Standard Test Method for Hot Water Accelerated Aging of Glass-Fiber Reinforced Cement-Based Composites

SIGNIFICANCE AND USE
3.1 The basis for this test as an indicator of the long term behavior of fiber reinforced composites is that elevated temperature and moisture content accelerate the formation of the products of hydration of the cement in the matrix, particularly calcium hydroxide.  
3.1.1 It is known that the interaction of these products of hydration, particularly calcium hydroxide, with the fibers can have a major effect on the long-term properties of the composites.  
3.1.2 The principal mechanism that occurs is that the calcium hydroxide forms within the bundles of filaments that form the glass fiber strand. This gradually bonds the filaments together, which reduces filament pull-out. This causes a reduction in the strain capacity of the composite, thereby reducing the strength of the composite and changing the composite from a ductile material to an increasingly brittle material.  
3.1.3 Accelerating the formation of the hydration products accelerates their interaction with the fibers, hence accelerating the aging of the composite.  
3.2 The data developed from this test are used by researchers and manufacturers to evaluate the long-term performance of different mixtures, reinforcements, mixture components, and to provide data for the development of design procedures for products made from these composites.  
3.2.1 The recorded data also provides screening information as new matrices and reinforcements are developed.  
3.3 The usefulness of the test as an indicator of long term composite performance is valid if the only reactions that are accelerated are those that occur more slowly under natural weathering, hot water can induce effects in some composites, for instance those containing acrylic polymer, that may not occur in natural weathering. This test method may not be a valid indicator of long-term performance of such composites.
SCOPE
1.1 This test method provides a way of accelerating the aging of glass fiber reinforced cementitious composites in order to develop data that will indicate real-life natural weathering performance.  
1.2 The coupons prepared for this test method will be tested using Test Method C947.  
1.3 This test method can be used to age coupons for other test methods.  
1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
30-Apr-2023

Relations

Effective Date
01-May-2009
Effective Date
01-May-2009
Effective Date
01-Dec-2004
Effective Date
10-Jun-2003
Effective Date
10-Jan-1999
Effective Date
01-Jan-1996

Overview

ASTM C1560-03(2023) is the internationally recognized standard test method for Hot Water Accelerated Aging of Glass-Fiber Reinforced Cement-Based Composites (GFRC). Developed by ASTM International, this method provides a practical protocol to simulate long-term aging effects on cement-based composites containing glass fibers by exposing them to elevated temperatures and moisture. The goal is to rapidly assess the durability, mechanical properties, and long-term performance of these composites, thereby supporting design procedures and material selection in construction and manufacturing.

Key Topics

  • Purpose of Accelerated Aging:
    Hot water exposure under controlled conditions accelerates the hydration process in cement-based matrices, particularly the formation of calcium hydroxide. This simulates and condenses years of natural weathering into a shorter testing period.

  • Impact on Composite Properties:
    The test reveals how calcium hydroxide interacts with glass fibers, which can alter the composite's mechanical integrity. Over time, these reactions can change the composite from ductile to brittle, affecting strain capacity and ultimate strength.

  • Test Procedure Basics:

    • Preparation of test coupons according to established methods.
    • Immersion of coupons in preheated water tanks, with temperatures typically controlled between 122°F (50°C) and 176°F (80°C).
    • Monitoring at set intervals (e.g., 0, 5, 10, 20, up to 90+ days) to track degradation effects.
    • Measurement of properties such as modulus of rupture and strain to failure, as specified in ASTM C947.
  • Interpretation of Data:
    Results provide essential screening data as new cement matrices and reinforcements are developed, aiding in comparative performance assessment and research.

Applications

  • Material Qualification and Research:
    Researchers and quality control laboratories use this standard to compare different GFRC formulations and reinforcement systems, ensuring consistent quality and performance in real-world applications.

  • Product Development:
    The data are instrumental in developing new mixtures with optimal durability, and in verifying the suitability of glass-fiber reinforcements for architectural panels, cladding, and infrastructure elements.

  • Design and Specification:
    Engineers and designers rely on accelerated aging data to inform structural calculations, especially for components exposed to moisture and fluctuating temperatures.

  • Quality Assurance for Manufacturers:
    The test supports manufacturers in maintaining material compliance and meeting client specifications for glass fiber reinforced concrete products.

Related Standards

  • ASTM C947:
    Test Method for Flexural Properties of Thin-Section Glass-Fiber-Reinforced Concrete (Using Simple Beam With Third-Point Loading). This method is used to evaluate mechanical properties of the aged test specimens.

  • ASTM C1228:
    Practice for Preparing Coupons for Flexural and Washout Tests on Glass Fiber Reinforced Concrete. Provides guidelines for preparing test pieces subjected to ASTM C1560 procedures.

  • International Standardization Principles:
    ASTM C1560 is aligned with the World Trade Organization’s TBT Committee guidelines, ensuring it meets globally recognized criteria for technical standards.


By adopting ASTM C1560-03(2023), organizations in the construction and composites industry can ensure more reliable evaluation of glass fiber reinforced cement-based composites, leading to improved product durability, safety, and performance in service. This standard is a crucial resource for accelerating material development while reducing risk associated with long-term degradation in GFRC applications.

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Frequently Asked Questions

ASTM C1560-03(2023) is a standard published by ASTM International. Its full title is "Standard Test Method for Hot Water Accelerated Aging of Glass-Fiber Reinforced Cement-Based Composites". This standard covers: SIGNIFICANCE AND USE 3.1 The basis for this test as an indicator of the long term behavior of fiber reinforced composites is that elevated temperature and moisture content accelerate the formation of the products of hydration of the cement in the matrix, particularly calcium hydroxide. 3.1.1 It is known that the interaction of these products of hydration, particularly calcium hydroxide, with the fibers can have a major effect on the long-term properties of the composites. 3.1.2 The principal mechanism that occurs is that the calcium hydroxide forms within the bundles of filaments that form the glass fiber strand. This gradually bonds the filaments together, which reduces filament pull-out. This causes a reduction in the strain capacity of the composite, thereby reducing the strength of the composite and changing the composite from a ductile material to an increasingly brittle material. 3.1.3 Accelerating the formation of the hydration products accelerates their interaction with the fibers, hence accelerating the aging of the composite. 3.2 The data developed from this test are used by researchers and manufacturers to evaluate the long-term performance of different mixtures, reinforcements, mixture components, and to provide data for the development of design procedures for products made from these composites. 3.2.1 The recorded data also provides screening information as new matrices and reinforcements are developed. 3.3 The usefulness of the test as an indicator of long term composite performance is valid if the only reactions that are accelerated are those that occur more slowly under natural weathering, hot water can induce effects in some composites, for instance those containing acrylic polymer, that may not occur in natural weathering. This test method may not be a valid indicator of long-term performance of such composites. SCOPE 1.1 This test method provides a way of accelerating the aging of glass fiber reinforced cementitious composites in order to develop data that will indicate real-life natural weathering performance. 1.2 The coupons prepared for this test method will be tested using Test Method C947. 1.3 This test method can be used to age coupons for other test methods. 1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE 3.1 The basis for this test as an indicator of the long term behavior of fiber reinforced composites is that elevated temperature and moisture content accelerate the formation of the products of hydration of the cement in the matrix, particularly calcium hydroxide. 3.1.1 It is known that the interaction of these products of hydration, particularly calcium hydroxide, with the fibers can have a major effect on the long-term properties of the composites. 3.1.2 The principal mechanism that occurs is that the calcium hydroxide forms within the bundles of filaments that form the glass fiber strand. This gradually bonds the filaments together, which reduces filament pull-out. This causes a reduction in the strain capacity of the composite, thereby reducing the strength of the composite and changing the composite from a ductile material to an increasingly brittle material. 3.1.3 Accelerating the formation of the hydration products accelerates their interaction with the fibers, hence accelerating the aging of the composite. 3.2 The data developed from this test are used by researchers and manufacturers to evaluate the long-term performance of different mixtures, reinforcements, mixture components, and to provide data for the development of design procedures for products made from these composites. 3.2.1 The recorded data also provides screening information as new matrices and reinforcements are developed. 3.3 The usefulness of the test as an indicator of long term composite performance is valid if the only reactions that are accelerated are those that occur more slowly under natural weathering, hot water can induce effects in some composites, for instance those containing acrylic polymer, that may not occur in natural weathering. This test method may not be a valid indicator of long-term performance of such composites. SCOPE 1.1 This test method provides a way of accelerating the aging of glass fiber reinforced cementitious composites in order to develop data that will indicate real-life natural weathering performance. 1.2 The coupons prepared for this test method will be tested using Test Method C947. 1.3 This test method can be used to age coupons for other test methods. 1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM C1560-03(2023) is classified under the following ICS (International Classification for Standards) categories: 91.100.30 - Concrete and concrete products. The ICS classification helps identify the subject area and facilitates finding related standards.

ASTM C1560-03(2023) has the following relationships with other standards: It is inter standard links to ASTM C1228-96(2009), ASTM C947-03(2009), ASTM C1228-96(2004), ASTM C947-03, ASTM C947-99, ASTM C1228-96. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

ASTM C1560-03(2023) is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.

Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: C1560 − 03 (Reapproved 2023)
Standard Test Method for
Hot Water Accelerated Aging of Glass-Fiber Reinforced
Cement-Based Composites
This standard is issued under the fixed designation C1560; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Washout Tests on Glass Fiber Reinforced Concrete
1.1 This test method provides a way of accelerating the
3. Significance and Use
aging of glass fiber reinforced cementitious composites in
3.1 The basis for this test as an indicator of the long term
order to develop data that will indicate real-life natural
behavior of fiber reinforced composites is that elevated tem-
weathering performance.
perature and moisture content accelerate the formation of the
1.2 The coupons prepared for this test method will be tested
products of hydration of the cement in the matrix, particularly
using Test Method C947.
calcium hydroxide.
1.3 This test method can be used to age coupons for other
3.1.1 It is known that the interaction of these products of
test methods.
hydration, particularly calcium hydroxide, with the fibers can
have a major effect on the long-term properties of the compos-
1.4 The values stated in inch-pound units are to be regarded
ites.
as standard. The values given in parentheses are mathematical
3.1.2 The principal mechanism that occurs is that the
conversions to SI units that are provided for information only
calcium hydroxide forms within the bundles of filaments that
and are not considered standard.
form the glass fiber strand. This gradually bonds the filaments
1.5 This standard does not purport to address all of the
together, which reduces filament pull-out. This causes a reduc-
safety concerns, if any, associated with its use. It is the
tion in the strain capacity of the composite, thereby reducing
responsibility of the user of this standard to establish appro-
the strength of the composite and changing the composite from
priate safety, health, and environmental practices and deter-
a ductile material to an increasingly brittle material.
mine the applicability of regulatory limitations prior to use.
3.1.3 Accelerating the formation of the hydration products
1.6 This international standard was developed in accor-
accelerates their interaction with the fibers, hence accelerating
dance with internationally recognized principles on standard-
the aging of the composite.
ization established in the Decision on Principles for the
3.2 The data developed from this test are used by research-
Development of International Standards, Guides and Recom-
ers and manufacturers to evaluate the long-term performance
mendations issued by the World Trade Organization Technical
of different mixtures, reinforcements, mixture components, and
Barriers to Trade (TBT) Committee.
to provide data for the development of design procedures for
products made from these composites.
2. Referenced Documents
3.2.1 The recorded data also provides screening information
2.1 ASTM Standards:
as new matrices and reinforcements are developed.
C947 Test Method for Flexural Properties of Thin-Section
3.3 The usefulness of the test as an indicator of long term
Glass-Fiber-Reinforced Concrete (Using Simple Beam
composite performance is valid if the only reactions that are
With Third-Point Loading)
accelerated are those that occur more slowly under natural
C1228 Practice for Preparing Coupons for Flexural and
weathering, hot water can induce effects in some composites,
for instance those containing acrylic polymer, that may not
occur in natural weathering. This test method may not be a
This test method is under the jurisdiction of ASTM Committee C27 on Precast
Concrete Products and is the direct responsibility of Subcommittee C27.40 on Glass
valid indicator of long-term performance of such composites.
Fiber Reinforced Concrete.
Current edition approved May 1, 2023. Published May 2023. Originally
4. Apparatus
approved in 2003. Last previous edition approved in 2016 as C1560 – 03(2016).
DOI: 10.1520/C1560-03R23.
4.1 Aging Tanks—Tank material can be but not limited to,
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
plastic, insulated to maintain a stable temperature. Insulation
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
should cover all exterior surfaces including the cover. Insula-
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. tion can be a foam product as used in building construction.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
C1560 − 03 (2023)
4.1.1 The size of the tank is typically 12 in. deep (300 mm), than a 5 % decrease in the flexural ultimate and/or a decrease
18 in. wide (450 mm), and 20 to 36 in. (600 to 900 mm), in of strain capacity of less than 10 %.
length. Size is determ
...

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