shall be
long enough to show all component temperatures descending with time. An example is shown below in Fig. 5.
7.1.4.2 Changes in the internal pressure shall be addressed. The internal pressure typically increases during the hypothetical
accident due to heating of contents. Chemical decomposition of the packaging materials and package contents shall be considered
and appropriately addressed.
7.1.4.3 Consideration of thermal stresses due to both normal conditions of transport and hypothetical accident conditions shall also
be included in the analysis.
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FIG. 5 Example for Temperature as a Function of Time for Selected Locations on a Sample Container
During a Hypothetical Thermal Accident
7.1.4.4 Post-fire steady state temperatures shall be analyzed. Any resultant damage (for example, smoldering or melting of a
neutron or gamma shield, or both) or change in the emissivity of the surface of the package shall be evaluated with respect to the
impact on the post-accident “normal” temperatures.
7.1.5 Analysis Conduct:
7.1.5.1 General-purpose heat transfer codes exist for performing the thermal analysis of packages for the transport of radioactive
materials. These codes model heat transfer phenomena (conduction, convection and radiation) for multidimensional geometries
with linear and non-linear steady-state or transient behavior. They model various materials with temperature dependent isotropic
and orthotropic thermal and other physical properties, including phase change.
7.1.5.2 These general-purpose codes treat constant or time-dependent spatially-distributed heat-generation sources, enclosure
radiation and boundary conditions including temperature and heat flux.
7.1.5.3 Most commercial FEA codes have thermal solvers and provide pre- and post-processors. The pre-processor is used to
create package geometry and generate a mesh for the package, while the post-processor provides results in a graphical format. Pre-
and post-processors are often in the form of a graphical user interface (GUI) which allows the user to enter data and retrieve results
through a number of menu driven choices. Some older codes require entry of data in the form of an input file, without the benefit
of a GUI, and rely on a third-party graphics program to plot results of an analysis. Some heat transfer codes require the use of a
separate code to determine radiation form factors, which are then used by the thermal code to treat enclosure radiation. The results
of the thermal analysis are often used by the structural analyst to perform thermal or pressure-induced stress analyses.
7.1.5.4 Thermal codes shall be qualified for package evaluation by verification, benchmarking, or validation. A code is verified
by comparison of the results with the results of appropriate closed form solutions.
7.1.5.5 Sample Problem Manual for Benchmarking of Cask Analysis Codes (Glass, et al, 1988) describes a series of problems,
which have been defined to evaluate structural and thermal codes. These problems were developed to simulate the hypothetical
accident conditions given in the regulations while retaining simple geometries. The intent of the manual is to provide code users
with a set of structural and thermal problems and solutions which are used to evaluate individual codes.
7.1.5.6 A code is benchmarked by comparison of the results with the results of other qualified codes. An alternative code validation
method is to compare the code results to results from package design-based test data or hand calculations performed under qualified
QA programs.
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NOTE 1—Some features are to meet geometrical requirements, some stabilize the plume, and others provide evidence of supplying the required
environment.
FIG. 6 A Pool Fire Test and Setup That Meets the Regulatory Requirements
7.1.5.7 Any code selected to perform the thermal design analysis of a radioactive material transportation package shall be subject
to the QA program requirements for nuclear facilities as prescribed in ASME NQA-1 or software requirements of ISO 9000 as
required by the certifying authority.
7.1.5.8 Several thermal analysis codes are available to licensees of radioactive packages to perform the qualification analyses. This
document is not intended to describe the various thermal codes in detail, but a few are mentioned and briefly described in Appendix
X4 for the reader’s benefit. Codes not mentioned in Appendix X4 are often equally adequate to perform thermal qualification of
packages to regulatory requirements. No comparison or evaluation of codes is provided in this document.
7.2 Pool Fire Testing
7.2.1 Benefits, Limitations:
7.2.1.1 Pool fire testing has been the traditional testing method by which a package is qualified to the thermal accident
environment set forth in the regulations. In the test, the prototype package is placed 1 m over a pool of fuel whose lateral
dimensions relative to the package meet the requirements stated in the regulation. When atmospheric conditions are quiescent, the
fuel is ignited and the package is engulfed in the fire plume. After 30 min, the fuel is consumed, the fire goes out, and the prototype
package is left to cool down naturally.
7.2.1.2 A convenient method for forming a pool consists of floating a layer of jet fuel (JP-8) on water in a deep steel tub (see Fig.
6). The water provides a flat surface for the fuel, which ensures the fire burns out evenly over the whole pool area when the fuel
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FIG. 7 Comparison of the Hypothetical Accident Fire Environment and the Actual Pool Fire Environment
is completely consumed. A deep tub (~0.7 m) provides enough water to maintain a constant fuel substrate temperature which helps
to maintain a constant fuel consumption rate during the fire. The packages are held at the required height above the pool surface
with a stainless steel grill. Structures are placed throughout the pool to support fire instrumentation that might include
thermocouples, calorimeters, heat flux gages, and gas velocity probes. The response of this instrumentation is used to provide
evidence that the required thermal environment has been met. Sheet metal side ramps on the outside of the tub, and sheet metal
skirts on the grill provide fire plume stability. These are necessary because the fuel vapor immediately above the fuel surface is
heavier than air, and subject to displacement by very low velocity air currents. The effect of wind is minimized by enclosing the
pool within a ring of 6 m high wind fencing.
7.2.1.3 The intention of a pool fire test is to subject the prototype package to an environment that is representative of conditions
found in a transportation accident fire. Note that two different environments are under consideration here. There is a hypothetical
accident condition or regulatory hydrocarbon fire environment, described in the regulations, and an actual pool fire environment,
which is created at 1 m above a pool of burning liquid hydrocarbon fuel in calm wind conditions. Packages that are designed to
withstand the regulatory hydrocarbon fire are considered to function safely in a transportation accident. The actual pool fire
environment is a convenient means for testing packages and is usually very different from the hypothetical accident conditions as
discussed below.
7.2.1.4 The hypothetical accident condition environment specified in the regulations is usually reduced to a schedule of heat flux
absorbed through the package surface as a function of the package surface temperature. A heat balance at any instant in time on
the surface of a package subjected to the regulatory hydrocarbon fire gives:
4 4
q 5 0.9·0.8·σ·T 2 0.8·σ·T (1)
absorbed environment surface
where:
q = heat flux pass
...








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