ASTM F2778-09(2020)

ASTM F2778-09(2020) is a standard published by ASTM International. Its full title is "Standard Test Method for Measurement of Percent Crystallinity of Polyetheretherketone (PEEK) Polymers by Means of Specular Reflectance Fourier Transform Infrared Spectroscopy (R-FTIR)". This standard covers: SIGNIFICANCE AND USE 4.1 Mechanical properties of PEEK polymers, such as stiffness or yield strength, are influenced by the level of crystallinity.5 The reported crystallinity index determined by this test method has been correlated with percent crystallinity in PEEK polymers by wide-angle X-ray scattering (WAXS) experiments.2, 3 4.2 This test method may be useful for both process development, process control, product development, and research. SCOPE 1.1 This test method describes the collection of absorption spectra of polyetheretherketone (PEEK) polymer in filled and unfilled grades, as supplied by a vendor, and the subsequent calculation of the percent crystallinity. The material is evaluated by infrared spectroscopy. The intensity (height) of the absorbance peaks is related to the amount of crystalline regions present in the material. 1.2 This test method can be used for PEEK consolidated forms, such as injection molded parts, as long as the samples are optically flat and smooth. 1.3 The applicability of the infrared method to industrial and medical grade PEEK materials has been demonstrated by scientific studies.2, 3 Percentage of crystallinity is related to R-FTIR measurement by calibration through wide-angle x-ray scattering (WAXS) crystallinity measurements.2, 3 It is anticipated that this test method, involving the peak heights near 1305 cm-1 and 1280 cm-1, will be evaluated in an Interlaboratory Study (ILS) conducted according to Test Method E691. 1.4 This test method does not suggest a desired range of crystallinity for specific applications. 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE 4.1 Mechanical properties of PEEK polymers, such as stiffness or yield strength, are influenced by the level of crystallinity.5 The reported crystallinity index determined by this test method has been correlated with percent crystallinity in PEEK polymers by wide-angle X-ray scattering (WAXS) experiments.2, 3 4.2 This test method may be useful for both process development, process control, product development, and research. SCOPE 1.1 This test method describes the collection of absorption spectra of polyetheretherketone (PEEK) polymer in filled and unfilled grades, as supplied by a vendor, and the subsequent calculation of the percent crystallinity. The material is evaluated by infrared spectroscopy. The intensity (height) of the absorbance peaks is related to the amount of crystalline regions present in the material. 1.2 This test method can be used for PEEK consolidated forms, such as injection molded parts, as long as the samples are optically flat and smooth. 1.3 The applicability of the infrared method to industrial and medical grade PEEK materials has been demonstrated by scientific studies.2, 3 Percentage of crystallinity is related to R-FTIR measurement by calibration through wide-angle x-ray scattering (WAXS) crystallinity measurements.2, 3 It is anticipated that this test method, involving the peak heights near 1305 cm-1 and 1280 cm-1, will be evaluated in an Interlaboratory Study (ILS) conducted according to Test Method E691. 1.4 This test method does not suggest a desired range of crystallinity for specific applications. 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM F2778-09(2020) is classified under the following ICS (International Classification for Standards) categories: 83.080.20 - Thermoplastic materials. The ICS classification helps identify the subject area and facilitates finding related standards.

ASTM F2778-09(2020) has the following relationships with other standards: It is inter standard links to ASTM E691-13, ASTM E691-11, ASTM E691-08, ASTM E691-05, ASTM E691-99. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

ASTM F2778-09(2020) is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.