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ASTM D1509-15

(Test Method)

Standard Test Methods for Carbon Black—Heating Loss

Standard Test Methods for Carbon Black—Heating Loss

SIGNIFICANCE AND USE
4.1 In addition to determining the heating loss (primarily moisture content) of carbon black, these drying conditions are used to prepare samples prior to performing other carbon black tests.  
4.2 When larger samples are prepared for other tests, use an open vessel of suitable dimensions so that the depth of the black is no more than 10 mm during conditioning.  
4.3 Carbon black is hygroscopic. The amount of moisture absorbed is related to the surface area of the black and to the relative humidity, ambient temperature, and time to which the material is exposed.
SCOPE
1.1 These test methods cover the determination of the heating loss of carbon black at 125°C. This heating loss consists primarily of moisture, but other volatile materials may also be lost. These test methods are not applicable to treated carbon blacks that contain added volatile materials, if moisture loss is to be measured.  
1.2 These test methods may also be used for the determination of the heating loss of recovered carbon fillers (rCF/rCB) at 125°C. However, these materials were not included in the precision studies and therefore, the precision statements contained in this standard may not be valid for these materials.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Oct-2015
ICS
83.040.20 - Rubber compounding ingredients
Technical Committee
D24 - Carbon Black
Drafting Committee
D24.31 - Non-Carbon Black Components of Carbon Black
Current Stage
Ref Project

Relations

Replaces
ASTM D1509-95(2012) - Standard Test Methods for Carbon Black—Heating Loss
Effective Date
01-Nov-2015
Referred By
ASTM D5817-20 - Standard Practice for Carbon Black, Pelleted—Reduction, Blending, and Drying of Gross Samples for Testing
Effective Date
01-Nov-2015
Referred By
ASTM D8466-22 - Standard Guide for Recovered Carbon Black—Carbon Black Test Methods for Testing rCB
Effective Date
01-Nov-2015
Referred By
ASTM D4139-04(2020) - Standard Guide for Determining Volatile and Nonvolatile Content of Pigments
Effective Date
01-Nov-2015
Referred By
ASTM D8043-20 - Standard Guide for Carbon Black—Shelf Life
Effective Date
01-Nov-2015
Referred By
ASTM D1799-20 - Standard Practice for Carbon Black—Sampling Packaged Shipments
Effective Date
01-Nov-2015
Referred By
ASTM D4122-17(2023) - Standard Practice for Carbon Black—Evaluation of an Industry Reference Black
Effective Date
01-Nov-2015
Referred By
ASTM E1868-10(2021) - Standard Test Methods for Loss-On-Drying by Thermogravimetry
Effective Date
01-Nov-2015
Referred By
ASTM D1900-20 - Standard Practice for Carbon Black—Sampling Bulk Shipments
Effective Date
01-Nov-2015
Referred By
ASTM D561-82(2020) - Standard Specification for Carbon Black Pigment for Paint
Effective Date
01-Nov-2015
Referred By
ASTM D3053-23 - Standard Terminology Relating to Carbon Black
Effective Date
01-Nov-2015
Referred By
ASTM D1619-22 - Standard Test Methods for Carbon Black—Sulfur Content
Effective Date
01-Nov-2015

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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D1509 − 15
Standard Test Methods for
1
Carbon Black—Heating Loss
This standard is issued under the fixed designation D1509; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope 3. Summary of Test Method
3.1 A carbon black sample is weighed before and after
1.1 These test methods cover the determination of the
heatingfor1hat125°C.Theobserveddifferenceinmassisthe
heating loss of carbon black at 125°C. This heating loss
heating loss.
consists primarily of moisture, but other volatile materials may
also be lost. These test methods are not applicable to treated
4. Significance and Use
carbon blacks that contain added volatile materials, if moisture
loss is to be measured.
4.1 In addition to determining the heating loss (primarily
moisture content) of carbon black, these drying conditions are
1.2 These test methods may also be used for the determi-
used to prepare samples prior to performing other carbon black
nation of the heating loss of recovered carbon fillers (rCF/rCB)
tests.
at 125°C. However, these materials were not included in the
precision studies and therefore, the precision statements con-
4.2 When larger samples are prepared for other tests, use an
tained in this standard may not be valid for these materials.
open vessel of suitable dimensions so that the depth of the
black is no more than 10 mm during conditioning.
1.3 The values stated in SI units are to be regarded as the
standard. The values given in parentheses are for information 4.3 Carbon black is hygroscopic. The amount of moisture
only.
absorbed is related to the surface area of the black and to the
relative humidity, ambient temperature, and time to which the
1.4 This standard does not purport to address all of the
material is exposed.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
Method A—Convection–Gravity Oven Method
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use.
5. Apparatus
5.1 Oven, gravity-convection type, capable of temperature
2. Referenced Documents
regulation of within 61°C at 125°C and temperature unifor-
2
2.1 ASTM Standards:
mity within 65°C.
D1799 Practice for Carbon Black—Sampling Packaged
5.2 WeighingBottle, low-form, 30 mm in height and 60 mm
Shipments
in diameter, equipped with a ground-glass stopper.
D1900 Practice for Carbon Black—Sampling Bulk Ship-
ments
5.3 Analytical Balance, having a sensitivity of 0.1 mg.
D4483 Practice for Evaluating Precision for Test Method
5.4 Desiccator.
Standards in the Rubber and Carbon Black Manufacturing
Industries
6. Sampling
6.1 Samples shall be taken in accordance with Practices
D1799 or D1900.
1
These test methods are under the jurisdiction of ASTM Committee D24 on
6.1.1 Place the samples of carbon black in airtight sample
Carbon Black and are the direct responsibility of Subcommittee D24.31 on
Non-Carbon Black Components of Carbon Black. containers.Allow the closed container to reach room tempera-
Current edition approved Nov. 1, 2015. Published December 2015. Originally
ture before starting the test.
approved in 1957. Last previous edition approved in 2012 as D1509 – 95 (2012).
DOI: 10.1520/D1509-15.
2
7. Procedure
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
7.1 Dry the weighing bottle and the stopper, with the
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. stopper removed, in the specified oven set at 125°C for 30 min.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D1509 − 15
Place the bottle and stopper in the desiccator and allow to cool 10.3.2. The precision parameters should not be used for
to room temperature. Weigh the bottle with stopper to the acceptance or rejection testing of any group of materials
nearest 0.1 mg. without documentation that they are applicable to those par-
ticular materials and the specific testing protocols of the test
7.2 Weigh2gofcarbonblackintotheweighingbottletothe
method.
nearest 0.1 mg.
10.3 Convection-Gravity Oven—Test Method A—A Type 1
7.3 Place the weighing bottle, sample, and stopper in the
interlaboratoryprecisionprogramwasconductedin1994.Both
specified oven set at 125°C for 1 h with the stopper removed.
repeatability and
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D1509 − 95 (Reapproved 2012) D1509 − 15
Standard Test Methods for
1
Carbon Black—Heating Loss
This standard is issued under the fixed designation D1509; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope
1.1 These test methods cover the determination of the heating loss of carbon black at 125°C. This heating loss consists primarily
of moisture, but other volatile materials may also be lost. These test methods are not applicable to treated carbon blacks that contain
added volatile materials, if moisture loss is to be measured.
1.2 These test methods may also be used for the determination of the heating loss of recovered carbon fillers (rCF/rCB) at
125°C. However, these materials were not included in the precision studies and therefore, the precision statements contained in
this standard may not be valid for these materials.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D1799 Practice for Carbon Black—Sampling Packaged Shipments
D1900 Practice for Carbon Black—Sampling Bulk Shipments
D4483 Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries
3. Summary of Test Method
3.1 A carbon black sample is weighed before and after heating for 1 h at 125°C. The observed difference in mass is the heating
loss.
4. Significance and Use
4.1 In addition to determining the heating loss (primarily moisture content) of carbon black, these drying conditions are used
to prepare samples prior to performing other carbon black tests.
4.2 When larger samples are prepared for other tests, use an open vessel of suitable dimensions so that the depth of the black
is no more than 10 mm during conditioning.
4.3 Carbon black is hygroscopic. The amount of moisture absorbed is related to the surface area of the black and to the relative
humidity, ambient temperature, and time to which the material is exposed.
Method A—Convection–Gravity Oven Method
5. Apparatus
5.1 Oven, gravity-convection type, capable of temperature regulation of within 61°C at 125°C and temperature uniformity
within 65°C.
1
These test methods are under the jurisdiction of ASTM Committee D24 on Carbon Black and are the direct responsibility of Subcommittee D24.31 on Non-Carbon Black
Components of Carbon Black.
Current edition approved June 1, 2012Nov. 1, 2015. Published November 2012December 2015. Originally approved in 1957. Last previous edition approved in 20072012
as D1509 – 95 (2007).(2012). DOI: 10.1520/D1509-95R12.10.1520/D1509-15.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D1509 − 15
5.2 Weighing Bottle, low-form, 30 mm in height and 60 mm in diameter, equipped with a ground-glass stopper.
5.3 Analytical Balance, having a sensitivity of 0.1 mg.
5.4 Desiccator.
6. Sampling
6.1 Samples shall be taken in accordance with Practices D1799 or D1900.
6.1.1 Place the samples of carbon black in airtight sample containers. Allow the closed container to reach room temperature
before starting the test.
7. Procedure
7.1 Dry the weighing bottle and the stopper, with the stopper removed, in the specified oven set at 125°C for 30 min. Place the
bottle and stopper in the desiccator and allow to cool to room temperature. Weigh the bottle with stopper to the nearest 0.1 mg.
7.2 Weigh 2 g of carbon black into the weighing bottle to the nearest 0.1 mg.
7.3 Place the weighing bottle, sample, and stopper in the specified oven set at 125°C for 1 h with the stopper remov
...

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