SIGNIFICANCE AND USE
4.1 The dissipation factor of natural muscovite mica, as determined by this test method, is of practical importance as a measure of the electrical energy lost as heat in the mica serving as the dielectric substance of capacitors, or in other applications in which the electric field is applied perpendicular to the plane of cleavage. The dissipation factor is particularly important in applications using mica at radio frequencies and in some less extensive audio frequency applications. This test method is suitable for specification acceptance and dielectric-loss control tests (see the Significance and Use of Test Methods D150).  
4.2 Relative Permittivity (Dielectric Constant)—The permittivity of natural muscovite mica is a measure of its relative ability to store electrostatic energy. Since the relative permittivity perpendicular to the cleavage plane is fairly uniform, regardless of origin, its practical significance is mainly for identification purposes, special uses, research, and design. If a loss index is desired, the value of the permittivity must be known (see the Significance and Use of Test Methods D150).
SCOPE
1.1 This test method covers the determination of the dissipation factor and the relative permittivity of natural block mica having thicknesses between 0.007 and 0.030 in. (0.18 and 0.77 mm) and mica films or capacitor splits between 0.0008 and 0.004 in. (0.02 and 0.10 mm) in thickness.  
1.2 The values stated in inch-pound units are to be regarded as the standard. The values in parentheses are for information purposes only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. A specific warning statement is given in Section 7 and 6.1.1.  
Note 1: Procedures for the measurement of dissipation factor and permittivity are given in IEC Publication 60371-2, but the details of the procedure are somewhat different from those specified in this test method.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
5.1 Fluorspar is used as a flux in the steelmaking and glass industries, and in the manufacture of HF.  
5.2 This test method is intended to be used for compliance with compositional specifications for calcium fluoride content. It is assumed that all who use these procedures will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices must be followed such as those described in Guide E882.
SCOPE
1.1 This test method covers the determination of calcium fluoride in acid-grade fluorspar and other types of fluorspar that can be rendered soluble by the procedure described in the test method.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This test method has been evaluated in accordance with Practice E1601 and Guide E1763. Unless otherwise noted in the precision and bias section, the lower limit in the scope of each method specifies the lowest analyte content that may be analyzed with acceptable error (defined as a nominal 5 % risk of obtaining a 50 % or larger relative difference in results on the same test sample in two laboratories).  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
5.1 This guide is intended as a means for obtaining an extract from mine rock and soil samples to measure cyanide content in the aqueous portion of the sample on a dry weight basis. Cyanide is analyzed in mine rock and soil extracts for measurement of cyanide concentration; however, improper sample collection and extraction can result in significant positive or negative bias.  
5.2 This guide is designed to mobilize aqueous cyanides present in the solids, so that the resulting extract can be used to assess leachate that could potentially be produced from mine rock or soil.  
5.3 This guide is not intended to simulate actual site leaching conditions.  
5.4 This guide produces extracts that are amenable to the determination of trace cyanides. When trace cyanides are being determined, it is especially important that precautions be taken in sample preservation, storage, and handling to avoid possible contamination of the extracts.  
5.5 This guide uses a comparative test method and is intended for use as a routine method for monitoring mine rock and soils. It is assumed that all who use this guide will be trained analysts capable of performing it skillfully and safely. It is expected that work will be performed in a properly equipped laboratory applying appropriate quality control practices such as those described in Guide D3856.  
5.6 This guide identifies proper methods for obtaining mine rock and soil samples for the specific purpose of measuring cyanide concentrations.
SCOPE
1.1 This guide is applicable for the collection, extraction, and preservation of extracts from mine rock and soil samples for the analysis of cyanide in the extracts. Responsibilities of field sampling personnel and the laboratory are indicated.  
1.2 The sampling, preservation, and extraction procedures described in this guide are recommended for the analysis of total cyanide, available cyanide, weak acid dissociable cyanide, and free cyanide by Test Methods D2036, D4282, D4374, D6888, D6994, D7237, and D7284. The information supplied in this guide can also be applied to other analytical methods for cyanide, for example, US EPA Method 335.4.  
1.3 The procedure options methods appear in the following order:    
Procedure Option  
Sections  
Option A
Laboratory Processing of Field
Preserved Samples  
11 and 12  
Option B
Laboratory Processing of Moist
Field Samples  
13 and 14  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ABSTRACT
This specification covers the determination of muscovite mica splittings of standard commercial grades and specifies the maximum allowable physical defects for each grade. It is applicable to commercially available natural muscovite mica splittings regardless of the basic color of the mica or its source. This specification covers thirteen grades of mica splittings based on size and form classification. Mica splittings shall meet the specified physical property requirements such as size, thickness, defects, and absence of any foreign matter. Where specified, the visual quality shall conform to the description of the visual category specified such as V-1, V-2, V-3, V-4, V-5, V-5.1, V-6, V-7, V-8, V-9, V-10, V-11, and V-12. The method of sampling of mica splittings in bookform and loose with powder form are specified and method of calculation of defect percentage is given.
SCOPE
1.1 This classification covers the determination of muscovite mica splittings of standard commercial grades and specifies the maximum allowable physical defects for each grade. It is applicable to commercially available natural muscovite mica splittings regardless of the basic color of the mica or its source.  
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard is very similar to ISO 6386. It is expected that materials would be classified identically using the criteria of either standard. The grades shown under “ASTM Grade No.” in Table 1 and Table 2 are shown under “Old Grade No.” in ISO 6386-1981.    
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
5.1 This test method is intended as a referee method for compliance with compositional specifications for impurity content. It is assumed that all who use this procedure will be trained analysts capable of performing common laboratory practices skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Follow appropriate quality control practices such as those described in Guide E882.
SCOPE
1.1 This test method covers the determination of silica in fluorspar from 0.5 % to 10 % by mass.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
5.1 This procedure is suitable for manufacturing control and verifying that the product meets specifications. It provides rapid, multi-element determinations with sufficient accuracy to ensure product quality and minimize production delays. The analytical performance data included may be used as a benchmark to determine whether similar X-ray spectrometers provide equivalent precision and accuracy, or whether the performance of a particular X-ray spectrometer has changed.
SCOPE
1.1 This test method covers the X-ray emission spectrometric analysis of limestone, quicklime, hydrated lime, and hydraulic lime using wavelength dispersive instruments.  
1.2 The values stated in SI units are to be regarded as the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  Specific precautionary statements are given in Section 10.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
3.1 These test methods may be used to confirm the stated SiO2, CaO, and MgO content of magnesium silicate for quality control.
SCOPE
1.1 These test methods cover the analysis of magnesium silicate pigment.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
3.1 This classification system is intended to encourage uniformity in reporting properties; to provide a common language for communications between suppliers and consumers; to guide engineers and designers in the test methods commonly used for commercially available materials; and to be versatile enough to cover new materials and test methods as they are introduced.  
3.2 This system is based on the principle that nonmetallic gasket materials can be described in terms of specific physical and mechanical properties. This enables the user, or producer, to characterize a nonmetallic gasket based on properties that are important for the application.
SCOPE
1.1 This classification system2 provides a means for specifying or describing pertinent properties of commercial nonmetallic gasket materials. Materials composed of asbestos, cork, cellulose, and other organic or inorganic materials in combination with various binders or impregnants are included. Materials normally classified as rubber compounds are not included, since they are covered in Classification D2000. Gasket coatings are not covered, since details thereof are intended to be given on engineering drawings or in separate specifications. Facing materials for laminate composite gasket materials (LCGM) are included in Classification System F104. Assembled LCGMs are covered in Classification F868.  
1.2 Since all of the properties that contribute to gasket performance are not included, use of the classification system as a basis for selecting materials is limited.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
5.1 This practice is designed to compare related materials under controlled conditions and their ability to maintain a minimum amount of thermal conductance. Test results should be correlated with field results in order to predict heat transfer properties in particular applications.  
5.2 This practice may be used as a routine test when agreed upon by the user and the producer.
SCOPE
1.1 This practice covers a means of measuring the amount of heat transfer quantitatively through a material or system.  
1.2 This practice is similar to the Heat Flow Meter System of Test Method C518, but modified to accommodate small test samples of higher thermal conductance.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
4.1 These test methods are designed to compare gasket materials under controlled conditions and to provide a precise measure of leakage rate.  
4.2 These test methods are suitable for measuring leakage rates as high as 6 L/h and as low as 0.3 mL/h. In many cases, “zero” leakage may not be attainable.  
4.3 These test methods evaluate leakage rates after time periods that are typically 5 to 30 min under load. Holding a gasket material under load for extended time periods may give different results.  
4.4 If the fluid being used in the test causes changes, such as swelling, in the gasket material, then unpredictable results may be obtained.
SCOPE
1.1 These test methods provide a means of evaluating the sealing properties of sheet and solid form-in-place gasket materials at room temperature. Test Method A is restricted to liquid leakage measurements, whereas Test Method B may be used for both liquid and gas leakage measurements.  
1.2 These test methods are suitable for evaluating the sealing characteristics of a gasket material under different compressive flange loads. The test method may be used as an acceptance test when the producer and user have agreed to specific test conditions for the following parameters: test medium, internal pressure on medium, and flange load on gasket specimens.  
1.3 These test methods use a small-diameter narrow-width gasket as the test specimen under relatively low gasket loads and relatively low pressures. Test Method F2378 is another sealability test method that uses a larger gasket specimen and higher internal pressures and flange loads.  
1.4 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (For specific hazard or warning statements, or both, see 5.2.11, Section 6, 6.3, 8.2.4, 11.3.2, and 11.4.2.)  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
4.1 This test method provides terms such as megapascals or pounds-force per square inch of gasket surface for expressing the extent of adhesion applicable to all materials within the scope of Classification System F104. Under certain conditions, adhesion develops when gasket materials are confined in a compressed state between metal flanges. Adhesion is important as an index of ease of removal of a gasket material. Since other variables may enter into the performance in an application, the results obtained should be correlated with field results. A typical set of conditions is described in this test method. This test method may be used as an acceptance test when agreed upon between the user and the producer.
SCOPE
1.1 This test method provides a means of determining the degree to which gasket materials under compressive load adhere to metal surfaces. The test conditions described are indicative of those frequently encountered in gasket applications. Test conditions may also be modified in accordance with the needs of specific applications as agreed upon between the user and the producer. The maximum temperature recommended for this test method is 205°C (400°F).  
1.2 The values stated in SI units are to be regarded as standard. The values in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
4.1 These test methods provide a standardized procedure to measure the effect of immersion in specified fluids under definite conditions of time and temperature. The results of these test methods are not intended to give any direct correlation with service conditions in view of the wide variations in temperature and special uses encountered in gasket applications. The specific test fluids and test conditions outlined were selected as typical for purposes of comparing different materials and can be used as a routine test when agreed upon between the purchaser and the manufacturer.
SCOPE
1.1 These test methods cover the determination of the effect on physical properties of nonmetallic gasketing materials after immersion in test fluids. The types of materials covered are Type 1, Type 2, Type 3, and Type 7 as described in Classification F104. These test methods are not applicable to the testing of vulcanized rubber, a procedure that is described in Test Method D471. It is designed for testing specimens cut from gasketing materials or from finished articles of commerce. These test methods may also be used as a pre-treatment for Multi-Layer Steel, MLS, or Metal Layer Gasket materials adhesion testing per Test Methods D3359. The pre-treatment of MLS or Metal Layer Gasket materials pertains only as a pre-cursor to the adhesion test. Other physical property tests described in this standard are not applicable to MLS or Metal Layer Gasket materials.  
1.2 The values stated in SI units are to be regarded as the standard. The inch-pound units in parentheses are for information only.  
1.3 Refer to the current Material Safety Data Sheet (MSDS) and any precautionary labeling provided by the supplier of any materials referred to in these test methods.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
5.1 This test method is designed to measure the chemical cure of the binder used in the manufacture of cork compositions. The results of this test method can be used only as a guide for its intended service in elevated temperature and environmental conditions.
SCOPE
1.1 This test method covers three procedures for determination of the binder durability of cork-containing materials.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
4.1 The properties included in this standard are those required to control the visual quality, usable area, thickness, hardness, and stiffness.
SCOPE
1.1 This classification covers the determination of commercially available natural muscovite block mica and is intended to be independent of the basic color of the mica or its source.  
1.2 Muscovite mica is characterized by having an optical axial angle between 50 and 75° (see Appendix X1); and has a weight loss when heated for 5 min at 600°C not exceeding 0.2 % (based on the weight after drying at 120°C).  
1.3 The visual system of classifying the quality of natural muscovite mica covered by this specification is based upon relative amounts of visible foreign inclusions such as air bubbles, stains, and spots in combination with relative amounts and types of waviness, as well as other physical properties. In this system, a perfectly clear, transparent, flat specimen of mica is the visual standard of perfection. Increasing amounts of visual defects lower the visual quality, and a total of 13 levels of visual quality are covered by this standard. This method of classification, generally known as the Bengal India System, is purely qualitative and is entirely dependent on personal opinion and judgment.  
1.4 The standards for visual quality classification that are covered in this classification are the best commercially available concept of the various qualities and their relative positions. Variations in the methods of using and applying these standards from those herein defined are specified by the purchaser, or defined by agreement between the supplier and the purchaser.  
1.5 Standard size classifications are defined, based upon available usable rectangular areas and the minimum dimensions of the rectangles that the pieces will yield. Precautions to be taken in making thickness measurements are also described.  
1.6 This standard covers the following two definite forms of commercial preparation:  
1.6.1 Form 1—Full-trimmed natural block mica, 0.007 in. (0.178 mm) minimum thickness.  
1.6.2 Form 2—Partially-trimmed natural block mica, 0.007 in. minimum thickness.  
1.7 The basic color of mica, such as white, ruby, light green, dark green, brownish green, and rum, as well as other colors, and the method of controlling the color and other problems associated with the basic color, are not a part of this classification.  
1.8 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.9 Section 5 is technically identical to procedures specified in ISO 67-1981.  
1.10 Section 6 differs somewhat in procedure from ISO 5972-1978, but data obtained by either is expected to be identical.  
1.11 Section 7 is technically identical to procedures specified in ISO 2185-1972.  
1.12 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
4.1 These test methods are designed to compare related materials under controlled conditions and their ability to maintain a given compressive stress as a function of time. A portion of the torque loss on the bolted flange is a result of creep relaxation. Torque loss can also be caused by elongation of the bolts, distortion of the flanges, and vibration; therefore, the results obtained should be correlated with field results. These test methods may be used as a routine test when agreed upon between the consumer and the producer.
Note 1: Test Method B was developed using asbestos gasket materials and at issuance substantiating data were not available for other gasket materials.
SCOPE
1.1 These test methods provide a means of measuring the amount of creep relaxation of a gasket material at a predetermined time after a compressive stress has been applied.  
1.1.1 Test Method A—Creep relaxation measured by means of a calibrated strain gauge on a bolt.  
1.1.2 Test Method B—Creep relaxation measured by means of a calibrated bolt with dial indicator.  
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
4.1 These test methods are described in order to standardize procedures for determining the tensile strength of nonmetallic gasket materials. The measurement of this property characterizes various classes and grades of materials of a given type and in so doing, it will give the manufacturer a measurement of the quality of his product. It also will aid the purchaser of the gasketing materials to be able to determine whether the gasket material that he has approved for a given application is being manufactured in acceptable quality.  
4.2 The measurement of this property should not be misconstrued as to give the purchaser of the gasket material an indication of the performance of that material in application.  
4.3 The property may be useful in establishing material specifications.  
4.4 Various procedures are given for the different types of materials, and in order to compare the results from one laboratory to another, it is imperative that the applicable procedure be selected.  
4.5 Various types of tension-testing apparatus are allowed to be used. These types of equipment can produce different indicated results. Laboratories having different equipment may have to establish correlations between each other; otherwise, misinterpretation of the test data could result.
SCOPE
1.1 These test methods cover the determination of tensile strength of certain nonmetallic gasketing materials at room temperature. The types of materials covered are those containing asbestos and other inorganic fibers (Type 1), cork (Type 2), cellulose or other organic fiber (Type 3), and flexible graphite (Type 5) as described in Classification F104. These test methods are not applicable to the testing of vulcanized rubber, a method for which is described in Test Methods D412 nor for rubber O-rings, a method for which is described in Test Methods D1414.  
1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ISO 10058-2:2008 specifies traditional (“wet process”) methods for the chemical analysis of magnesite and dolomite refractory products and raw materials.

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ISO 10058-1:2008 specifies apparatus, reagents, dissolution and gravimetric silica analysis for the chemical analysis of magnesite and dolomite refractory products and raw materials.

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ISO 10058-3:2008 specifies atomic absorption spectrometry (AAS) and inductively coupled plasma atomic emission spectrometry (ICP-AES) methods for the chemical analysis of magnesite and dolomite refractory products and raw materials.

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ISO 10058-2:2008 specifies traditional (“wet process”) methods for the chemical analysis of magnesite and dolomite refractory products and raw materials.

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ISO 10058-1:2008 specifies apparatus, reagents, dissolution and gravimetric silica analysis for the chemical analysis of magnesite and dolomite refractory products and raw materials.

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ISO 10058-3:2008 specifies atomic absorption spectrometry (AAS) and inductively coupled plasma atomic emission spectrometry (ICP-AES) methods for the chemical analysis of magnesite and dolomite refractory products and raw materials.

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ISO 10058-2:2008 specifies traditional (“wet process”) methods for the chemical analysis of magnesite and dolomite refractory products and raw materials.

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ISO 10058-1:2008 specifies apparatus, reagents, dissolution and gravimetric silica analysis for the chemical analysis of magnesite and dolomite refractory products and raw materials.

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ISO 10058-3:2008 specifies atomic absorption spectrometry (AAS) and inductively coupled plasma atomic emission spectrometry (ICP-AES) methods for the chemical analysis of magnesite and dolomite refractory products and raw materials.

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Contains minor amendments and additions only.

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Describes a method for the determination of the precision of fluorspar sampling and sample preparation carried out by the methods specified in ISO 8868.

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Sampling and sample preparation of similar types of fluorspar is assumed to be carried out in accordance with the methods specified in ISO 8868. The experimental methods given are based on comparing the results obtained from the method to be checked with the results of a reference method which, for all practical purposes, is considered to produce practically unbiased results.

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Specifies experimental methods for the evaluation of quality variation of fluorspar lots from the same source. These methods are to be used in conjunction with the sampling procedures specified in ISO 8868.

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The principle of the method specified is to decompose a test portion by a mixture of nitric, hydrofluoric and perchloric acids, dissolving the salts in hydrochloric acid after evaporation to fumes of sulfuric acid, extracting the antimony from a dilute hydrochloric acid solution of the decomposed test portion into a solution of tri-n-octylphosphine oxide in 4-methyl-2-pentanone, aspirating the extract into the air/acetylene flame of an atomic absorption spectrometer, and measuring the absorbance at 217,6 nm. Applies to products having an antimony content equal to or greater than 0,001 % (m/m).

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The principle of the method specified is to decompose a test portion by a mixture of nitric, hydrofluoric and perchloric acids, dissolving the salts in hydrochloric acid after evaporation to dryness, extracting the lead from a dilute hydrochloric acid solution of the decomposed test portion into a solution of tri-n-octylphosphine oxide in 4-methyl-2-pentanone, aspirating the extract into the air/acetylene flame of an atomic absorption spectrometer, and measuring the absorbance at 283,3 nm. Applies to products having lead contents in the range 0,0006 % (m/m) to 0,01 % (m/m).

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The principle of the method specified is to decompose a test portion by alkaline fusion and subsequent dissolution of the melt in excess of nitric acid, precipitation of iron(III) phosphate with ammonia solution, dissolution of the precipitate in nitric acid, formation of the molybdophosphate complex and extraction, followed by selective reduction of the complex to molybdenum blue, spectrometric measurement of the absorbance of the coloured complex at the wavelength of maximum absorption (about 710 nm). Applies to products having total phosphorus contents, expressed as PO4^3-, in the range 0,01 % (m/m) to 1,0 % (m/m).

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The method specified is based on alkaline fusion of a test portion with a mixture of sodium carbonate and boric acid, dissolution of the melt in excess hydrochloric acid, reduction of the iron(III) with hydroxylammonium chloride, formation of the iron(II)-1,10-phenanthroline complex in a buffered medium (pH between 3 and 5), spectrometric measurement of the absorbance of the coloured complex at a wavelength of about 510 nm, corresponding to the absorption maximum. Applies to products having iron contents, expressed as Fe2O3, in the range 0,1 % (m/m) to 2,0 % (m/m).

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The method specified is based on dissolution of a test portion by fusion with a mixture of sodium carbonate, boric acid and sodium nitrate and subsequent acidification with nitric acid, formation of the molybdophosphate complex and extraction with a mixture of ethyl acetate and butyl acetate, followed by selective reduction of the complex to molybdenum blue by means of tin(II) chloride added to the organic phase, spectrometric measurement of the absorbance of the coloured complex at the wavelength of maximum absorption (about 710 nm). Applies to products having total phosphorus contents, expressed as PO4^3-, in the range 0,01 % (m/m) to 1,0 % (m/m).

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The principle of the method specified is to decompose a test portion by alkaline fusion with sodium carbonate and subsequent acidification with hydrochloric acid in the presence of boric acid to complex fluoride, selective reduction to the blue molybdosilicic acid complex, spectrometric measurement of the absorbance of the coloured complex at a wavelength corresponding to the absorption maximum of approximately 650 nm. Applies to products having silica contents, expressed as SiO2, in the range 0,2 % (m/m) to 30 % (m/m).

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The method specified is based on decomposition of a test portion by fusion with sodium carbonate and subsequent acidification with hydrochloric acid in the presence of boric acid to complex fluoride, formation of the molybdosilicic acid complex and selective reduction to the blue molybdosilicic acid complex with addition of tartaric acid to prevent interference from phosphate, spectrometric measurement of the absorbance of the coloured complex at the wavelength of maximum absorption (about 795 nm). Applies to products having silica contents, expressed as SiO2, in the range 0,05 % (m/m) to 4,0 % (m/m).

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The principle of the method is treatment of a test portion with a mixture of dilute hydrochloric acid and an organic solvent, removal of the insoluble fluorspar by filtration under vacuum, separation of the organic phase containing the flotation agent, evaporation of the solvent and weighing of the residue. Applies to materials which have been subjected to flotation process and which have flotation agent contents equal to or greater than 0,002 % (m/m) of the dried material.

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The principle of the method specified is treatment of a test portion with hydrochloric acid solution, absorption of the evolved carbon dioxide in barium hydroxide solution, neutralization of excess alkali with hydrochloric acid solution, addition of an exactly measured excess of a standard volumetric hydrochloric acid solution to dissolve the precipitated barium carbonate and back-titration with a standard volumetric sodium hydroxide solution using methyl orange as indicator. The method is applicable to products having carbonate contents equal to or greater than 0,04 % (m/m).

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The principle of the method specified is digestion of a test portion in a sealed apparatus in a mixture of hydrochloric acid, tin(II) chloride and boric acid solutions, absorption of the liberated hydrogen sulfide, entrained in a stream of oxygen-free argon or nitrogen, in zinc acetate solution and iodometric determination of the zinc sulfide formed. The method is applicable to products having a sulfide content equal to or greater than 0,001 % (m/m). It is not applicable, if presence of polysulfides is suspected.

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Applicable to products having Mn-contents in the range 0,006 % to 0,4 %. Decomposition of the test portion with nitric and perchloric acids. After dilution follows oxidation of manganese to permanganate with sodium metaperiodate. Spectrometric measurement at 545 nm.

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The principle of the method is drying of a test portion in air at 105 °C to constant mass. Determines the mean value of the moisture content.

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The method is based on drying a test portion at 105 °C and determination of the loss in mass, which corresponds to the content of water and other components volatile at that temperature. Applies to fluorspars, which may be dried material containing not less than 0,02 % (m/m) of components volatile at 105 °C, or filter cake.

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The method is based on evaporation to dryness of a test portion in the presence of hydrofluoric acid and concentrated sulfuric acid, extraction of the soluble salts from the mixture, filtration, drying and weighing of the residual barium sulfate. Applies to products having barium sulfate contents equal to or greater than 0,1 % (m/m).

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Specifies methods for determining silica, alumina, titania, iron oxide and oxides of manganese, chromium, calcium, magnesium, sodium, potassium and lithium. It also specifies methods for determining the loss of ignition of magnesite and dolomite, and of refractories based on these raw materials. Annex A describes a method for determining the boron content of magnesites only.

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Specifies the principle, the reagents, the apparatus, the preparation of the test sample, the test procedure, the expression of results and the test report.

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Specifies a test method. Describes the principle, the reagents, the apparatus, the test sample, the test procedure, the expression of results, and the contents of the test report.

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The method given is applicable to fluorspars having sulfur contents in the range 0,01 % (m/m) to 1,0 % (m/m). Describes in detail: principle, reagents and materials, apparatus, test sample, procedure, expression of results, and test report. Annex A gives values of total sulfur content of metallurgical grade fluorspars obtained in interlaboratory trials using the iodometric method after combustion specified in this standard.

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