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ASTM D7707-21

(Specification)

Standard Specification for Wipe Sampling Materials for Beryllium in Surface Dust

Standard Specification for Wipe Sampling Materials for Beryllium in Surface Dust

SCOPE
1.1 This specification covers requirements for premoistened wipe materials that are used to collect settled dusts on surfaces for the subsequent determination of beryllium.  
1.2 For wipe materials used for the determination of lead in surface dust, refer to Specification E1792. This is mentioned to insure that users of wipes recognize that there is some relationship between wipes and the analyte of interest.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This specification contains notes that are explanatory and are not part of the mandatory requirements of the specification.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Aug-2021
ICS
71.040.50 - Physicochemical methods of analysis
Technical Committee
D22 - Air Quality
Drafting Committee
D22.04 - Workplace Air Quality
Current Stage
Ref Project

Relations

Refers
ASTM D1356-20a - Standard Terminology Relating to Sampling and Analysis of Atmospheres
Effective Date
01-Sep-2020
Refers
ASTM D1356-20 - Standard Terminology Relating to Sampling and Analysis of Atmospheres
Effective Date
15-Mar-2020

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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation:D7707 −21
Standard Specification for
1
Wipe Sampling Materials for Beryllium in Surface Dust
This standard is issued under the fixed designation D7707; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D7035 Test Method for Determination of Metals and Met-
alloids in Airborne Particulate Matter by Inductively
1.1 This specification covers requirements for premoistened
Coupled Plasma Atomic Emission Spectrometry (ICP-
wipe materials that are used to collect settled dusts on surfaces
AES)
for the subsequent determination of beryllium.
D7202 Test Method for Determination of Beryllium in the
1.2 For wipe materials used for the determination of lead in
Workplace by Extraction and Optical Fluorescence Detec-
surface dust, refer to Specification E1792.This is mentioned to
tion
insure that users of wipes recognize that there is some
D7439 Test Method for Determination of Elements in Air-
relationship between wipes and the analyte of interest.
borne Particulate Matter by Inductively Coupled Plasma-
–Mass Spectrometry
1.3 The values stated in SI units are to be regarded as
standard. No other units of measurement are included in this E105 Guide for Probability Sampling of Materials
E691 Practice for Conducting an Interlaboratory Study to
standard.
Determine the Precision of a Test Method
1.4 This specification contains notes that are explanatory
E1792 Specification for Wipe Sampling Materials for Lead
and are not part of the mandatory requirements of the specifi-
in Surface Dust
cation.
1.5 This standard does not purport to address all of the
3. Terminology
safety concerns, if any, associated with its use. It is the
3.1 For definitions of pertinent terms not listed here, see
responsibility of the user of this standard to establish appro-
Terminology D1356.
priate safety, health, and environmental practices and deter-
3.2 Definitions of Terms Specific to This Standard:
mine the applicability of regulatory limitations prior to use.
3.2.1 lot, n—a finite quantity of a given product manufac-
1.6 This international standard was developed in accor-
tured under production conditions that are considered uniform.
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the
3.2.2 standard beryllium test method, n—as used in this
Development of International Standards, Guides and Recom-
specification, any of the following test methods: D7035,
mendations issued by the World Trade Organization Technical
D7202, D7439, the graphite furnace atomic absorption tech-
3
Barriers to Trade (TBT) Committee.
nique in NIOSH Method 7102, or a equivalent test method
issued by a national or international consensus standard orga-
2. Referenced Documents
nization.
2
2.1 ASTM Standards:
3.2.3 wipe, n—a disposable towellette that may or may not
D1356 Terminology Relating to Sampling and Analysis of
be premoistened with an acceptable wetting agent, depending
Atmospheres
on the intended application for obtaining beryllium samples.
D6966 Practice for Collection of Settled Dust Samples
3.2.3.1 Discussion—The towellette is used to collect a
Using Wipe Sampling Methods for Subsequent Determi-
sample of settled dust on a surface for subsequent beryllium
nation of Metals
analysis.
4. Significance and Use
1
This specification is under the jurisdiction of ASTM Committee D22 on Air
Quality and is the direct responsibility of Subcommittee D22.04 on Workplace Air
4.1 This specification is intended for use by manufacturers
Quality.
and suppliers to evaluate the performance of wipe sampling
Current edition approved Sept. 1, 2021. Published October 2021. Originally
materials for beryllium in surface dust.
approved in 2011. Last previous edition approved in 2016 as D7707 – 11 (2016).
DOI: 10.1520/D7707-21.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
3
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM National Institute for Occupational Safety and Health, NIOSH Manual of
Standards volume information, refer to the standard’s Document Summary page on Analytical Methods, 4th ed., NIOSH, Cincinnati, OH, 1994, available from
the ASTM website. www.cdc.gov/niosh/nmam.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D7707−21
4.2 This specification may also be employed by
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D7707 − 11 (Reapproved 2016) D7707 − 21
Standard Specification for
1
Wipe Sampling Materials for Beryllium in Surface Dust
This standard is issued under the fixed designation D7707; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This specification covers requirements for premoistened wipe materials that are used to collect settled dusts on surfaces for
the subsequent determination of beryllium.
1.2 For wipe materials used for the determination of lead in surface dust, refer to Specification E1792. This is mentioned to insure
that users of wipes recognize that there is some relationship between wipes and the analyte of interest.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This specification contains notes that are explanatory and are not part of the mandatory requirements of the specification.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D1356 Terminology Relating to Sampling and Analysis of Atmospheres
D6966 Practice for Collection of Settled Dust Samples Using Wipe Sampling Methods for Subsequent Determination of Metals
D7035 Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma
Atomic Emission Spectrometry (ICP-AES)
D7202 Test Method for Determination of Beryllium in the Workplace by Extraction and Optical Fluorescence Detection
D7439 Test Method for Determination of Elements in Airborne Particulate Matter by Inductively Coupled Plasma–Mass
Spectrometry
E105 Guide for Probability Sampling of Materials
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
E1613 Test Method for Determination of Lead by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES),
Flame Atomic Absorption Spectrometry (FAAS), or Graphite Furnace Atomic Absorption Spectrometry (GFAAS) Techniques
3
(Withdrawn 2021)
1
This specification is under the jurisdiction of ASTM Committee D22 on Air Quality and is the direct responsibility of Subcommittee D22.04 on Workplace Air Quality.
Current edition approved Oct. 1, 2016Sept. 1, 2021. Published October 2016October 2021. Originally approved in 2011. Last previous edition approved in 20112016 as
D7707 – 11.D7707 DOI: 10.1520/D7707-11R16. – 11 (2016). DOI: 10.1520/D7707-21.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D7707 − 21
E1792 Specification for Wipe Sampling Materials for Lead in Surface Dust
3. Terminology
3.1 For definitions of pertinent terms not listed here, see Terminology D1356.
3.2 Definitions of Terms Specific to This Standard:
3.2.1 lot, n—a finite quantity of a given product manufactured under production conditions that are considered uniform.
3.2.2 standard beryllium test method, n—as used in this specification, any of the following test methods: D7035, D7202, D7439,
3
the graphite furnace atomic absorption technique in TestNIOSH Method E1613,7102, or a equivalent test method issued by a
national or international consensus standard organization.
3.2.3 wipe, n—a disposable towellette that is may or may not be premoistened with an acceptable agent.wetting agent, depending
on the intended application for obtaining beryllium samples.
3.2.3.1 Discussion—
The towellette is used to colle
...

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5.1 This practice is for use in the preparation of no more than four wipe samples combined to form a composited sample for subsequent determination of lead content.  
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1.1 This practice covers the acid digestion of surface dust samples (collected using wipe sampling practices) and associated quality control (QC) samples for the determination of lead.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Exception—Informational inch-pound units are provided in Note 3.  
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5.1 This practice is for use in the preparation of no more than four wipe samples collected from equally-sized areas in the same space combined to form a composited sample for subsequent determination of lead content.  
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1.1 This practice covers the extraction of lead (Pb) using ultrasonication, heat and nitric acid from a composited sample of up to four individual wipe samples of settled dust collected from equally-sized areas in the same space.  
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1.1 This practice covers drying, homogenization, and acid digestion of soil samples and associated quality control (QC) samples using a hot plate type method for the determination of lead using laboratory atomic spectrometry analysis techniques such as inductively coupled plasma atomic emission spectrometry (ICP-AES), flame atomic absorption spectrometry (FAAS), and graphite furnace atomic absorption spectrometry (GFAAS).  
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1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Standard Guide for Evaluating Performance of On-Site Extraction and Field-Portable Electrochemical or Spectrophotometric Analysis for Lead

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4.1 This guide is intended for use in evaluating the performance of field-portable electroanalytical or spectrophotometric devices for lead determination, or both.  
4.2 Desired performance criteria for field-based extraction procedures are provided.  
4.3 Performance parameters of concern may be determined using protocols that are referenced in this guide.  
4.4 Example reference materials to be used in assessing the performance of field-portable lead analyzers are listed.  
4.5 Exhaustive details regarding quality assurance issues are outside the scope of this guide. Applicable quality assurance aspects are dealt with extensively in references that are cited in this guide.
SCOPE
1.1 This guide provides guidelines for determining the performance of field-portable quantitative lead analysis instruments.  
1.2 This guide applies to field-portable electroanalytical and spectrophotometric (including reflectance and colorimetric) analyzers.  
1.3 Sample matrices of concern herein include paint, dust, soil, and airborne particles.  
1.4 This guide addresses the desired performance characteristics of field-based sample extraction procedures for lead, as well as on-site extraction followed by field-portable analysis.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM E1792-20(Specification)
Standard Specification for Wipe Sampling Materials for Lead in Surface Dust

ABSTRACT
This specification covers requirements for wipe sampling materials that are used to collect settled dusts on surfaces for the subsequent determination of lead. The wipes shall be tested for conformance to background lead, lead recoverability, collection efficiency, ruggedness which shall be determined using butted vinyl-composite floor tiles as a test surface, moisture content, coefficient of variation in mass, linear dimensions such as mean area and mean length, and mean thickness requirements.
SCOPE
1.1 This specification covers requirements for wipes that are used to collect settled dusts on surfaces for the subsequent determination of lead.  
1.2 For wipe materials used for the determination of beryllium in surface dust refer to Specification D7707. This is mentioned to insure that users of wipes recognize that there is some relationship between the analytical backgrounds found in wipes and the analyte of interest.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D6785-20(Test Method)
Standard Test Method for Determination of Lead in Workplace Air Using Flame or Graphite Furnace Atomic Absorption Spectrometry

SIGNIFICANCE AND USE
6.1 The health of workers in many industries, for example, mining, metal refining, battery manufacture, construction, etc., is at risk through exposure by inhalation of particulate lead and lead compounds. Industrial hygienists and other public health professionals need to determine the effectiveness of measures taken to control workers' exposure, and this is generally achieved by making workplace air measurements. This standard has been published in order to make available a method for making valid exposure measurements for lead. It will be of benefit to: agencies concerned with health and safety at work; industrial hygienists and other public health professionals; analytical laboratories; industrial users of metals and metalloids and their workers, etc. It has been assumed in the drafting of this standard that the execution of its provisions, and the interpretation of the results obtained, is entrusted to appropriately qualified and experienced people.  
6.2 The measuring procedure shall comply with any relevant International, European or National Standard that specifies performance requirements for procedures for measuring chemical agents in workplace air (for example, ISO 20581).
SCOPE
1.1 This standard specifies flame and graphite furnace atomic absorption spectrometric methods for the determination of the time-weighted average mass concentration of particulate lead and lead compounds in workplace air.  
1.2 The method is applicable to personal sampling of the inhalable fraction of airborne particles, as defined in ISO 7708, and to static (area) sampling.  
1.3 The sample dissolution procedure specifies hot plate or microwave digestion, or ultrasonic extraction (10.2). The sample dissolution procedure is not effective for all lead compounds (see Section 5). The use of an alternative, more vigorous dissolution procedure is necessary when it is desired to extract lead from compounds present in the test atmosphere that are insoluble using the dissolution procedures described herein. For example if it is desired to determine silicate lead, a hydrofluoric acid dissolution procedure is required.  
1.4 The flame atomic absorption method is applicable to the determination of masses of approximately 1 to 200 μg of lead per sample, without dilution (1).2 The graphite furnace atomic absorption method is applicable to the determination of masses of approximately 0.01 to 0.5 μg of lead per sample, without dilution (1).  
1.5 The ultrasonic extraction procedure has been validated for the determination of masses of approximately 20 to 100 μg of lead per sample, for laboratory-generated lead fume air filter samples  (2).  
1.6 The concentration range for lead in air for which this procedure is applicable is determined in part by the sampling procedure selected by the user (see Section 9).  
1.7 Anions that form precipitates with lead may interfere, but this potential interference is overcome by the addition of the disodium salt of ethylenediamine tetraacetic acid (EDTA) when necessary.  
1.8 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.  
1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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