ASTM D6686-01(2019)
(Test Method)Standard Test Method for Evaluation of Tannin Stain Resistance of Coatings
Standard Test Method for Evaluation of Tannin Stain Resistance of Coatings
SIGNIFICANCE AND USE
5.1 Tannins and other chromophoric extractives are naturally occurring materials in wood and wood-based substrates. Tannins are prevalent to a high degree in cedar, redwood, oak, and to a lesser degree in white and yellow pine. Tannins are also present in varying amounts in wood composition products. These extractives are solubilized and darkened in color by aqueous coatings, resulting in unsightly yellow or brown discolorations. This test method is designed to show the relative ability of paints to prevent tannin bleed-through. Typically, cedar or redwood panels are used for this test.
SCOPE
1.1 This test method is an accelerated procedure to determine the effectiveness of latex coatings at preventing the migration of tannin stains from wood substrates.
1.2 The values in SI units are to be regarded as the standard. The values in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
General Information
- Status
- Published
- Publication Date
- 31-Mar-2019
- Technical Committee
- D01 - Paint and Related Coatings, Materials, and Applications
- Drafting Committee
- D01.42 - Architectural Coatings
Relations
- Replaces
ASTM D6686-01(2013) - Standard Test Method for Evaluation of Tannin Stain Resistance of Coatings - Effective Date
- 01-Apr-2019
- Effective Date
- 01-Oct-2019
- Effective Date
- 01-Jun-2013
- Effective Date
- 01-Nov-2012
- Effective Date
- 01-Jun-2009
- Effective Date
- 01-Jun-2008
- Effective Date
- 01-Jun-2007
- Effective Date
- 01-Jun-2004
- Effective Date
- 01-Dec-2003
- Effective Date
- 10-Feb-2002
- Effective Date
- 10-Dec-1999
- Refers
ASTM D1475-98 - Standard Test Method for Density of Liquid Coatings, Inks, and Related Products - Effective Date
- 10-Oct-1998
- Effective Date
- 01-Apr-2019
- Referred By
ASTM D6763-16(2022) - Standard Guide for Testing Exterior Wood Stains and Clear Water Repellents - Effective Date
- 01-Apr-2019
- Effective Date
- 01-Apr-2019
Overview
ASTM D6686-01(2019), "Standard Test Method for Evaluation of Tannin Stain Resistance of Coatings," is a widely-recognized ASTM International standard that provides an accelerated procedure for assessing the effectiveness of latex coatings in preventing tannin stain migration from wood substrates. Tannins and other chromophoric extractives in woods such as cedar, redwood, oak, and pines can lead to undesirable yellow or brown discoloration when they migrate through coatings. This standard is essential for manufacturers, coating formulators, and quality assurance professionals seeking reliable and standardized methods for evaluating stain-blocking performance on wood and wood-based products.
Key Topics
- Tannin Stain Resistance: Defines and measures the ability of a coating, particularly latex paints, to prevent tannins and other extractives from migrating to and discoloring the surface.
- Accelerated Testing: Uses a controlled condensation chamber to simulate challenging conditions and accelerate the exposure of coated wood to moisture, increasing the likelihood of tannin migration.
- Objective and Subjective Evaluation: Incorporates both quantitative data, such as CIELAB L* (lightness) and b* (yellowness) values via spectrophotometry, and subjective ratings using an ASTM 0-10 scale to assess stain severity.
- Standardized Apparatus and Procedures: Specifies substrate dimensions and types, preparation of test samples and brushes, environmental chamber conditions, and protocols for applying and curing coatings.
- Universal Applicability: Acknowledges variations in wood species, grain patterns, and extractive contents, emphasizing the importance of using control paints and careful sample selection.
Applications
Adoption of ASTM D6686-01(2019) is particularly valuable for:
- Paint and Coating Manufacturers: Verifying claims related to stain-blocking properties and ensuring product consistency before market release.
- Quality Control Laboratories: Providing a reliable, repeatable method for evaluating batches of coatings during production, reducing the risk of product failure in the field.
- Architectural and Wood Product Industries: Assisting specifiers in selecting coatings that offer superior tannin stain resistance, contributing to the long-term appearance and performance of exterior and interior woodwork.
- Regulatory Compliance and R&D: Supporting documentation needed for compliance with industry and client-specific requirements, as well as benchmarking new coating formulations.
- Technical Communication: Facilitating clear reporting, comparison, and communication of results using both objective metrics (L*, b* values) and subjective scores.
Related Standards
Several other ASTM standards are referenced or commonly used in conjunction with ASTM D6686-01(2019):
- ASTM D1475 – Test Method for Density of Liquid Coatings, Inks, and Related Products
- ASTM D4585 – Practice for Testing Water Resistance of Coatings Using Controlled Condensation
- ASTM D5068 – Practice for Preparation of Paint Brushes for Evaluation
These related standards help ensure the accuracy and consistency of the tannin stain resistance test by providing additional procedures for equipment and substrate preparation, as well as physical property measurement.
Keywords: tannin stain resistance, coatings, latex paint, ASTM D6686, wood stain blocking, wood extractives, accelerated testing, CIELAB, stain-blocking coatings, quality control.
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Frequently Asked Questions
ASTM D6686-01(2019) is a standard published by ASTM International. Its full title is "Standard Test Method for Evaluation of Tannin Stain Resistance of Coatings". This standard covers: SIGNIFICANCE AND USE 5.1 Tannins and other chromophoric extractives are naturally occurring materials in wood and wood-based substrates. Tannins are prevalent to a high degree in cedar, redwood, oak, and to a lesser degree in white and yellow pine. Tannins are also present in varying amounts in wood composition products. These extractives are solubilized and darkened in color by aqueous coatings, resulting in unsightly yellow or brown discolorations. This test method is designed to show the relative ability of paints to prevent tannin bleed-through. Typically, cedar or redwood panels are used for this test. SCOPE 1.1 This test method is an accelerated procedure to determine the effectiveness of latex coatings at preventing the migration of tannin stains from wood substrates. 1.2 The values in SI units are to be regarded as the standard. The values in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
SIGNIFICANCE AND USE 5.1 Tannins and other chromophoric extractives are naturally occurring materials in wood and wood-based substrates. Tannins are prevalent to a high degree in cedar, redwood, oak, and to a lesser degree in white and yellow pine. Tannins are also present in varying amounts in wood composition products. These extractives are solubilized and darkened in color by aqueous coatings, resulting in unsightly yellow or brown discolorations. This test method is designed to show the relative ability of paints to prevent tannin bleed-through. Typically, cedar or redwood panels are used for this test. SCOPE 1.1 This test method is an accelerated procedure to determine the effectiveness of latex coatings at preventing the migration of tannin stains from wood substrates. 1.2 The values in SI units are to be regarded as the standard. The values in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM D6686-01(2019) is classified under the following ICS (International Classification for Standards) categories: 19.040 - Environmental testing; 25.220.01 - Surface treatment and coating in general. The ICS classification helps identify the subject area and facilitates finding related standards.
ASTM D6686-01(2019) has the following relationships with other standards: It is inter standard links to ASTM D6686-01(2013), ASTM D5068-04(2019), ASTM D5068-04(2013), ASTM D1475-98(2012), ASTM D5068-04(2009), ASTM D1475-98(2008), ASTM D4585-07, ASTM D5068-04, ASTM D1475-98(2003), ASTM D5068-02, ASTM D4585-99, ASTM D1475-98, ASTM D5324-16(2022), ASTM D6763-16(2022), ASTM D5146-10(2019). Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
ASTM D6686-01(2019) is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.
Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D6686 − 01 (Reapproved 2019)
Standard Test Method for
Evaluation of Tannin Stain Resistance of Coatings
This standard is issued under the fixed designation D6686; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 4. Summary of Test Method
1.1 This test method is an accelerated procedure to deter-
4.1 This test method utilizes a condensation test chamber to
mine the effectiveness of latex coatings at preventing the
determine the tannin stain resistance of latex paints. The test
migration of tannin stains from wood substrates.
paints are applied to substrates that contain tannin extractives
and are placed on or in the test chamber. CIELAB L* and b*
1.2 The values in SI units are to be regarded as the standard.
valuesaswellassubjectiveratingsarerecordedafterexposure.
The values in parentheses are for information only.
1.3 This standard does not purport to address all of the
5. Significance and Use
safety concerns, if any, associated with its use. It is the
5.1 Tannins and other chromophoric extractives are natu-
responsibility of the user of this standard to establish appro-
priate safety, health, and environmental practices and deter- rally occurring materials in wood and wood-based substrates.
Tannins are prevalent to a high degree in cedar, redwood, oak,
mine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accor- and to a lesser degree in white and yellow pine. Tannins are
alsopresentinvaryingamountsinwoodcompositionproducts.
dance with internationally recognized principles on standard-
These extractives are solubilized and darkened in color by
ization established in the Decision on Principles for the
aqueous coatings, resulting in unsightly yellow or brown
Development of International Standards, Guides and Recom-
discolorations. This test method is designed to show the
mendations issued by the World Trade Organization Technical
relative ability of paints to prevent tannin bleed-through.
Barriers to Trade (TBT) Committee.
Typically, cedar or redwood panels are used for this test.
2. Referenced Documents
6. Apparatus
2.1 ASTM Standards:
D1475 Test Method for Density of Liquid Coatings, Inks,
6.1 Test Chamber, as described in Practice D4585.
and Related Products
6.2 Test Substrate, 15.2 by 121.9 cm (6 by 48 in.) substrate
D4585 Practice for Testing Water Resistance of Coatings
or of a size agreed upon by the purchaser and seller of the
Using Controlled Condensation
coating being tested.
D5068 Practice for Preparation of Paint Brushes for Evalu-
6.3 Paint Brush, nylon/polyester brush of good quality.
ation
6.4 Spectrophotometer.
3. Terminology
6.5 Electronic Balance.
3.1 Definitions:
6.6 Conditioned Room,at18to29.5 °C(65to85 °F)and40
3.1.1 tannin stain resistance, n—the ability of a coating to
prevent the migration of tannins or other wood-based chromo- to 60 % relative humidity.
spheres to the surface of a film.
7. Reagents and Materials
7.1 Wood Panels—Such as cedar, redwood, oak, white pine,
This test method is under the jurisdiction of ASTM Committee D01 on Paint
yellow pine, or other substrate as agreed upon between the
and Related Coatings, Materials, andApplications and is the direct responsibility of
purchaser and the seller of the coating being tested.
Subcommittee D01.42 on Architectural Coatings.
Current edition approved April 1, 2019. Published April 2019. Originally
7.2 Control Paint—An agreed-upon paint of known tannin
approved in 2001. Last previous edition approved in 2013 as D6686 – 01 (2013).
stain resistance.
DOI: 10.1520/D6686-01R19.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
7.3 Test Paints—Since there are no standard panels,
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
photographs, or paints for this test method, an agreed-upon
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. control paint (7.2) should be included as one of the test paints.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D6686 − 01 (2019)
8. Procedure place backprimed panels fully inside the chamber if agreed
uponbetweenthepurchaserandseller.Allpanelsshouldberun
8.1 Choose a substrate with a consistent grain pattern.
similarly. If the panels are placed on the chamber, fill all spaces
Patterns vary greatly from panel to panel, so try to select a
in the specimen rack with test boards or blanks. Close all
board that has consistent wood grain across the length of the
cracks between boards to prevent water vapor loss and tem-
substrate. Results may vary from panel to panel because of
perature variation. Larger cracks may be closed with tape or
different growth rates, grain angles, colors, and species of
metal strips. If the panels are placed inside the chamber, make
wood. If necessary, panels may be sanded to remove raised
sure panels are placed at an angle to avoid water spotting and
grain. Substrates with areas of rough spots should be avoided,
run off onto the test areas
...




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