M/588 - Industrial emissions

This document specifies a method for the enumeration of Escherichia coli (E. coli) in soil improvers and growing media. This document is applicable to material in solid form (including pre-shaped growing media) and liquid form.
This document is applicable to fertilizing product blends, where a blend is a mix of two or more fertilizing products belonging to the categories of fertilizers, liming material, soil improvers, growing media, inhibitors and plant biostimulants, and where soil improvers and/or growing media comprise the highest percentage in the blend by mass or volume, or in the case of liquid form by dry mass. If soil improvers and/or growing media do not comprise the highest percentage in the blend, the European Standard for the highest percentage in the blend applies. In case a blend is composed of fertilising products in equal quantity, the user of the standard decides which standard to apply.
NOTE 1   A soil improver or a growing medium consists of a single bulky (volume-building) component or a mix of bulky (volume-building) components (for example peat, wood fibres, coconut coir, compost, expanded perlite).
Strains of E. coli which do not grow at 44 °C ± 1 °C and, in particular, those that are β-D-glucuronidase-negative, such as E. coli O157, will not be detected. Some strains of Shigella spp. and Salmonella spp. within the family Enterobacteriaceae can also show β-D-glucuronidase activity at 44 °C ± 1 °C.
NOTE 2   This method has been validated in an interlaboratory study with specific products that were present on the market during the study (Annex C).

This document specifies a method for the enumeration of enterococci in soil improvers and growing media. This document is applicable to material in solid form (including pre-shaped growing media) and liquid form.
This document is applicable to fertilizing product blends, where a blend is a mix of two or more fertilising products belonging to the categories of fertilizers, liming material, soil improvers, growing media, inhibitors and plant biostimulants, and where soil improvers and/or growing media comprise the highest percentage in the blend by mass or volume, or in the case of liquid form by dry mass. If soil improvers and/or growing media do not comprise the highest percentage in the blend, the European Standard for the highest percentage in the blend applies. In case a blend is composed of fertilising products in equal quantity, the user of the standard decides which standard to apply.
NOTE 1   A soil improver or a growing medium consists of a single bulky (volume-building) component or a mix of bulky (volume-building) components (for example peat, wood fibres, coconut coir, compost, expanded perlite).
NOTE 2   This method has been validated in an interlaboratory study with specific products that were present on the market during the study (Annex C).

This document specifies a method for the enumeration of enterococci in soil improvers and growing media. This document is applicable to material in solid form (including pre-shaped growing media) and liquid form.
This document is applicable to fertilizing product blends, where a blend is a mix of two or more fertilising products belonging to the categories of fertilizers, liming material, soil improvers, growing media, inhibitors and plant biostimulants, and where soil improvers and/or growing media comprise the highest percentage in the blend by mass or volume, or in the case of liquid form by dry mass. If soil improvers and/or growing media do not comprise the highest percentage in the blend, the European Standard for the highest percentage in the blend applies. In case a blend is composed of fertilising products in equal quantity, the user of the standard decides which standard to apply.
NOTE 1   A soil improver or a growing medium consists of a single bulky (volume-building) component or a mix of bulky (volume-building) components (for example peat, wood fibres, coconut coir, compost, expanded perlite).
NOTE 2   This method has been validated in an interlaboratory study with specific products that were present on the market during the study (Annex C).

This document specifies a method for the enumeration of Escherichia coli (E. coli) in soil improvers and growing media. This document is applicable to material in solid form (including pre-shaped growing media) and liquid form.
This document is applicable to fertilizing product blends, where a blend is a mix of two or more fertilizing products belonging to the categories of fertilizers, liming material, soil improvers, growing media, inhibitors and plant biostimulants, and where soil improvers and/or growing media comprise the highest percentage in the blend by mass or volume, or in the case of liquid form by dry mass. If soil improvers and/or growing media do not comprise the highest percentage in the blend, the European Standard for the highest percentage in the blend applies. In case a blend is composed of fertilising products in equal quantity, the user of the standard decides which standard to apply.
NOTE 1   A soil improver or a growing medium consists of a single bulky (volume-building) component or a mix of bulky (volume-building) components (for example peat, wood fibres, coconut coir, compost, expanded perlite).
Strains of E. coli which do not grow at 44 °C ± 1 °C and, in particular, those that are β-D-glucuronidase-negative, such as E. coli O157, will not be detected. Some strains of Shigella spp. and Salmonella spp. within the family Enterobacteriaceae can also show β-D-glucuronidase activity at 44 °C ± 1 °C.
NOTE 2   This method has been validated in an interlaboratory study with specific products that were present on the market during the study (Annex C).

This document specifies a method for extraction, separation, and determination of inorganic arsenic (iAs) in growing media and soil improvers using anion-exchange high performance liquid chromatography (HPLC) or ion chromatography (IC) coupled to ICP-MS.
This document is applicable to the fertilizing product blends where a blend is a mix of two or more fertilising products belonging to the categories of fertilizers, liming material, soil improvers, growing media, inhibitors and plant biostimulants, and where soil improvers and/or growing media are the components with the highest percentage in the blend by mass or volume, or in the case of products in liquid form by dry mass. If the soil improvers and/or growing media are not the components with the highest percentage in the blend, the document relevant to the component with the highest percentage in the blend applies. In case a blend is composed of fertilising products mixed in equal quantities, the user of the document decides which standard to apply.
NOTE A soil improver consists of a single bulky (volume-building) component or a mix of bulky (volume-building) components (for example peat, wood fibres, coconut coir, compost, expanded perlite).

This document specifies a method for the determination of the organic nitrogen content in organic soil improvers.

This document specifies different methods for quantitative determination of 16 polycyclic aromatic hydrocarbons (PAH) (see Table 1) in compost or digestate, using GC-MS, GCMS/MS or HPLC UV DAD/FLD covering a wide range of PAH contamination levels (see Table 1).
When using fluorescence detection, acenaphthylene cannot be measured.
Table 1 — Target analytes of this document
[...table not reproduced...]
The limit of detection depends on the determinants, the equipment used, the quality of chemicals used for the extraction of the sample and the clean-up of the extract.
This document contains decision tables based on the properties of the sample and the extraction and clean-up procedure to be used.
The method may be applied to the analysis of other PAH not specified in the scope, provided suitability is proven by proper in-house validation experiments.

This document specifies a method for the determination of the residual biogas potential in digestate in an anaerobic environment.

This document specifies a method for the determination of total organic carbon (TOC) in soil improvers and growing media containing more than 1 g carbon per kg of dry matter (0,1 %).
NOTE Samples with a low dry matter content can have an influence on the achievable limit of quantification as defined in the scope (i.e. 1 g carbon per kg of dry matter).

This document specifies a method for the determination of the organic nitrogen content in organic soil improvers.

Soil improvers and growing media - Determination of mercury in aqua regia soil extracts with cold-vapour atomic spectrometry or cold-vapour atomic fluorescence spectrometry

This document specifies a method for extraction, separation, and determination of inorganic arsenic (iAs) in growing media and soil improvers using anion-exchange high performance liquid chromatography (HPLC) or ion chromatography (IC) coupled to ICP-MS.
This document is applicable to the fertilizing product blends where a blend is a mix of two or more fertilising products belonging to the categories of fertilizers, liming material, soil improvers, growing media, inhibitors and plant biostimulants, and where soil improvers and/or growing media are the components with the highest percentage in the blend by mass or volume, or in the case of products in liquid form by dry mass. If the soil improvers and/or growing media are not the components with the highest percentage in the blend, the document relevant to the component with the highest percentage in the blend applies. In case a blend is composed of fertilising products mixed in equal quantities, the user of the document decides which standard to apply.
NOTE A soil improver consists of a single bulky (volume-building) component or a mix of bulky (volume-building) components (for example peat, wood fibres, coconut coir, compost, expanded perlite).

This document specifies a method for the determination of the residual biogas potential in digestate in an anaerobic environment.

This document specifies different methods for quantitative determination of 16 polycyclic aromatic hydrocarbons (PAH) (see Table 1) in compost or digestate, using GC-MS, GCMS/MS or HPLC UV DAD/FLD covering a wide range of PAH contamination levels (see Table 1).
When using fluorescence detection, acenaphthylene cannot be measured.
Table 1 — Target analytes of this document
[...table not reproduced...]
The limit of detection depends on the determinants, the equipment used, the quality of chemicals used for the extraction of the sample and the clean-up of the extract.
This document contains decision tables based on the properties of the sample and the extraction and clean-up procedure to be used.
The method may be applied to the analysis of other PAH not specified in the scope, provided suitability is proven by proper in-house validation experiments.

This document specifies a method for the determination of total organic carbon (TOC) in soil improvers and growing media containing more than 1 g carbon per kg of dry matter (0,1 %).
NOTE Samples with a low dry matter content can have an influence on the achievable limit of quantification as defined in the scope (i.e. 1 g carbon per kg of dry matter).

Soil improvers and growing media - Determination of mercury in aqua regia soil extracts with cold-vapour atomic spectrometry or cold-vapour atomic fluorescence spectrometry