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ASTM E439-10

(Test Method)

Standard Test Methods for Chemical Analysis of Beryllium

Standard Test Methods for Chemical Analysis of Beryllium

SIGNIFICANCE AND USE
These test methods for the chemical analysis of beryllium metal are primarily intended as referee methods to test such materials for compliance with compositional specifications. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.
SCOPE
1.1 These test methods cover the chemical analysis of beryllium having chemical compositions within the following limits:
1.2 The test methods in this standard are contained in the sections indicated below.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
10.1 This test method covers the determination of chromium in concentrations from 0.004 % to 0.04 %.  
20.1 This test method covers the determination of iron in concentrations from 0.05 % to 0.25 %.  
30.1 This test method covers the determination of manganese in beryllium metal in concentrations from 0.008 % to 0.04 %.  
40.1 This test method covers the determination of nickel in concentrations from 0.001 % to 0.04 %.

General Information

Status
Historical
Publication Date
14-Jan-2010
ICS
77.040.30 - Chemical analysis of metals
77.120.99 - Other non-ferrous metals and their alloys
Technical Committee
E01 - Analytical Chemistry for Metals, Ores, and Related Materials
Drafting Committee
E01.05 - Cu, Pb, Zn, Cd, Sn, Be, Precious Metals, their Alloys, and Related Metals
Current Stage
Ref Project

Relations

Replaces
ASTM E439-04a - Standard Test Methods for Chemical Analysis of Beryllium
Effective Date
15-Jan-2010

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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: E439 − 10
Standard Test Methods for
1
Chemical Analysis of Beryllium
This standard is issued under the fixed designation E439; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
2
1.1 These test methods cover the chemical analysis of 2.1 ASTM Standards:
beryllium having chemical compositions within the following D1193 Specification for Reagent Water
limits: E29 Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
Concentration
Element Range, %
E50 Practices for Apparatus, Reagents, and Safety Consid-
Aluminum 0.05 to 0.30
erations for Chemical Analysis of Metals, Ores, and
Beryllium 97.5 to 100
Related Materials
Beryllium Oxide 0.3 to 3
Carbon 0.05 to 0.30
E55 Practice for Sampling Wrought Nonferrous Metals and
Copper 0.005 to 0.10
Alloys for Determination of Chemical Composition
Chromium 0.005 to 0.10
E60 Practice for Analysis of Metals, Ores, and Related
Iron 0.05 to 0.30
Magnesium 0.02 to 0.15
Materials by Spectrophotometry
Nickel 0.005 to 0.10
E88 Practice for Sampling Nonferrous Metals and Alloys in
Silicon 0.02 to 0.15
Cast Form for Determination of Chemical Composition
1.2 The test methods in this standard are contained in the
E135 Terminology Relating to Analytical Chemistry for
sections indicated below.
Metals, Ores, and Related Materials
Sections
E173 Practice for Conducting Interlaboratory Studies of
Chromium by the Diphenylcarbazide Photometric Test Method
Methods for Chemical Analysis of Metals (Withdrawn
[0.004 % to 0.04 %] 10-19
3
Iron by the 1,10-Phenanthroline Photometric Test Method
1998)
[0.05 % to 0.25 %] 20-29
E1601 Practice for Conducting an Interlaboratory Study to
Manganese by the Periodate Photometric Test Method
Evaluate the Performance of an Analytical Method
[0.008 % to 0.04 %] 30-39
Nickel by the Dimethylglyoxime Photometric Test Method
[0.001 % to 0.04 %] 40-49 3. Terminology
1.3 The values stated in SI units are to be regarded as
3.1 For definitions of terms used in this test method, refer to
standard. No other units of measurement are included in this
Terminology E135.
standard.
4. Significance and Use
1.4 This standard does not purport to address all of the
4.1 These test methods for the chemical analysis of beryl-
safety problems, if any, associated with its use. It is the
lium metal are primarily intended as referee methods to test
responsibility of the user of this standard to establish appro-
such materials for compliance with compositional specifica-
priate safety and health practices and determine the applica-
tions. It is assumed that all who use these test methods will be
bility of regulatory limitations prior to use.
trained analysts capable of performing common laboratory
1
These test methods are under the jurisdiction of ASTM Committee E01 on
2
Analytical Chemistry for Metals, Ores, and Related Materials and are the direct For referenced ASTM standards, visit the ASTM website, www.astm.org, or
responsibility of Subcommittee E01.05 on Cu, Pb, Zn, Cd, Sn, Be, theirAlloys, and contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Related Metals. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved Jan. 15, 2010. Published February 2010. Originally the ASTM website.
3
published in 1971. Last previous edition approved in 2004 as E439 – 04a. DOI: The last approved version of this historical standard is referenced on
10.1520/E0439-10. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E439 − 10
NOTE1—Thistestmethodhasbeenwrittenforcellshavinga2-cmlight
proceduresskillfullyandsafely.Itisexpectedthatworkwillbe
path. Cells having other dimensions may be used, provided suitable
performed in a properly equipped laboratory.
adjustments can be made in the amounts of sample and reagents used.
5. Apparatus, Reagents, and Photometric Practice
13. Stability of Color
5.1 Apparatus and reagents required for each determination
13.1 The color of the chromium complex develops almost
are listed in separate sections preceding the procedure unless
immediately but starts to fade after about 10 min. Photometric
otherwise specified. The apparatus, standard solutions, and
measurements should be made within 5 min after developing
reagents shall conform to the requirements prescribed in
the color.
Practices E50. Photometers shall conform to the requirements
prescribed in Practice E60. 14. Interferences
...

This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:E439–04a Designation:E439–10
Standard Test Methods for
1
Chemical Analysis of Beryllium
This standard is issued under the fixed designation E439; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 These test methods cover the chemical analysis of beryllium having chemical compositions within the following limits:
Concentration
Element Range, %
Aluminum 0.05 to 0.30
Beryllium 97.5 to 100
Beryllium Oxide 0.3 to 3
Carbon 0.05 to 0.30
Copper 0.005 to 0.10
Chromium 0.005 to 0.10
Iron 0.05 to 0.30
Magnesium 0.02 to 0.15
Nickel 0.005 to 0.10
Silicon 0.02 to 0.15
1.2 The test methods in this standard are contained in the sections indicated below.
Sections
Chromium by the Diphenylcarbazide Photometric Test Method
[0.004 to 0.04 %] 10-19
Chromium by the Diphenylcarbazide Photometric Test Method
[0.004 % to 0.04 %] 10-19
Iron by the 1,10-Phenanthroline Photometric Test Method
[0.05 to 0.25 %] 20-29
Iron by the 1,10-Phenanthroline Photometric Test Method
[0.05 % to 0.25 %] 20-29
Manganese by the Periodate Photometric Test Method
[0.008 to 0.04 %] 30-39
Manganese by the Periodate Photometric Test Method
[0.008 % to 0.04 %] 30-39
Nickel by the Dimethylglyoxime Photometric Test Method
[0.001 to 0.04 %] 40-49
Nickel by the Dimethylglyoxime Photometric Test Method
[0.001 % to 0.04 %] 40-49
1.3
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D1193 Specification for Reagent Water
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E50 PracticesforApparatus,Reagents,andSafetyConsiderationsforChemicalAnalysisofMetals,Ores,andRelatedMaterials
E55 Practice for Sampling Wrought Nonferrous Metals and Alloys for Determination of Chemical Composition
E60 Practice for Analysis of Metals, Ores, and Related Materials by Molecular Absorption Spectrometry
E88 Practice for Sampling Nonferrous Metals and Alloys in Cast Form for Determination of Chemical Composition
1
These test methods are under the jurisdiction ofASTM Committee E01 onAnalytical Chemistry for Metals, Ores, and Related Materials and are the direct responsibility
of Subcommittee E01.05 on Cu, Pb, Zn, Cd, Sn, Be, their Alloys, and Related Metals.
Current edition approved Oct. 1, 2004.Jan. 15, 2010. Published November 2004.February 2010. Originally published in 1971. Last previous edition approved in 2004 as
E439 – 04a. DOI: 10.1520/E0439-04A.10.1520/E0439-10.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
E439–10
E135 Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
3
E173 Practice for Conducting Interlaboratory Studies of Methods for Chemical Analysis of Metals
E1601 Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
3. Terminology
3.1 For definitions of terms used in this test method, refer to Terminology E135.
4. Significance and Use
4.1 These test methods for the chemical analysis of beryllium metal are primarily intended as referee methods to test such
materials for compliance with compositional specifications. It is assumed that all who use these test methods will be trained
analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in
a properly equipped laboratory.
5. Apparatus, Reagents, and Photometric Practice
5.1 Apparatus and reagents required for each determination are listed in separate sections preceding the procedure unless
otherwise specified.The apparatus, standard solutions, and reagents shall co
...

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ASTM E439-23(Test Method)
Standard Test Methods for Chemical Analysis of Beryllium

SIGNIFICANCE AND USE
4.1 These test methods for the chemical analysis of beryllium metal are primarily intended as referee methods to test such materials for compliance with compositional specifications. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.
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1.1 These test methods cover the chemical analysis of beryllium having chemical compositions within the following limits:    
Element  
Range, %  
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0.05 to 0.30  
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4.1 These test methods for the chemical analysis of beryllium metal are primarily intended as referee methods to test such materials for compliance with compositional specifications. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.
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  • Standard
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ASTM
ASTM B472-23(Specification)
Standard Specification for Nickel Alloy Billets and Bars for Reforging

ABSTRACT
This specification covers UNS N06002, UNS N06030, UNS N06035, UNS N06022, UNS N06200, UNS N06230, UNS N06600, UNS N06617, UNS N06625, UNS N08020, UNS N08026, UNS N08024, UNS N08120, UNS N08926, UNS N08367, UNS N10242, UNS N10276, UNS N10665, UNS N10675, UNS N12160, UNS R20033, UNS N06059, UNS N06686, UNS N10629, UNS N08031, UNS N06045, UNS N06025, and UNS R30556 nickel alloy billets and bars for reforging. The products shall be hot worked from ingots by rolling, forging, extruding, hammering, or pressing. The material shall conform to the chemical composition requirements prescribed by the reference material. The chemical composition of the material shall be determined by chemical analysis in accordance with test method E1473.
SCOPE
1.1 This specification covers UNS N06002, UNS N06030, UNS N06035, UNS N06022, UNS N06200, UNS N10362, UNS N06230, UNS N06600, UNS N06617, UNS N06625, UNS N08020, UNS N08026, UNS N08024, UNS N08120, UNS N08926, UNS N08367, UNS N10242, UNS N10276, UNS N10665, UNS N10675, UNS N12160, UNS R20033, UNS N06059, UNS N06686, UNS N10629, UNS N08031, UNS N06045, UNS N06025, UNS N06699, and UNS R305562 billets and bars for reforging.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to become familiar with all hazards including those identified in the appropriate Safety Data Sheet (SDS) for this product/material as provided by the manufacturer, to establish appropriate safety, health, and environmental practices, and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Technical specification
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  • Technical specification
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    English language
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