ASTM D1489-09(2021)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D1489 − 09 (Reapproved 2021)
Standard Test Method for
Nonvolatile Content of Aqueous Adhesives
This standard is issued under the fixed designation D1489; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
This test method replaces Method 4021 of Federal Test Method Standard No. 175a.
1. Scope 4.2 This test method can be used to compare the nonvolatile
content of various adhesives for adhesive selection and product
1.1 This test method covers the determination of the non-
uniformity.
volatile content of aqueous adhesives, such as dextrin, starch,
casein, and animal gelatin.
4.3 This test method is suitable for quality control and
research purposes.
1.2 The values stated in SI units are to be regarded as the
standard. The values given in parentheses are for information
5. Apparatus and Materials
only.
1.3 This standard does not purport to address all of the 5.1 Analytical Balance, for weighing of specimen, accurate
to 60.001 g.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
5.2 Laboratory Balance, for weighing of sample, accurate
priate safety, health, and environmental practices and deter-
to 60.01 g.
mine the applicability of regulatory limitations prior to use.
5.3 Constant-Temperature Oven, capable of maintaining a
1.4 This international standard was developed in accor-
temperature of 105 6 1°C (221 6 2°F).
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the
5.4 Glass Jar, of sufficient size, 1 Lor more, to store sample
Development of International Standards, Guides and Recom-
of adhesive prior to testing. The jar shall be such that it can be
mendations issued by the World Trade Organization Technical
sealed to prevent the loss of volatile content during the storage
Barriers to Trade (TBT) Committee.
period.
5.5 Beaker, of 100 mL capacity.
2. Referenced Documents
5.6 Weighing Bottles—Wide-mouth cylindrical glass weigh-
2.1 ASTM Standards:
ing bottles, of flat form, about 30 mm in height and 50 mm in
D907 Terminology of Adhesives
diameter, having interchangeable ground-in glass caps.
3. Terminology
5.7 Volumetric Flasks, of 200-mL capacity, with glass stop-
pers.
3.1 Definitions—Many terms in this test method are defined
in Terminology D907.
5.8 Volumetric Pipet, of 10-mL capacity.
5.9 Desiccator, with drying agent and tray.
4. Significance and Use
5.10 Silica Sand.
4.1 Adhesive cost is often related to the solids level (non-
volatile content).
5.11 Water, Hot—Distilled water heated to at least 80°C.
5.12 Hot Plate, used to heat the water.
This test method is under the jurisdiction of ASTM Committee D14 on
6. Sampling
Adhesives and is the direct responsibility of Subcommittee D14.10 on Working
Properties.
6.1 Thesampleoftheadhesiveshallberepresentativeofthe
Current edition approved April 1, 2021. Published April 2021. Originally
lot being evaluated. The quantity shall be at least 1.0 L aliquot
approved in 1957. Last previous edition approved in 2016 as D1489 – 09 (2016).
DOI: 10.1520/D1489-09R21.
consisting of a composite taken, when possible, from three or
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
more separate containers chosen at random. Thoroughly mix
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
the sample to uniform consistency. Immediately place the
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. composite sample in an airtight glass jar until tested.
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