ASTM D7453-17
(Practice)Standard Practice for Sampling of Petroleum Products for Analysis by Process Stream Analyzers and for Process Stream Analyzer System Validation
Standard Practice for Sampling of Petroleum Products for Analysis by Process Stream Analyzers and for Process Stream Analyzer System Validation
SIGNIFICANCE AND USE
5.1 Analyzer systems require representative samples of petroleum products delivered in a timely manner to (1) facilitate the control of process or blending units or (2) calculate a flow proportioned property value.
5.2 Representative samples of petroleum products are required for the determination of chemical and physical properties. These properties are used to establish the relationship between the analyzer system and the primary test method during initial and ongoing validation of the system.
5.3 Representative samples of petroleum products are tested to determine the chemical and physical properties of a batch offered for tender.
SCOPE
1.1 This practice covers the performance requirements for sample systems employed to deliver process stream samples (1) to analyzer system for analyses or (2) for analyzer validation or (3) for composite sample systems. It also outlines the selection and operation of line or batch sampling equipment intended for analyzer flow proportioned average property value system validation. Sample handling, mixing, and conditioning procedures are required to ensure that a representative sample of the liquid petroleum product is collected from the sampling source.
1.2 Applicable Fluids—This practice is applicable to single liquid phase petroleum products whose vapor pressure at sampling and sample storage conditions is less than or equal to 110 kPa (16.0 psi), and, with a D86 final boiling point less than or equal to 400 °C (752 °F).
1.2.1 Specialized sample handling may be necessary to maintain sample integrity of more volatile materials at high temperatures or extended residence time in the receiver. Such handling requirements are not within the scope of this practice. Users should consult the analytical methods to be performed on the sample for special sample storage or conditioning requirements.
1.3 Some or all of the processes outlined in this practice may be applicable to other liquids. Applying this practice to other liquids will require the consideration of additional methods and practices. It is the responsibility of the user of this standard to identify any and all applicable safety and sampling considerations and establish appropriate procedures to handle these additional considerations.
1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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Designation: D7453 − 17
Standard Practice for
Sampling of Petroleum Products for Analysis by Process
Stream Analyzers and for Process Stream Analyzer System
1
Validation
This standard is issued under the fixed designation D7453; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
The primary focus of sampling petroleum product is the timely presentation of the sample for (1)
analysis by online analyzers, (2) validation of an analyzer system and (3) collecting a composite
sample for batch physical property determination. Sediment, free water, rust, and other contaminants
found in the sample may be removed in the sample conditioning system to protect the hardware and
analytical systems. If a sample is being collected for later analysis, the sample receiver must not alter
or degrade the physical make up of the sample in any way. If a sample is being fed to an analyzer or
sampled for later determination of water or particulate contamination then filtering is not an option.
1. Scope* 1.3 Some or all of the processes outlined in this practice
may be applicable to other liquids. Applying this practice to
1.1 This practice covers the performance requirements for
other liquids will require the consideration of additional
sample systems employed to deliver process stream samples
methods and practices. It is the responsibility of the user of this
(1) to analyzer system for analyses or (2) for analyzer
standard to identify any and all applicable safety and sampling
validation or (3) for composite sample systems. It also outlines
considerations and establish appropriate procedures to handle
theselectionandoperationoflineorbatchsamplingequipment
these additional considerations.
intendedforanalyzerflowproportionedaveragepropertyvalue
system validation. Sample handling, mixing, and conditioning 1.4 The values stated in SI units are to be regarded as the
procedures are required to ensure that a representative sample standard. The values given in parentheses are for information
of the liquid petroleum product is collected from the sampling only.
source.
1.5 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
1.2 Applicable Fluids—This practice is applicable to single
responsibility of the user of this standard to establish appro-
liquid phase petroleum products whose vapor pressure at
priate safety, health, and environmental practices and deter-
sampling and sample storage conditions is less than or equal to
mine the applicability of regulatory limitations prior to use.
110 kPa (16.0 psi), and, with a D86 final boiling point less than
1.6 This international standard was developed in accor-
or equal to 400 °C (752 °F).
dance with internationally recognized principles on standard-
1.2.1 Specialized sample handling may be necessary to
ization established in the Decision on Principles for the
maintain sample integrity of more volatile materials at high
Development of International Standards, Guides and Recom-
temperatures or extended residence time in the receiver. Such
mendations issued by the World Trade Organization Technical
handling requirements are not within the scope of this practice.
Barriers to Trade (TBT) Committee.
Usersshouldconsulttheanalyticalmethodstobeperformedon
the sample for special sample storage or conditioning require-
2. Referenced Documents
ments.
2
2.1 ASTM Standards:
D3764 Practice forValidation of the Performance of Process
1 Stream Analyzer Systems
This practice is under the jurisdiction of ASTM Committee D02 on Petroleum
Products, Liquid Fuels, and Lubricants and is the direct responsibility of Subcom-
mittee D02.25 on Performance Assessment and Validation of Process Stream
2
Analyzer Systems. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Dec. 1, 2017. Published January 2018. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 2009. Last previous edition approved in 2015 as D7453 – 09 (2015). Standards volume information, refer to the standard’s Document Summary page on
DOI: 10.1520/D7453-17. the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D7453 − 17
D6122 Practice for Validation of the Performance of Multi- indicates a value corresponding to 99.5 % of the subsequent
variate Online, At-Line, and Laboratory Infrared Spectr
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D7453 − 09 (Reapproved 2015) D7453 − 17
Standard Practice for
Sampling of Petroleum Products for Analysis by Process
Stream Analyzers and for Process Stream Analyzer System
1
Validation
This standard is issued under the fixed designation D7453; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
The primary focus of sampling petroleum product is the timely presentation of the sample for (1)
analysis by online analyzers, (2) validation of an analyzer system and (3) collecting a composite
sample for batch physical property determination. Sediment, free water, rust, and other contaminants
found in the sample may be removed in the sample conditioning system to protect the hardware and
analytical systems. If a sample is being collected for later analysis, the sample receiver must not alter
or degrade the physical make up of the sample in any way. If a sample is being feedfed to an analyzer
or sampled for latterlater determination of water or particulate contamination then filtering is not an
option.
1. Scope Scope*
1.1 This practice covers the performance requirements for sample systems employed to deliver process stream samples (1) to
analyzer system for analyses or (2) for analyzer validation or (3) for composite sample systems. It also outlines the selection and
operation of line or batch sampling equipment intended for analyzer flow proportioned average property value system validation.
Sample handling, mixing, and conditioning procedures are required to ensure that a representative sample of the liquid petroleum
product is collected from the sampling source.
1.2 Applicable Fluids—This practice is applicable to single liquid phase petroleum products whose vapor pressure at sampling
and sample storage conditions is less than or equal to 110 kPa (16.0 psi), and, with a D86 final boiling point less than or equal to
400 °C (752 °F).
1.2.1 Specialized sample handling may be necessary to maintain sample integrity of more volatile materials at high temperatures
or extended residence time in the receiver. Such handling requirements are not within the scope of this practice. Users should
consult the analytical methods to be performed on the sample for special sample storage or conditioning requirements.
1.3 Some or all of the processes outlined in this practice may be applicable to other liquids. Applying this practice to other
liquids will require the consideration of additional methods and practices. It is the responsibility of the user of this standard to
identify any and all applicable safety and sampling considerations and establish appropriate procedures to handle these additional
considerations.
1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
1
This practice is under the jurisdiction of ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of Subcommittee
D02.25 on Performance Assessment and Validation of Process Stream Analyzer Systems.
Current edition approved April 1, 2015Dec. 1, 2017. Published May 2015January 2018. Originally approved in 2009. Last previous edition approved in 20092015 as
D7453 – 09.D7453 – 09 (2015). DOI: 10.1520/D7453-09R15.10.1520/D7453-17.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D7453 − 17
2. Referenced Documents
2
2.1 ASTM Standards:
D3764 Practice for Validation of the Performance of Process Stream Analyzer Systems
D6122 Practice
...
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