Standard Test Method for Residue by Evaporation of Emulsified Asphalt

SIGNIFICANCE AND USE
3.1 The test may be used to indicate compositional characteristics of emulsified asphalt. Evaporation residue may also be subjected to other characterization tests.  
3.2 This test method for residue by evaporation tends to give an asphaltic residue lower in penetration and ductility than the distillation test method (D6997). Material may be accepted but shall not be rejected as failing to meet specifications containing requirements for determination of residue by distillation, on data obtained by evaporation. If residue from evaporation fails to meet the requirements for properties specified for residue from distillation, tests shall be rerun using the distillation test method.
Note 1: The quality of results produced by this standard is dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guidance provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers the quantitative determination of residue in emulsified asphalts composed principally of a semisolid or liquid asphaltic base, water, and an emulsifying agent.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Publication Date
30-Jun-2022
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation:D6934 −22
Standard Test Method for
1
Residue by Evaporation of Emulsified Asphalt
This standard is issued under the fixed designation D6934; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3. Significance and Use
3.1 The test may be used to indicate compositional charac-
1.1 This test method covers the quantitative determination
teristics of emulsified asphalt. Evaporation residue may also be
of residue in emulsified asphalts composed principally of a
subjected to other characterization tests.
semisolid or liquid asphaltic base, water, and an emulsifying
agent.
3.2 This test method for residue by evaporation tends to
giveanasphalticresiduelowerinpenetrationandductilitythan
1.2 The values stated in SI units are to be regarded as
the distillation test method (D6997). Material may be accepted
standard. No other units of measurement are included in this
but shall not be rejected as failing to meet specifications
standard.
containing requirements for determination of residue by
1.3 The text of this standard references notes and footnotes distillation, on data obtained by evaporation. If residue from
which provide explanatory material. These notes and footnotes
evaporation fails to meet the requirements for properties
(excluding those in tables and figures) shall not be considered specified for residue from distillation, tests shall be rerun using
as requirements of the standard.
the distillation test method.
1.4 This standard does not purport to address all of the NOTE 1—The quality of results produced by this standard is dependent
on the competence of the personnel performing the procedure and the
safety concerns, if any, associated with its use. It is the
capability, calibration, and maintenance of the equipment used. Agencies
responsibility of the user of this standard to establish appro-
that meet the criteria of Specification D3666 are generally considered
priate safety, health, and environmental practices and deter-
capable of competent and objective testing, sampling, inspection, etc.
mine the applicability of regulatory limitations prior to use.
Users of this standard are cautioned that compliance with Specification
D3666 alone does not completely ensure reliable results. Reliable results
1.5 This international standard was developed in accor-
dependonmanyfactors;followingthesuggestionsofSpecificationD3666
dance with internationally recognized principles on standard-
or some similar acceptable guidance provides a means of evaluating and
ization established in the Decision on Principles for the
controlling some of those factors.
Development of International Standards, Guides and Recom-
4. Summary of Method
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
4.1 A sample of emulsified asphalt in an open top beaker is
heated in an oven at 163 6 3 °C to determine the percentage of
2. Referenced Documents
asphalt residue. The residue from the evaporation may be
2 tested as required.
2.1 ASTM Standards:
D3666 Specification for Minimum Requirements for Agen-
5. Sample Conditioning for Testing
cies Testing and Inspecting Road and Paving Materials
5.1 All emulsified asphalts shall be properly stirred to
D6997 Test Method for Distillation of Emulsified Asphalt
achieve homogeneity before testing.
E11 Specification for Woven Wire Test Sieve Cloth and Test
Sieves 5.2 All emulsified asphalts with viscosity testing require-
ments of 50 °C shall be heated to 50 6 3 °C in the original
sample container in a water bath or oven. The container should
be vented to relieve pressure. After the sample reaches 50 6
1
This test method is under the jurisdiction of ASTM Committee D04 on Road
3 °C, stir the sample to achieve homogeneity.
and Paving Materials and is the direct responsibility of Subcommittee D04.42 on
Emulsified Asphalt Test.
5.3 Emulsified asphalts with viscosity testing requirements
Current edition approved July 1, 2022. Published July 2022. Originally approved
of 25 °C should be mixed or stirred at 25 6 3 °C in the original
in 2004. Last previous edition approved in 2016 as D6934 – 08 (2016). DOI:
10.1520/D6934-22.
sample container to achieve homogeneity.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
NOTE 2—Emulsified asphalts with viscosity testing requirements of
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D6934 − 08 (Reapproved 2016) D6934 − 22
Standard Test Method for
1
Residue by Evaporation of Emulsified Asphalt
This standard is issued under the fixed designation D6934; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers the quantitative determination of residue in emulsified asphalts composed principally of a semisolid
or liquid asphaltic base, water, and an emulsifying agent.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes
(excluding those in tables and figures) shall not be considered as requirements of the standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D3666 Specification for Minimum Requirements for Agencies Testing and Inspecting Road and Paving Materials
D6997 Test Method for Distillation of Emulsified Asphalt
E11 Specification for Woven Wire Test Sieve Cloth and Test Sieves
3. Significance and Use
3.1 The test may be used to indicate compositional characteristics of emulsified asphalt. Evaporation residue may also be subjected
to other characterization tests.
3.2 This test method for residue by evaporation tends to give an asphaltic residue lower in penetration and ductility than the
distillation test method (D6997). Material may be accepted but shall not be rejected as failing to meet specifications containing
requirements for determination of residue by distillation, on data obtained by evaporation. If residue from evaporation fails to meet
the requirements for properties specified for residue from distillation, tests shall be rerun using the distillation test method.
1
This test method is under the jurisdiction of ASTM Committee D04 on Road and Paving Materials and areis the direct responsibility of Subcommittee D04.42 on
Emulsified Asphalt Test.
Current edition approved May 1, 2016July 1, 2022. Published May 2016July 2022. Originally approved in 2004. Last previous edition approved in 20082016 as
D6934 – 08.D6934 – 08 (2016). DOI: 10.1520/D6934-08R16.10.1520/D6934-22.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D6934 − 22
NOTE 1—The quality of results produced by this standard is dependent on the competence of the personnel performing the procedure and the capability,
calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent
and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely
ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guidance
provides a means of evaluating and controlling some of those factors.
4. Summary of Method
4.1 A sample of emulsified asphalt in an open top beaker is heated in an oven at 163 6 3°C3 °C to determine the percentage of
asphalt residue. The residue from the evaporation may be tested as required.
5. Sample Conditioning for Testing
5.1 All emulsified asphalts shall be properly stirred to achieve homogeneity before testing.
5.2 All emulsified asphalts with viscosity testin
...

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