Test on gases evolved during combustion of materials from cables - Part 1: Determination of the halogen acid gas content

IEC 60754-1:2011 specifies the apparatus and procedure for the determination of the amount of halogen acid gas, other than hydrofluoric acid, evolved during the combustion of compounds based on halogenated polymers and compounds containing halogenated additives taken from electric or optical fibre cable constructions. The method specified in this standard is intended for the testing of individual components used in a cable construction. The use of this method will enable the verification of requirements which are stated in the appropriate cable specification for individual components of a cable construction. The significant technical changes with respect to the previous edition are as follows: - improved definition of safety requirements relating to capture of gases and use of reagents; - introduction of guidance on preparation of test specimens for a more even combustion; - improvements to the procedure for establishing the heating regime; - improved expression of tolerances and precision; - definition of the procedure for the blank test; - introduction of an informative annex giving details of a methodology for the determination of the halogen acid gas content of a sample representative of a cable construction. IEC 60754-1:2011 Has the status of a group safety publication in accordance with IEC Guide 104.

Prüfung der bei der Verbrennung der Werkstoffe von Kabeln und isolierten Leitungen entstehenden Gase - Teil 1: Bestimmung des Gehaltes an Halogenwasserstoffsäure

Essai sur les gaz émis lors de la combustion des matériaux prélevés sur câbles - Partie 1: Détermination de la quantité de gaz acide halogéné

La CEI 60754-1:2011 décrit l'appareillage et la procédure d'essai pour la détermination de la quantité de gaz acide halogéné, autre que l'acide fluorhydrique, émis au cours de la combustion de mélanges à base de polymères halogénés et de mélanges contenant des additifs halogénés prélevés sur un câble électrique ou à fibre optique. La présente méthode décrite dans cette norme est destinée à être utilisée pour l'analyse des composants individuels utilisés dans la construction d'un câble. L'emploi de cette méthode d'essai permettra de vérifier les exigences qui sont établies dans la spécification du câble pour les composants individuels du câble. Les modifications techniques importantes par rapport aux publications antérieures sont les suivantes: - amélioration définition des exigences de sécurité relatives au piégeage des gaz et à l'utilisation des réactifs; - introduction de recommandations pour la préparation des éprouvettes d'essai pour une meilleure combustion; - améliorations du mode opératoire pour établir le régime de chauffage; - amélioration de l'expression des tolérances et précisions; - définition de la procédure d'un essai à blanc; - introduction d'une annexe informative donnant des détails sur la méthodologie pour la détermination de la quantité de gaz acides halogénés contenus dans un échantillon représentatif de la construction du câble. Elle a le statut d'une publication groupée de sécurité conformément au Guide CEI 104.

Ugotavljanje nastajanja plinov pri gorenju kabelskih materialov - 1. del: Ugotavljanje količine plina halogenske kisline (IEC 60754-1:2011)

Ta del standarda IEC 60754 določa napravo in postopek za ugotavljanje količine plina halogenske kisline, ki ni fluorovodikova kislina, nastale pri gorenju spojin, ki temeljijo na halogeniranih polimerih, in gorenju spojin, ki vsebujejo halogenirane dodatke iz konstrukcij električnih ali optičnih kablov. OPOMBA 1: s to preskusno metodo ni mogoče določiti fluorovodikove kisline. Primerno metodo je mogoče poiskati v standardu IEC 60684-2. OPOMBA 2: ta preskusna metoda se lahko uporabi za preskušanje materialov, ki so namenjeni uporabi pri izdelavi kablov, a deklaracija zmogljivosti kabla naj ne bi temeljila na takem preskusu. OPOMBA 3: ustrezni standard za kable navaja, katere komponente kabla je treba testirati. OPOMBA 4: za namen tega standarda pojem »električni kabel« zajema vse izolirane kovinske vodnike, ki se uporabljajo za prenos energije ali signalov. Metoda, določena v tem standardu, je namenjena preskušanju posameznih komponent, ki se uporabljajo pri izdelavi kablov. Uporaba te metode bo omogočila preverjanje zahtev, ki so navedene v ustrezni kabelski specifikaciji za posamezne komponente kabelske zgradbe. OPOMBA 5: po dogovoru med proizvajalcem in kupcem se metodologija, podana v tem standardu, lahko uporablja za testiranje kombinacij materialov, ki predstavljajo zgradbo kabla, vendar deklaracija o zmogljivosti kabla k temu standardu naj ne bi temeljila na takem preskusu. Informacije o takšnem načinu so podane v dodatku A. Zaradi natančnosti ta metoda ni priporočljiva za poročanje o vrednosti halogenske kisline z manj kot 5 mg/g odvzetega vzorca.

General Information

Status
Published
Publication Date
17-Apr-2014
Technical Committee
Drafting Committee
Current Stage
6060 - Document made available - Publishing
Start Date
18-Apr-2014
Completion Date
18-Apr-2014

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SLOVENSKI STANDARD
01-junij-2014
1DGRPHãþD
SIST EN 50267-1:1999
SIST EN 50267-2-1:1999
SIST EN 50267-2-2:1999
SIST EN 50267-2-3:1999
8JRWDYOMDQMHQDVWDMDQMDSOLQRYSULJRUHQMXNDEHOVNLKPDWHULDORYGHO
8JRWDYOMDQMHNROLþLQHSOLQDKDORJHQVNHNLVOLQH ,(&
Test on gases evolved during combustion of materials from cables - Part 1:
Determination of the halogen acid gas content
Prüfung der bei der Verbrennung der Werkstoffe von Kabeln und isolierten Leitungen
entstehenden Gase -- Teil 1: Bestimmung des Gehaltes an Halogenwasserstoffsäure
Essai sur les gaz émis lors de la combustion des matériaux prélevés sur câbles -- Partie
1: Détermination de la quantité de gaz acide halogéné
Ta slovenski standard je istoveten z: EN 60754-1:2014
ICS:
13.220.40 Sposobnost vžiga in Ignitability and burning
obnašanje materialov in behaviour of materials and
proizvodov pri gorenju products
29.060.20 Kabli Cables
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EUROPEAN STANDARD
EN 60754-1
NORME EUROPÉENNE
April 2014
EUROPÄISCHE NORM
ICS 13.220.40; 29.020; 29.060.20 Supersedes EN 50267-1:1998 (partially), EN 50267-2-1:1998 (partially), EN 50267-2-2:1998
(partially), EN 50267-2-3:1998 (partially)

English version
Test on gases evolved during combustion of materials from cables -
Part 1: Determination of the halogen acid gas content
(IEC 60754-1:2011 + corrigendum Nov. 2013)

Essai sur les gaz émis lors de la Prüfung der bei der Verbrennung der
combustion des matériaux prélevés Werkstoffe von Kabeln und isolierten
sur câbles - Leitungen entstehenden Gase -
Partie 1: Détermination de la quantité Teil 1: Bestimmung des Gehaltes an
de gaz acide halogéné Halogenwasserstoffsäure
(CEI 60754-1:2011 + corrigendum Nov. (IEC 60754-1:2011 + Corrigendum Nov.
2013) 2013)
This European Standard was approved by CENELEC on 2014-01-27. CENELEC members are bound to comply
with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard
the status of a national standard without any alteration.

Up-to-date lists and bibliographical references concerning such national standards may be obtained on
application to the CEN-CENELEC Management Centre or to any CENELEC member.

This European Standard exists in three official versions (English, French, German). A version in any other
language made by translation under the responsibility of a CENELEC member into its own language and notified
to the CEN-CENELEC Management Centre has the same status as the official versions.

CENELEC members are the national electrotechnical committees of Austria, Belgium, Bulgaria, Croatia, Cyprus,
the Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany,
Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, the Netherlands, Norway, Poland,
Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom.

CENELEC
European Committee for Electrotechnical Standardization
Comité Européen de Normalisation Electrotechnique
Europäisches Komitee für Elektrotechnische Normung

CEN-CENELEC Management Centre: Avenue Marnix 17, B - 1000 Brussels

© 2014 CENELEC - All rights of exploitation in any form and by any means reserved worldwide for CENELEC members.
Ref. No. EN 60754-1:2014 E
Foreword
This document (EN 60754-1:2014) consists of the text of IEC 60754-1:2011 +
corrigendum November 2013, prepared by IEC/TC 20 "Electric cables".

The following dates are fixed:
(dop) 2015-01-27
• latest date by which the document has to be
implemented at national level by
publication of an identical national
standard or by endorsement
(dow) 2017-01-27
• latest date by which the national
standards conflicting with the
document have to be withdrawn
This document supersedes EN 50267-1:1998 (PART), EN 50267-2-1:1998 (PART),
EN 50267-2-2:1998 (PART) and EN 50267-2-3:1998 (PART).

Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CENELEC [and/or CEN] shall not be held responsible for identifying any or all such
patent rights.
This standard covers the Principle Elements of the Safety Objectives for Electrical Equipment
Designed for Use within Certain Voltage Limits (LVD - 2006/95/EC).

Endorsement notice
The text of the International Standard IEC 60754-1:2011 + corrigendum November 2013 was
approved by CENELEC as a European Standard without any modification.
In the official version, for Bibliography, the following note has to be added for the standard indicated :

IEC 60684-2 NOTE Harmonized as EN 60684-2.

- 3 - EN 60754-1:2014
Annex ZA
(normative)
Normative references to international publications
with their corresponding European publications

The following documents, in whole or in part, are normatively referenced in this document and are
indispensable for its application. For dated references, only the edition cited applies. For undated
references, the latest edition of the referenced document (including any amendments) applies.

NOTE  When an international publication has been modified by common modifications, indicated by (mod), the relevant EN/HD
applies.
Publication Year Title EN/HD Year

ISO 385 - Laboratory glassware - Burettes EN ISO 385 -

ISO 1042 - Laboratory glassware - One-mark EN ISO 1042 -
volumetric flasks
ISO 3696 - Water for analytical laboratory use - EN ISO 3696 -
Specification and test methods

IEC 60754-1 ®
Edition 3.0 2011-11
INTERNATIONAL
STANDARD
NORME
INTERNATIONALE
GROUP SAFETY PUBLICATION
PUBLICATION GROUPÉE DE SÉCURITÉ

Test on gases evolved during combustion of materials from cables –
Part 1: Determination of the halogen acid gas content

Essai sur les gaz émis lors de la combustion des matériaux prélevés sur câbles
– Partie 1: Détermination de la quantité de gaz acide halogéné

INTERNATIONAL
ELECTROTECHNICAL
COMMISSION
COMMISSION
ELECTROTECHNIQUE
PRICE CODE
INTERNATIONALE
CODE PRIX S
ICS 13.220.40; 29.020; 29.060.20 ISBN 978-2-88912-715-3

– 2 – 60754-1 © IEC:2011
CONTENTS
FOREWORD . 4
INTRODUCTION . 6
1 Scope . 7
2 Normative references . 7
3 Terms and definitions . 7
4 Test method principle . 8
5 Test apparatus . 8
5.1 General . 8
5.2 Tube furnace . 8
5.3 Quartz glass tube . 8
5.4 Combustion boats . 8
5.5 Bubbling devices for gases . 9
5.6 Air supply system . 9
5.7 Analytical balance . 10
5.8 Laboratory glassware . 10
5.9 Reagents . 10
6 Test specimen . 10
6.1 General . 10
6.2 Conditioning of specimen . 10
6.3 Mass of specimen . 11
7 Test procedure . 11
7.1 General . 11
7.2 Test apparatus and arrangement . 11
7.3 Heating procedure . 11
7.3.1 Determination of heating regime . 11
7.3.2 Test specimen heating procedure . 11
7.4 Washing procedure . 12
7.5 Determination of halogen acid content . 12
7.5.1 Blank test . 12
7.5.2 Material test . 12
7.5.3 Halogen acid content calculation . 13
8 Evaluation of the test results . 13
9 Performance requirement . 13
10 Test report. 13
Annex A (informative) Determination of the halogen acid gas content of a sample
representative of a cable construction . 20
Bibliography . 21

Figure 1 – Device for inserting combustion boat and test specimen . 15
Figure 2 – Example of a gas washing bottle . 16
Figure 3 – Test apparatus: method 1 – Use of synthetic or compressed air from a
bottle . 17
Figure 4 – Test apparatus: method 2 – Use of laboratory compressed air supply . 18

60754-1 © IEC:2011 – 3 –
Figure 5 – Test apparatus: method 3 – Use of ambient air sucked by means of a
suction pump . 19

– 4 – 60754-1 © IEC:2011
INTERNATIONAL ELECTROTECHNICAL COMMISSION
____________
TEST ON GASES EVOLVED DURING
COMBUSTION OF MATERIALS FROM CABLES –

Part 1: Determination of the halogen acid gas content

FOREWORD
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