Solid biofuels - Sample preparation (ISO 14780:2017)

ISO 14780:2017 defines methods for reducing combined samples (or increments) to laboratory samples and laboratory samples to sub-samples and general analysis samples and is applicable to solid biofuels.
The methods defined in this document can be used for sample preparation, for example, when the samples are to be tested for calorific value, moisture content, ash content, bulk density, durability, particle size distribution, ash melting behaviour, chemical composition, and impurities.

Biogene Festbrennstoffe - Probenherstellung (ISO 14780:2017)

Dieses Dokument legt Verfahren zur Reduktion von Gesamtproben (oder Einzelproben) auf Laboratoriums-proben und von Laboratoriumsproben auf Teilproben und allgemeine Analysenproben fest und gilt für biogene Festbrennstoffe.
Die in diesem Dokument festgelegten Verfahren können bei der Probenvorbereitung angewendet werden, zum Beispiel, wenn Proben im Hinblick auf Energiegehalt, Wasser- und Aschegehalt, Schüttdichte, mechanische Festigkeit, Partikelgrößenverteilung, Ascheschmelzverhalten, chemische Zusammensetzung und Verunreinigungen zu prüfen sind.

Biocombustibles solides - Préparation des échantillons (ISO 14780:2017)

ISO 14780:2017 définit les méthodes permettant de réduire les échantillons composites (ou les prélèvements élémentaires) en échantillons pour laboratoire et les échantillons pour laboratoire en sous-échantillons et en échantillons pour analyse générale. Elle s'applique aux biocombustibles solides.
Les méthodes définies dans le présent document peuvent être utilisées pour la préparation d'échantillons devant, par exemple, être soumis à des essais portant sur le pouvoir calorifique, le taux d'humidité, la teneur en cendres, la masse volumique apparente, la durabilité, la distribution granulométrique, le comportement des cendres en fusion, la composition chimique et les impuretés.

Trdna biogoriva - Priprava vzorcev (ISO 14780:2017)

Predlagani mednarodni standard opisuje metode za zmanjšanje kombiniranih vzorcev (ali vzorcev) na laboratorijske vzorce in laboratorijskih vzorcev na podvzorce ter splošne analizne vzorce, uporablja pa se tudi za trdna biogoriva. Metode, ki so opisane v tem predlaganem dokumentu, se lahko uporabijo za pripravo vzorcev, ko je potrebno preskusiti na primer kalorično vrednost, vsebnost vlage, vsebnost pepela, prostorninsko maso, odpornost, porazdelitev velikosti delcev, lastnosti pepela pri taljenju, kemično sestavo in nečistoče. Te metode niso namenjene za uporabo pri zelo velikih vzorcih, ki so potrebni za preskušanje premostitvenih lastnosti.

General Information

Status
Published
Publication Date
16-May-2017
Withdrawal Date
29-Nov-2017
Technical Committee
Drafting Committee
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
17-May-2017
Completion Date
17-May-2017

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SLOVENSKI STANDARD
01-julij-2017
1DGRPHãþD
SIST EN 14780:2011
Trdna biogoriva - Priprava vzorcev (ISO 14780:2017)
Solid biofuels - Sample preparation (ISO 14780:2017)
Biogene Festbrennstoffe - Probenherstellung (ISO 14780:2017)
Biocombustibles solides - Préparation des échantillons (ISO 14780:2017)
Ta slovenski standard je istoveten z: EN ISO 14780:2017
ICS:
75.160.40 Biogoriva Biofuels
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 14780
EUROPEAN STANDARD
NORME EUROPÉENNE
May 2017
EUROPÄISCHE NORM
ICS 75.160.40; 27.190 Supersedes EN 14780:2011
English Version
Solid biofuels - Sample preparation (ISO 14780:2017)
Biocombustibles solides - Préparation des échantillons Biogene Festbrennstoffe - Probenherstellung (ISO
(ISO 14780:2017) 14780:2017)
This European Standard was approved by CEN on 15 March 2017.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2017 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 14780:2017 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
This document (EN ISO 14780:2017) has been prepared by Technical Committee ISO/TC 238 "Solid
biofuels" in collaboration with Technical Committee CEN/TC 335 “Solid biofuels” the secretariat of
which is held by SIS.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by November 2017, and conflicting national standards
shall be withdrawn at the latest by November 2017.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent
rights.
This document supersedes EN 14780:2011.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 14780:2017 has been approved by CEN as EN ISO 14780:2017 without any modification.

INTERNATIONAL ISO
STANDARD 14780
First edition
2017-04
Solid biofuels — Sample preparation
Biocombustibles solides — Préparation des échantillons
Reference number
ISO 14780:2017(E)
©
ISO 2017
ISO 14780:2017(E)
© ISO 2017, Published in Switzerland
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Ch. de Blandonnet 8 • CP 401
CH-1214 Vernier, Geneva, Switzerland
Tel. +41 22 749 01 11
Fax +41 22 749 09 47
copyright@iso.org
www.iso.org
ii © ISO 2017 – All rights reserved

ISO 14780:2017(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Symbols . 2
5 Principles of correct sample reduction . 2
6 Apparatus . 2
6.1 Apparatus for sample division. 2
6.1.1 General. 2
6.1.2 Riffle boxes . 2
6.1.3 Rotary sample dividers . 3
6.1.4 Shovels and scoops . 4
6.2 Apparatus for particle size-reduction . 5
6.2.1 Coarse cutting mill or wood crusher . 5
6.2.2 Cutting mill . 5
6.2.3 Axe . 6
6.2.4 Hand saw . 6
6.2.5 Sieves . 6
6.2.6 Balance . 6
7 Sample reduction — General principles . 6
8 Methods for sample division . 8
8.1 General . 8
8.2 Riffling . 9
8.3 Strip mixing. 9
8.4 Long pile-alternate shovel method . 9
8.5 Rotary divider .10
8.6 Coning and quartering .10
8.7 Mass reducing straw-like material (handful sampling).10
9 Method for reducing laboratory samples to sub-samples and general analysis samples.11
9.1 Mixing .11
9.2 Initial sample division .11
9.3 Pre-drying .11
9.4 Coarse cutting (particle size reduction to <31,5 mm) .12
9.5 Sample division of <31,5 mm material .12
9.6 Particle size reduction of <31,5 mm material to <1 mm .12
9.7 Sample division of <1 mm material .13
9.8 Particle size reduction of <1 mm material to <0,25 mm .13
10 Storage and labelling.13
11 Performance characteristics .13
Annex A (informative) Precision in relation to division method .14
Annex B (informative) Scheme of sample preparation for samples from single delivery .19
Annex C (informative) Scheme of sample preparation for samples from continuous delivery .20
Bibliography .22
ISO 14780:2017(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see ww
...


SLOVENSKI STANDARD
01-julij-2017
Nadomešča:
SIST EN 14780:2011
Trdna biogoriva - Priprava vzorcev (ISO 14780:2017)
Solid biofuels - Sample preparation (ISO 14780:2017)
Biogene Festbrennstoffe - Probenherstellung (ISO 14780:2017)
Biocombustibles solides - Préparation des échantillons (ISO 14780:2017)
Ta slovenski standard je istoveten z: EN ISO 14780:2017
ICS:
75.160.10 Trda goriva Solid fuels
75.160.40 Biogoriva Biofuels
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 14780
EUROPEAN STANDARD
NORME EUROPÉENNE
May 2017
EUROPÄISCHE NORM
ICS 75.160.40; 27.190 Supersedes EN 14780:2011
English Version
Solid biofuels - Sample preparation (ISO 14780:2017)
Biocombustibles solides - Préparation des échantillons Biogene Festbrennstoffe - Probenherstellung (ISO
(ISO 14780:2017) 14780:2017)
This European Standard was approved by CEN on 15 March 2017.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2017 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 14780:2017 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
This document (EN ISO 14780:2017) has been prepared by Technical Committee ISO/TC 238 "Solid
biofuels" in collaboration with Technical Committee CEN/TC 335 “Solid biofuels” the secretariat of
which is held by SIS.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by November 2017, and conflicting national standards
shall be withdrawn at the latest by November 2017.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent
rights.
This document supersedes EN 14780:2011.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 14780:2017 has been approved by CEN as EN ISO 14780:2017 without any modification.

INTERNATIONAL ISO
STANDARD 14780
First edition
2017-04
Solid biofuels — Sample preparation
Biocombustibles solides — Préparation des échantillons
Reference number
ISO 14780:2017(E)
©
ISO 2017
ISO 14780:2017(E)
© ISO 2017, Published in Switzerland
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Ch. de Blandonnet 8 • CP 401
CH-1214 Vernier, Geneva, Switzerland
Tel. +41 22 749 01 11
Fax +41 22 749 09 47
copyright@iso.org
www.iso.org
ii © ISO 2017 – All rights reserved

ISO 14780:2017(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Symbols . 2
5 Principles of correct sample reduction . 2
6 Apparatus . 2
6.1 Apparatus for sample division. 2
6.1.1 General. 2
6.1.2 Riffle boxes . 2
6.1.3 Rotary sample dividers . 3
6.1.4 Shovels and scoops . 4
6.2 Apparatus for particle size-reduction . 5
6.2.1 Coarse cutting mill or wood crusher . 5
6.2.2 Cutting mill . 5
6.2.3 Axe . 6
6.2.4 Hand saw . 6
6.2.5 Sieves . 6
6.2.6 Balance . 6
7 Sample reduction — General principles . 6
8 Methods for sample division . 8
8.1 General . 8
8.2 Riffling . 9
8.3 Strip mixing. 9
8.4 Long pile-alternate shovel method . 9
8.5 Rotary divider .10
8.6 Coning and quartering .10
8.7 Mass reducing straw-like material (handful sampling).10
9 Method for reducing laboratory samples to sub-samples and general analysis samples.11
9.1 Mixing .11
9.2 Initial sample division .11
9.3 Pre-drying .11
9.4 Coarse cutting (particle size reduction to <31,5 mm) .12
9.5 Sample division of <31,5 mm material .12
9.6 Particle size reduction of <31,5 mm material to <1 mm .12
9.7 Sample division of <1 mm material .13
9.8 Particle size reduction of <1 mm material to <0,25 mm .13
10 Storage and labelling.13
11 Performance characteristics .13
Annex A (informative) Precision in relation to division method .14
Annex B (informative) Scheme of sample preparation for samples from single delivery .19
Annex C (informative) Scheme of sample preparation for samples from continuous delivery .20
Bibliography .22
ISO 14780:2017(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directive
...

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