Standard Test Method for Reboiling Tendency of Sheet Steel for Porcelain Enameling

SIGNIFICANCE AND USE
5.1 The results of this test indicate whether or not a sheet steel will cause reboiling under one given set of enameling conditions and enable the enamel processor to establish a possible source of imperfections in the finished coating.  
5.2 This test method is normally used to test samples from lots, coils, or lifts of sheet steel which for some reason, production problems, defects evident on enameled parts, or production experience are suspected of causing defects in enameled ware which have the appearance of reboiling. It is often used to establish whether a problem exists with the bare steel or other factors such as the porcelain enamel, processing contamination, and so forth.
SCOPE
1.1 This test method covers the determination of whether a sheet steel for porcelain enameling will reboil under a given set of worse case conditions.  
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Mar-2021

Relations

Effective Date
01-Sep-2009
Effective Date
01-Oct-2004
Effective Date
10-Oct-1999

Overview

ASTM C632-88(2021): Standard Test Method for Reboiling Tendency of Sheet Steel for Porcelain Enameling is a key ASTM International standard developed to determine whether sheet steel is likely to cause reboiling under specified porcelain enameling conditions. This test method supports enamel processors and manufacturers in evaluating potential defects in the coating, enhancing both the quality and reliability of enameled steel products. By simulating worst-case enameling scenarios, the standard provides critical data for identifying sources of imperfections in finished ware, such as gas evolution or blistering.

Key Topics

  • Purpose: The primary focus of ASTM C632 is to indicate if a particular sheet steel sample will cause reboiling, typically manifested as bubbling or blistering, under controlled enameling conditions.
  • Sampling: The test is applied to samples from lots, coils, or lifts of sheet steel, especially when defects have been observed or are suspected during production.
  • Test Method: Steel samples are cleaned, coated with a porcelain enamel ground coat, and subjected to repeated firing cycles. The surfaces are then visually inspected for signs of reboiling, such as the formation of bubbles.
  • Condition Assessment: Determining reboiling helps establish whether observed defects in enameled ware are attributable to the base steel, the enamel itself, or other processing factors.
  • Definitions: The standard clarifies terms such as ‘ground coat,’ ‘reboiling,’ and ‘slip (slurry),’ ensuring consistent communication and application across laboratories.

Applications

ASTM C632 is widely recognized as an essential quality assurance tool in the porcelain enameling industry, particularly for manufacturers of home appliances, commercial cookware, sanitary ware, architectural components, and automotive parts. Key applications include:

  • Quality Control: Enables rapid identification of incompatible or defective sheet steel prior to full-scale enamel production, reducing material waste and rework.
  • Troubleshooting: Assists in isolating the source of coating defects, whether they arise from the base steel, enameling process, or external contamination.
  • Supplier Evaluation: Facilitates material acceptance checks and supplier quality audits by verifying the suitability of steel shipments for high-quality porcelain enameling.
  • Process Validation: Supports fine-tuning of manufacturing and enameling processes by providing clear pass/fail criteria for reboiling.
  • R&D Support: Offers a standardized method for developing and refining new porcelain enamel formulations and processing techniques.

Related Standards

  • ASTM C286: Terminology Relating to Porcelain Enamel and Ceramic-Metal Systems - defines essential terms and concepts referenced throughout ASTM C632.
  • ISO and EN standards related to porcelain enameling and ceramic-metal systems - complementary resources for global manufacturers and multi-standard compliance.
  • Other ASTM Metallic and Inorganic Coatings standards - provide guidelines for enamel ground coat properties, adherence testing, and production quality.

Practical Value

Implementing ASTM C632-88(2021) helps porcelain enamel processors ensure high product quality, reduce production downtime due to unforeseen defects, and optimize material selection. By adhering to this international test method, organizations can improve their capability to deliver durable, aesthetically pleasing, and defect-free enameled steel products that meet stringent industry and customer requirements.

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Frequently Asked Questions

ASTM C632-88(2021) is a standard published by ASTM International. Its full title is "Standard Test Method for Reboiling Tendency of Sheet Steel for Porcelain Enameling". This standard covers: SIGNIFICANCE AND USE 5.1 The results of this test indicate whether or not a sheet steel will cause reboiling under one given set of enameling conditions and enable the enamel processor to establish a possible source of imperfections in the finished coating. 5.2 This test method is normally used to test samples from lots, coils, or lifts of sheet steel which for some reason, production problems, defects evident on enameled parts, or production experience are suspected of causing defects in enameled ware which have the appearance of reboiling. It is often used to establish whether a problem exists with the bare steel or other factors such as the porcelain enamel, processing contamination, and so forth. SCOPE 1.1 This test method covers the determination of whether a sheet steel for porcelain enameling will reboil under a given set of worse case conditions. 1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE 5.1 The results of this test indicate whether or not a sheet steel will cause reboiling under one given set of enameling conditions and enable the enamel processor to establish a possible source of imperfections in the finished coating. 5.2 This test method is normally used to test samples from lots, coils, or lifts of sheet steel which for some reason, production problems, defects evident on enameled parts, or production experience are suspected of causing defects in enameled ware which have the appearance of reboiling. It is often used to establish whether a problem exists with the bare steel or other factors such as the porcelain enamel, processing contamination, and so forth. SCOPE 1.1 This test method covers the determination of whether a sheet steel for porcelain enameling will reboil under a given set of worse case conditions. 1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM C632-88(2021) is classified under the following ICS (International Classification for Standards) categories: 25.220.50 - Enamels. The ICS classification helps identify the subject area and facilitates finding related standards.

ASTM C632-88(2021) has the following relationships with other standards: It is inter standard links to ASTM C286-99(2009), ASTM C286-99(2004), ASTM C286-99. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

ASTM C632-88(2021) is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.

Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: C632 − 88 (Reapproved 2021)
Standard Test Method for
Reboiling Tendency of Sheet Steel for Porcelain Enameling
This standard is issued under the fixed designation C632; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
The results of this test indicate whether or not a sheet steel will cause reboiling under one given set
of enameling conditions, and enable the enamel processor to establish a possible cause of
imperfections in the finished coating. This may be performed in any laboratory equipped for porcelain
enamel. It does not require facilities for metal surface preparation.
1. Scope 3.1.1 ground coat—a porcelain enamel applied directly to
the base metal to function as an intermediate layer between the
1.1 This test method covers the determination of whether a
metal and the cover coat (see Terminology C286).
sheet steel for porcelain enameling will reboil under a given set
of worse case conditions.
3.1.2 reboiling—gas evolution occurring and recurring dur-
ing repeated firing of the ground coat, sometimes a defect (see
1.2 The values stated in inch-pound units are to be regarded
Terminology C286).
as the standard. The values given in parentheses are for
information only.
3.1.3 slip (slurry)— a suspension of finely divided material
1.3 This standard does not purport to address all of the in liquid (see Terminology C286).
safety concerns, if any, associated with its use. It is the
3.2 Definitions of Terms Specific to This Standard:
responsibility of the user of this standard to establish appro-
3.2.1 quarter lines—imaginary lines parallel to the direction
priate safety, health, and environmental practices and deter-
of rolling positioned at a distance from the sheet mill edge,
mine the applicability of regulatory limitations prior to use.
equal to one quarter of the sheet width.
1.4 This international standard was developed in accor-
dance with internationally recognized principles on standard-
4. Summary of Test Method
ization established in the Decision on Principles for the
Development of International Standards, Guides and Recom-
4.1 Both surfaces of sheet steel sample plates are subjected
mendations issued by the World Trade Organization Technical
to a cleaning treatment and are then porcelain enameled with a
Barriers to Trade (TBT) Committee.
sheet-steel, ground-coat type finish. Subsequent reheating at
various times is performed to reveal whether or not the steel
2. Referenced Documents
will cause reboiling. The presence or absence of reboiling is
2.1 ASTM Standards: determined by visual inspection.
C286 Terminology Relating to Porcelain Enamel and
Ceramic-Metal Systems 5. Significance and Use
5.1 The results of this test indicate whether or not a sheet
3. Terminology
steel will cause reboiling under one given set of enameling
3.1 Definitions:
conditions and enable the enamel processor to establish a
possible source of imperfections in the finished coating.
This test method is under the jurisdiction ofASTM Committee B08 on Metallic 5.2 This test method is normally used to test samples from
and Inorganic Coatings and is the direct responsibility of Subcommittee B08.12 on
lots, coils, or lifts of sheet steel which for some reason,
Materials for Porcelain Enamel and Ceramic-Metal Systems.
production problems, defects evident on enameled parts, or
Current edition approved April 1, 2021. Published May 2021. Originally
production experience are suspected of causing defects in
approvedin1969.Lastpreviouseditionapprovedin2016asC632 – 88(2016).DOI:
10.1520/C0632-88R21.
enameled ware which have the appearance of reboiling. It is
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
often used to establish whether a problem exists with the bare
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
steel or other factors such as the porcelain enamel, processing
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. contamination, and so forth.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
C632 − 88 (2021)
6. Apparatus sufficient time to fuse the ground-coat enamel to the base
metal. This time and temperature should be that recommended
6.1 This test can be conducted in any laboratory equipped
by the porcelain enamel manufacturers for optimum adherence
for general porcelain enameling. It does not require facilities
(maturing temperature).
for metal surface preparation.
NOTE 1—Thin fired coatings of 2 ⁄2 to 3 mils (
...

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