ASTM D7013/D7013M-23
(Guide)Standard Guide for Calibration Facility Setup for Nuclear Surface Gauges
Standard Guide for Calibration Facility Setup for Nuclear Surface Gauges
SIGNIFICANCE AND USE
5.1 To establish a proper calibration area for nuclear surface gauges.
5.2 To reduce the chance of improper calibration.
Note 1: The quality of the results produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of practice D3740 are generally considered capable of competent and objective testing/inspection/etc. Users of this standard are cautioned that compliance with practice D3740 does not in itself assure a means of evaluating some of those factors.
SCOPE
1.1 This guide outlines procedures for setup of a nuclear gauge calibration facility in either a shielded bay or an unshielded area—Guide A and Guide B, respectively.
1.2 This guide does not attempt to describe the calibration techniques or methods. It is assumed that this guide will be used by persons familiar with the operations of the gauge and in performing proper calibration, service and maintenance.
1.3 This guide does not attempt to address maintenance or service procedures related to the gauge.
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This guide offers an organized collection of information or a series of options and does not recommend a specific course of action. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this guide may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project’s many unique aspects. The word “Standard” in the title of this document has been approved through ASTM consensus process.
1.7 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in practice D6026.
1.7.1 The method used to specify how data are collected, calculated, or recorded in this standard is not directly related to the accuracy to which the data can be applied in the design or other uses, or both. How one applies the results obtained using this standard is beyond its scope.
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
General Information
- Status
- Published
- Publication Date
- 14-Feb-2023
- Technical Committee
- D18 - Soil and Rock
- Drafting Committee
- D18.08 - Special and Construction Control Tests
Relations
- Effective Date
- 01-Nov-2023
- Effective Date
- 01-Oct-2019
- Effective Date
- 01-Mar-2017
- Effective Date
- 01-Aug-2015
- Effective Date
- 01-Aug-2014
- Effective Date
- 01-May-2012
- Effective Date
- 01-Mar-2012
- Effective Date
- 01-Sep-2011
- Effective Date
- 01-Sep-2011
- Effective Date
- 01-May-2010
- Effective Date
- 01-Mar-2010
- Effective Date
- 01-Jan-2009
- Effective Date
- 01-Dec-2008
- Effective Date
- 01-Nov-2008
- Effective Date
- 01-Jun-2008
Overview
ASTM D7013/D7013M-23: Standard Guide for Calibration Facility Setup for Nuclear Surface Gauges provides a comprehensive framework for setting up calibration facilities used with nuclear surface gauges. These gauges are critical for measuring in-place density and moisture of soils and aggregates, primarily in civil engineering and construction. The guide outlines requirements for facility setup in both shielded bays and unshielded areas to ensure safe, accurate, and repeatable calibration results.
The standard aims to:
- Establish a proper calibration environment for nuclear gauges.
- Reduce the risk of improper calibration resulting from environmental or procedural factors.
- Maintain safety, health, and compliance with regulatory requirements.
Key Topics
1. Calibration Area Requirements
- Shielded Calibration Bay: Specifies construction and configuration details for shielded areas, including required wall materials, thickness, and distance from other gauges.
- Unshielded Area: Outlines minimum separation distances between gauges and storage to minimize background radiation effects during calibration.
2. Shielded Storage Bay
- Criteria for storage areas based on number of gauges in use.
- Recommendations for materials, wall thickness, and layout to control radiation background and prevent cross-interference during storage and calibration activities.
3. Wall Influence and Cross Talk Verification
- Procedures to assess and minimize influence from surrounding physical structures (walls) or from adjacent calibration bays.
- Methods for wall influence verification and between-bay cross talk to ensure accurate measurements.
4. Documentation and Reporting
- Specifies the minimum information to record during calibration, such as density and moisture counts, background readings, gauge serial numbers, and operator identification.
- Emphasizes consistent data collection in accordance with significant digit and rounding guidelines.
5. Safety and Compliance
- The user is responsible for safety, health practices, and complying with regulatory limitations.
- Additional local licensing rules may apply, including secure storage and warning signage.
Applications
Practical uses for ASTM D7013/D7013M-23 include:
- Civil and Geotechnical Engineering: Ensuring reliable calibration of nuclear moisture-density gauges for soil compaction and moisture testing on construction sites.
- Construction Quality Control: Enhancing accuracy and consistency of density and moisture measurements, impacting pavement, embankment, or foundation integrity.
- Materials Testing Laboratories: Guiding the setup of compliant, safe calibration facilities for multiple nuclear gauges.
- Regulatory Compliance: Assisting organizations in meeting industry standards and minimizing radiation safety risks.
Related Standards
Key standards referenced and associated with ASTM D7013/D7013M-23 include:
- ASTM D653 - Terminology Relating to Soil, Rock, and Contained Fluids
- ASTM D3740 - Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock for Engineering Design and Construction
- ASTM D6026 - Practice for Using Significant Digits and Data Records in Geotechnical Data
- ASTM D6938 - Test Methods for In-Place Density and Water Content of Soil and Soil-Aggregate by Nuclear Methods (Shallow Depth)
Summary
This standard guide provides essential criteria for the setup and operation of calibration facilities for nuclear surface gauges, emphasizing both accuracy and radiation safety. By following ASTM D7013/D7013M-23, agencies and laboratories ensure that nuclear gauge calibration is performed under controlled, compliant conditions, supporting the validity and repeatability of geotechnical testing results. Compliance with this guide supports adherence to best practices in construction quality assurance and laboratory management.
Keywords: calibration facility, nuclear surface gauge, shielded bay, unshielded area, radiation safety, moisture-density calibration, ASTM D7013/D7013M-23, geotechnical testing, quality assurance, construction standards.
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Frequently Asked Questions
ASTM D7013/D7013M-23 is a guide published by ASTM International. Its full title is "Standard Guide for Calibration Facility Setup for Nuclear Surface Gauges". This standard covers: SIGNIFICANCE AND USE 5.1 To establish a proper calibration area for nuclear surface gauges. 5.2 To reduce the chance of improper calibration. Note 1: The quality of the results produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of practice D3740 are generally considered capable of competent and objective testing/inspection/etc. Users of this standard are cautioned that compliance with practice D3740 does not in itself assure a means of evaluating some of those factors. SCOPE 1.1 This guide outlines procedures for setup of a nuclear gauge calibration facility in either a shielded bay or an unshielded area—Guide A and Guide B, respectively. 1.2 This guide does not attempt to describe the calibration techniques or methods. It is assumed that this guide will be used by persons familiar with the operations of the gauge and in performing proper calibration, service and maintenance. 1.3 This guide does not attempt to address maintenance or service procedures related to the gauge. 1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.6 This guide offers an organized collection of information or a series of options and does not recommend a specific course of action. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this guide may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project’s many unique aspects. The word “Standard” in the title of this document has been approved through ASTM consensus process. 1.7 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in practice D6026. 1.7.1 The method used to specify how data are collected, calculated, or recorded in this standard is not directly related to the accuracy to which the data can be applied in the design or other uses, or both. How one applies the results obtained using this standard is beyond its scope. 1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
SIGNIFICANCE AND USE 5.1 To establish a proper calibration area for nuclear surface gauges. 5.2 To reduce the chance of improper calibration. Note 1: The quality of the results produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of practice D3740 are generally considered capable of competent and objective testing/inspection/etc. Users of this standard are cautioned that compliance with practice D3740 does not in itself assure a means of evaluating some of those factors. SCOPE 1.1 This guide outlines procedures for setup of a nuclear gauge calibration facility in either a shielded bay or an unshielded area—Guide A and Guide B, respectively. 1.2 This guide does not attempt to describe the calibration techniques or methods. It is assumed that this guide will be used by persons familiar with the operations of the gauge and in performing proper calibration, service and maintenance. 1.3 This guide does not attempt to address maintenance or service procedures related to the gauge. 1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.6 This guide offers an organized collection of information or a series of options and does not recommend a specific course of action. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this guide may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project’s many unique aspects. The word “Standard” in the title of this document has been approved through ASTM consensus process. 1.7 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in practice D6026. 1.7.1 The method used to specify how data are collected, calculated, or recorded in this standard is not directly related to the accuracy to which the data can be applied in the design or other uses, or both. How one applies the results obtained using this standard is beyond its scope. 1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM D7013/D7013M-23 is classified under the following ICS (International Classification for Standards) categories: 27.120.10 - Reactor engineering. The ICS classification helps identify the subject area and facilitates finding related standards.
ASTM D7013/D7013M-23 has the following relationships with other standards: It is inter standard links to ASTM D3740-23, ASTM D3740-19, ASTM D6938-17, ASTM D6938-15, ASTM D653-14, ASTM D3740-12a, ASTM D3740-12, ASTM D653-11, ASTM D3740-11, ASTM D6938-10, ASTM D3740-10, ASTM D653-09, ASTM D653-08a, ASTM D653-08, ASTM D6938-08a. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
ASTM D7013/D7013M-23 is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.
Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D7013/D7013M − 23
Standard Guide for
Calibration Facility Setup for Nuclear Surface Gauges
This standard is issued under the fixed designation D7013/D7013M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* 1.7.1 The method used to specify how data are collected,
calculated, or recorded in this standard is not directly related
1.1 This guide outlines procedures for setup of a nuclear
to the accuracy to which the data can be applied in the design
gauge calibration facility in either a shielded bay or an
or other uses, or both. How one applies the results obtained
unshielded area—Guide A and Guide B, respectively.
using this standard is beyond its scope.
1.2 This guide does not attempt to describe the calibration
1.8 This international standard was developed in accor-
techniques or methods. It is assumed that this guide will be
dance with internationally recognized principles on standard-
used by persons familiar with the operations of the gauge and
ization established in the Decision on Principles for the
in performing proper calibration, service and maintenance.
Development of International Standards, Guides and Recom-
1.3 This guide does not attempt to address maintenance or
mendations issued by the World Trade Organization Technical
service procedures related to the gauge.
Barriers to Trade (TBT) Committee.
1.4 The values stated in either SI units or inch-pound units
2. Referenced Documents
are to be regarded separately as standard. The values stated in
2.1 ASTM Standards:
each system may not be exact equivalents; therefore, each
D653 Terminology Relating to Soil, Rock, and Contained
system shall be used independently of the other. Combining
Fluids
values from the two systems may result in non-conformance
D3740 Practice for Minimum Requirements for Agencies
with the standard.
Engaged in Testing and/or Inspection of Soil and Rock as
1.5 This standard does not purport to address all of the
Used in Engineering Design and Construction
safety concerns, if any, associated with its use. It is the
D6026 Practice for Using Significant Digits and Data Re-
responsibility of the user of this standard to establish appro-
cords in Geotechnical Data
priate safety, health, and environmental practices and deter-
D6938 Test Methods for In-Place Density and Water Content
mine the applicability of regulatory limitations prior to use.
of Soil and Soil-Aggregate by Nuclear Methods (Shallow
1.6 This guide offers an organized collection of information
Depth)
or a series of options and does not recommend a specific
course of action. This document cannot replace education or
3. Terminology
experience and should be used in conjunction with professional
3.1 For definitions of common technical terms in this
judgment. Not all aspects of this guide may be applicable in all
standard, refer to Terminology D653.
circumstances. This ASTM standard is not intended to repre-
sent or replace the standard of care by which the adequacy of
3.2 Definitions of Terms Specific to This Standard:
a given professional service must be judged, nor should this
3.2.1 cinder block—a hollow building block made with
document be applied without consideration of a project’s many
concrete and coal cinders.
unique aspects. The word “Standard” in the title of this
3.2.2 solid concrete blocks—solid concrete blocks designed
document has been approved through ASTM consensus pro-
for areas requiring radiation shielding.
cess.
3.2.3 safe position—position of the density source during
1.7 All observed and calculated values shall conform to the
the standardization process of the gauge.
guidelines for significant digits and rounding established in
3.2.4 shielded calibration bay—an enclosed area sur-
practice D6026.
rounded by walls in order to reduce background radiation to an
acceptable level.
This guide is under the jurisdiction of ASTM Committee D18 on Soil and Rock
and is the direct responsibility of Subcommittee D18.08 on Special and Construc-
tion Control Tests. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Feb. 15, 2023. Published March 2023. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 2004. Last previous edition approved in 2015 as D7013–15. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/D7013_D7013M-23. the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D7013/D7013M − 23
3.2.5 shielded storage bay—an enclosed area with sufficient 7.1.3 If more than five gauges are routinely stored in the
shielding material to maintain and control radiation back- storage bay, build a wall made from solid concrete or cinder
ground in the facility and to reduce influences from stored blocks filled with sand or fine aggregate material.
gauges. 7.1.4 The wall thickness for the storage bay shall be a
minimum of 410 mm [16 in]. The wall shall completely
3.2.6 unshielded area—an open area within a calibration
surround the area where the gauges are planned to be stored. If
facility where the closest wall is a minimum of 1 m [3 ft] from
gauges are stored on shelves that are elevated from the floor,
the spot in which the gauge is being calibrated.
the height of the wall shall be a minimum of 0.5 m [20 in]
above the height of the shelves on which gauges are stored.
4. Summary of Method
4.1 Nuclear moisture density gauges require proper calibra-
8. Guide A: Shielded Calibration Bay Setup
tion. Since these gauges contain radioactive isotopes, influ-
8.1 Set up a shielded calibration bay if two or more gauges
ences from the surroundings and other gauges shall be con-
are going to be calibrated simultaneously, and the space
trolled during the calibration process. This guide provides
between gauges being calibrated is less than 10 m [33 ft]. If the
procedures to facilities involved in calibration of one or more
gauge in storage bay is less than 10 m [33 ft] from the area
gauges in a shielded bay or and an unshielded area. The goal of
where the calibration is going to take place, or if the area where
this guide is to provide a calibration and storage facility for
gauges are routinely serviced is less than 10 meters [33 ft] from
proper gauge calibration.
the calibration area. Refer to Appendix X1 for examples of
shielded calibration bay configurations. Use Guide B if 8.1
5. Significance and Use
does not apply to the calibration facility.
5.1 To establish a proper calibration area for nuclear surface
8.1.1 Determine the number of bays required for calibration
gauges.
of nuclear gauges. This can be based on the number of gauges
calibrated per year and can vary from one to several bays.
5.2 To reduce the chance of improper calibration.
8.1.2 The bay inside dimensions should be established
NOTE 1—The quality of the results produced by this standard is
dependent on the competence of the personnel performing it, and the
based on the bay walls being a minimum of 610 mm [24 in.]
suitability of the equipment and facilities used. Agencies that meet the
from the center of calibration blocks and lined with 1 mm
criteria of practice D3740 are generally considered capable of competent
[0.032 in.] of lead. Smaller inside dimensions can be used if
and objective testing/inspection/etc. Users of this standard are cautioned
lead sheets thicker than 6 mm [0.25 in.] are used on the walls.
that compliance with practice D3740 does not in itself assure a means of
However, under no circumstances shall the walls be less than
evaluating some of those factors.
610 mm [24 in.] from center of the calibration block.
6. Apparatus
NOTE 2—Lead sheets may not be required, if it is determined that the
6.1 Calibration reference block(s) as per the requirements of wall influence (counts inside and outside the bay (See 8.2.1)) is within an
acceptable limit.
Test Method D6938 with density certification from a qualified
calibration facility.
8.1.3 A calibration bay wall thickness of 410 mm [16 in.]
thick has been proven to be successful. Walls constructed of
6.2 Solid concrete blocks 9 cm high × 20 cm wide × 41 cm
solid concrete blocks or cinder blocks filled with sand or fine
long [3.5 in. × 8 in. × 16 in.] or cinder blocks 20 cm high × 20
aggregate material have been used effectively for minimizing
cm wide × 41 cm long [8 in. × 8 in. × 16 in.] filled with sand or
outside influences. Stagger the blocks during wall construction
other fine aggregate materials for construction of bay walls.
to reduce gaps between blocks and to improve wall integrity.
6.3 Lead sheet 1 to 6 mm [0.032 to 0.25 in.] thick for lining
8.1.4 The wall height should be at a minimum from 1.0 to
the bay walls. The exposed surfaces containing lead shall be
1.3 m [40 to 50 in.].
painted or covered.
8.1.5 Design and construct the bay such that the opening of
6.4 Miscellaneous hardware for securing lead sheets to the the bay is not in direct line with the opening of the storage bay
calibration bay walls. or the area where the gauges are serviced.
8.1.6 Center the calibration reference block(s) in the bay.
7. Sh
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D7013/D7013M − 15 D7013/D7013M − 23
Standard Guide for
Calibration Facility Setup for Nuclear Surface Gauges
This standard is issued under the fixed designation D7013/D7013M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope*
1.1 This guide outlines procedures for setup of a nuclear gauge calibration facility in either a shielded bay or an unshielded
area—Guide A and Guide B, respectively.
1.2 This guide does not attempt to describe the calibration techniques or methods. It is assumed that this guide will be used by
persons familiar with the operations of the gauge and in performing proper calibration, service and maintenance.
1.3 This guide does not attempt to address maintenance or service procedures related to the gauge.
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each
system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the
two systems may result in non-conformance with the standard.
1.5 This guidestandard does not purport to address all of the safety concerns, if any, associated with its use. It is the
responsibility of the user of this guidestandard to establish appropriate safety, health, and healthenvironmental practices and
determine the applicability of regulatory limitations prior to use.
1.6 This guide offers an organized collection of information or a series of options and does not recommend a specific course of
action. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not
all aspects of this guide may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the
standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied
without consideration of a project’s many unique aspects. The word “Standard” in the title of this document has been approved
through ASTM consensus process.
1.7 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in practice
D6026.
1.7.1 The method used to specify how data are collected, calculated, or recorded in this standard is not directly related to the
accuracy to which the data can be applied in the design or other uses, or both. How one applies the results obtained using this
standard is beyond its scope.
1.8 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
This guide is under the jurisdiction of ASTM Committee D18 on Soil and Rock and is the direct responsibility of Subcommittee D18.08 on Special and Construction
Control Tests.
Current edition approved May 1, 2015Feb. 15, 2023. Published June 2015March 2023. Originally approved in 2004. Last previous edition approved in 20112015 as
D7013–11. DOI: 10.1520/D7013_D7013M-15.–15. DOI: 10.1520/D7013_D7013M-23.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D7013/D7013M − 23
2. Referenced Documents
2.1 ASTM Standards:
D653 Terminology Relating to Soil, Rock, and Contained Fluids
D3740 Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in
Engineering Design and Construction
D6026 Practice for Using Significant Digits and Data Records in Geotechnical Data
D6938 Test Methods for In-Place Density and Water Content of Soil and Soil-Aggregate by Nuclear Methods (Shallow Depth)
3. Terminology
3.1 For definitions of common technical terms in this standard, refer to Terminology D653.
3.2 Definitions of Terms Specific to This Standard:
3.2.1 cinder block—a hollow building block made with concrete and coal cinders.
3.2.2 high density solid concrete blocks—solid concrete blocks designed for areas requiring radiation shielding.
3.2.3 safe position—position of the density source during the standardization process of the gauge.
3.2.4 shielded calibration bay—an enclosed area surrounded by walls in order to reduce background radiation to an acceptable
level.
3.2.5 shielded storage bay—an enclosed area with sufficient shielding material to maintain and control radiation background in
the facility and to reduce influences from stored gauges.
3.2.6 unshielded area—an open area within a calibration facility where the closest wall is a minimum of 1 m [3 ft] from the spot
in which the gauge is being calibrated.
4. Summary of Method
4.1 Nuclear moisture density gauges require proper calibration. Since these gauges contain radioactive isotopes, influences from
the surroundings and other gauges shouldshall be controlled during the calibration process. This guide provides procedures to
facilities involved in calibration of one or more gauges in a shielded bay or and an unshielded area. The goal of this guide is to
provide a calibration and storage facility for proper gauge calibration.
5. Significance and Use
5.1 To establish a proper calibration area for nuclear surface gauges.
5.2 To reduce the chance of improper calibration.
NOTE 1—The quality of the results produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the
equipment and facilities used. Agencies that meet the criteria of practice D3740 are generally considered capable of competent and objective
testing/inspection/etc. Users of this standard are cautioned that compliance with practice D3740 does not in itself assure a means of evaluating some of
those factors.
6. Apparatus
6.1 Calibration reference block(s) as per the requirements of Test Method D6938 with density certification from a qualified
calibration facility.
6.2 High density Solid concrete blocks 9 cm high × 20 cm wide × 41 high × 20 cm wide × 41 cm long [3.5 in. × 8 in. × 16 in. × 8
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
D7013/D7013M − 23
in. × 16 in.] or cinder blocks 20 cm high × 20 cm wide × 41 high × 20 cm wide × 41 cm long [8 in. × 8 in. × 16 in. × 8 in. × 16
in.] filled with sand or other fine aggregate materials for construction of bay walls.
6.3 Lead sheet 1 to 6 mm [0.032 to 0.25 in.] thick for lining the bay walls. The exposed surfaces containing lead shouldshall be
painted or covered.
6.4 Miscellaneous hardware for securing lead sheets to the calibration bay walls.
7. Shielded Storage Bay Setup
7.1 Set up a shielded storage bay if more than five gauges are routinely stored at a distance of 10 m [33 ft] or less from the area
where gauge calibration is to take place. If five or less gauges are routinely stored in the storage area, concrete walls are not
necessary. However, gauges shouldshall be stored in their shipping cases or likewise secured while other gauges are being
calibrated. Refer to Appendix X1 for examples of shielded storage bay configurations.
7.1.1 The storage bay shouldshall not be set up directly under or over the area where gauges are to be calibrated.
7.1.2 Stagger the blocks during wall construction to reduce gaps between blocks and to improve wall integrity.
7.1.3 If more than five gauges are routinely stored in the storage bay, build a wall made from high density solid concrete or cinder
blocks filled with sand or fine aggregate material.
7.1.4 The wall thickness for the storage bay shouldshall be a minimum of 410 mm [16 in]. The wall shouldshall completely
surround the area where the gauges are planned to be stored. If gauges are stored on shelves that are elevated from the floor, the
height of the wall shouldshall be a minimum of 0.5 m [20 in] above the height of the shelves on which gauges are stored.
NOTE 2—Additional requirements might be necessary in order to meet state and federal licensing regulations. These requirements might include, lockable
doors to limit access and appropriate caution signs. Users should check their materials license requirements and check with their regulatory agency when
building storage bays for nuclear gauges.
8. Guide A: Shielded Calibration Bay Setup
8.1 Set up a shielded calibration bay if two or more gauges are going to be calibrated simultaneously, and the space between
gauges being calibrated is less than 10 m [33 ft]. If the gauge in storage bay is less than 10 m [33 ft] from the area where the
calibration is going to take place, or if the area where gauges are routinely serviced is less than 10 meters [33 ft] from the
calibration area. Refer to Appendix X1 for examples of shielded calibration bay configurations. Use Guide B if 8.1 does not apply
to the calibration facility.
NOTE 3—Use Guide B if 8.1 does not apply to your calibration facility.
8.1.1 Determine the number of bays required for calibration of nuclear gauges. This can be based on the number of gauges
calibrated per year and can vary from one to several bays.
8.1.2 The bay inside dimensions should be established based on the bay walls being a minimum of 610 mm [24 in.] from the center
of calibration blocks and lined with 1 mm [0.032 in.] of lead. Smaller inside dimensions can be used if lead sheets thicker than
6 mm [0.25 in.] are used on the walls. However, under no circumstances shouldshall the walls be less than 610 mm [24 in.] from
center of the calibration block.
NOTE 2—Lead sheets may not be required, if it is determined that the wall influence (counts inside and outside the bay (See 8.2.1)) is within an accepta
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