ISO 616:2021
(Main)Coke - Determination of shatter indices
Coke - Determination of shatter indices
This document specifies a method for determining the strength of coke by the shatter test.
Coke — Détermination des indices de chute
General Information
- Status
- Published
- Publication Date
- 14-Oct-2021
- Technical Committee
- ISO/TC 27/SC 3 - Coke
- Drafting Committee
- ISO/TC 27/SC 3 - Coke
- Current Stage
- 6060 - International Standard published
- Start Date
- 15-Oct-2021
- Due Date
- 31-May-2022
- Completion Date
- 15-Oct-2021
Relations
- Effective Date
- 23-Apr-2020
Overview
ISO 616:2021 - "Coke - Determination of shatter indices" specifies a standardized laboratory method to determine the mechanical strength of coke using the shatter test. The shatter index is reported as the percentage of a prepared coke sample that remains on a specified test sieve after a defined dropping procedure. The standard describes sampling, apparatus, test procedure, result calculation and reporting for consistent, repeatable coke strength measurements.
Key topics and technical requirements
- Definition: The shatter index is the percentage of a test portion retained on a sieve of nominal opening x mm after the prescribed dropping test.
- Sampling & preconditioning: Follow ISO 18283 or ISO 13909-6 for sampling. Moisture is checked per ISO 579; if moisture > 5% the sample must be dried before testing.
- Size analysis: Perform sieve analysis in accordance with ISO 728 to prepare size fractions and assemble a representative test portion.
- Test portion: Reconstitute a 25 kg ± 0.1 kg test portion containing all fractions >63 mm in original proportions.
- Apparatus: Shatter test apparatus with base unit (minimum 1 220 × 970 mm base), sample box (internal 710 × 460 × 380 mm) and raising/lowering mechanism. Standard drop positions: bottom of box 1 830 mm above base when raised, and 460 mm when lowered.
- Procedure: Transfer test portion into the sample box, raise to the standard height, release doors to allow free fall onto base plate - repeat for a total of four drops. Recover coke, sieve using ISO 3310-2 compliant test sieves (common sizes listed) and weigh fractions to nearest 10 g (or 0.01 kg during preparation).
- Result calculation: Shatter index Sx = (cumulative mass retained on sieves ≥ x mm) / (total mass after test) × 100. Report to 0.1 percentage unit.
- Validity & precision: Test is valid if total mass after sieving differs from original test portion by ≤ 100 g. Example repeatability limits: duplicate S40 results should not differ by more than 4.0 units; S12.5 by more than 1.0 unit. Reproducibility between laboratories is not quoted due to sample transport breakage risk.
Applications
- Quality control for coke production and blending
- Feedstock assessment for blast furnaces and foundries
- Supplier/contract compliance and material acceptance testing
- Research on coke mechanical properties and coke-making process optimization
Who uses this standard
- Coke producers and quality laboratories
- Steelmakers and foundries specifying coke feed quality
- Independent testing laboratories and material inspectors
- R&D engineers studying coke durability
Related standards
- ISO 579 (moisture)
- ISO 728 (sieve size analysis)
- ISO 3310-2 (test sieves)
- ISO 13909-6 and ISO 18283 (sampling and sample preparation)
Keywords: ISO 616:2021, coke shatter index, shatter test, coke strength, test sieves, coke testing, ISO coke standards.
Frequently Asked Questions
ISO 616:2021 is a standard published by the International Organization for Standardization (ISO). Its full title is "Coke - Determination of shatter indices". This standard covers: This document specifies a method for determining the strength of coke by the shatter test.
This document specifies a method for determining the strength of coke by the shatter test.
ISO 616:2021 is classified under the following ICS (International Classification for Standards) categories: 75.160.10 - Solid fuels. The ICS classification helps identify the subject area and facilitates finding related standards.
ISO 616:2021 has the following relationships with other standards: It is inter standard links to ISO 616:1995. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
You can purchase ISO 616:2021 directly from iTeh Standards. The document is available in PDF format and is delivered instantly after payment. Add the standard to your cart and complete the secure checkout process. iTeh Standards is an authorized distributor of ISO standards.
Standards Content (Sample)
INTERNATIONAL ISO
STANDARD 616
Third edition
2021-10
Coke — Determination of shatter
indices
Coke — Détermination des indices de chute
Reference number
© ISO 2021
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
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or ISO’s member body in the country of the requester.
ISO copyright office
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Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Apparatus . 1
6 Sampling and size analysis .3
7 Preparation of test portion . 3
8 Procedure .4
8.1 Determination . 4
8.2 Validity of determination . 4
9 Expression of results . 4
10 Precision . 5
10.1 General . 5
10.2 Repeatability limit . 5
10.3 Reproducibility . . 5
11 Test report . 5
iii
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
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ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www.iso.org/patents).
Any trade name used in this document is information given for the convenience of users and does not
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For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO's adherence to
the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see
www.iso.org/iso/foreword.html.
This document was prepared by Technical Committee ISO/TC 27, Coal and coke, Subcommittee SC 3,
Coke.
This third edition cancels and replaces the second edition (ISO 616:1995), which has been technically
revised.
The main changes are as follows:
— general and technical revision;
— inclusion of references to ISO 13909-6 and ISO 18283 in Clause 6;
— provision of an example of an apparatus and a modernized mechanism that can raise the sample box
to the standard height is permitted.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www.iso.org/members.html.
iv
Introduction
The shatter index of coke is the percentage of test sample (initially plus 63 mm) that remains on a test
sieve of stated size of openings after the sample has been subjected to a specified dropping test.
The shatter index of coke can be determined for one test sieve or for each of a number of test sieves of
different sizes of holes (e.g. 80 mm and 40 mm). The higher the shatter index, the greater the resistance
of the coke to breakage into pieces which are smaller than the stated size.
The mean size of the coke before and after the shatter test may also be determined to give additional
information about the strength of the coke.
v
INTERNATIONAL STANDARD ISO 616:2021(E)
Coke — Determination of shatter indices
1 Scope
This document specifies a method for determining the strength of coke by the shatter test.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 579, Coke — Determination of total moisture
ISO 728, Coke — Size analysis by sieving
ISO 3310-2, Test sieves — Technical requirements and testing — Part 2: Test sieves of perforated metal
plate
ISO 13909-6, Hard coal and coke — Mechanical sampling — Part 6: Coke — Preparation of test samples
ISO 18283, Hard coal and coke — Manual sampling
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.
ISO and IEC maintain terminology databases for use in standardization at the following addresses:
— ISO Online browsing platform: available at https:// www .iso .org/ obp
— IEC Electropedia: available at https:// www .electropedia .org/
3.1
shatter index
percentage of a specially prepared sample of coke remaining on a test sieve of stated size of openings
after the sample has been subjected to
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