Petroleum products - Determination of cloud point - Automated step-wise cooling method (ISO 22995:2019)

This method determines cloud point using a step-wise cooling technique that is executed through automated equipment types with optical detection mode. This method is an alternative to the normal, manual technique as described in EN 23015. It is a generic method that covers existing automated equipment.
The determination method covers distillate fuels (automotive and marine), paraffinic diesel fuel, fatty acid methyl ester and blends thereof at 7% up to 30% in volume.

Mineralölerzeugnisse - Bestimmung des Cloudpoints - Verfahren mit automatischer schrittweiser Abkühlung (ISO 22995:2019)

Dieses Dokument legt ein Verfahren zur Bestimmung des Cloudpoints unter Anwendung eines stufenweisen Abkühlverfahrens fest, die Messung erfolgt dabei durch automatisch arbeitende Geräte mit optischer Detektion.
Das Verfahren gilt für Destillatkraftstoffe, Fettsäure-Methylester (FAME) und paraffinische Dieselkraftstoffe sowie Mischungen aus diesen, ebenso für solche, die Fließverbesserer oder sonstige Additive enthalten, die für die Verwendung in Dieselmotoren und Haushalts-Heizanlagen vorgesehen sind.
Das Verfahren kann auf weitere Produkte, wie z. B. pflanzliche Öle oder Schmierstoffe, angewendet werden, jedoch wurde diese Art von Produkten nicht in dem Ringversuch (en: interlaboratory study, ILS) beurteilt und somit stehen keine Präzisionsdaten zur Verfügung.

Produits pétroliers - Détermination du point de trouble - Méthode automatique par refroidissement par paliers (ISO 22995:2019)

Le présent document spécifie une méthode d'essai qui permet de déterminer, selon un mode de détection optique, le point de trouble de produits qui sont refroidis par paliers successifs au moyen d'un équipement automatisé.
La présente méthode est applicable aux combustibles distillés, aux esters méthyliques d'acides gras (EMAG) et aux carburants diesel paraffiniques, y compris leurs mélanges, ainsi qu'aux combustibles contenant des additifs comme ceux améliorant la fluidité, destinés à être utilisés dans des moteurs diesel et des installations de chauffage domestique.
Cette méthode peut être appliquée à d'autres produits tels que les huiles végétales ou lubrifiants mais ils n'ont pas été évalués lors de l'étude interlaboratoires.

Naftni proizvodi - Ugotavljanje točke zmotnitve - Metoda z avtomatskim stopenjskim ohlajanjem (ISO 22995:2019)

Ta metoda določa točko zmotnitve s tehniko stopenjskega ohlajanja, ki se izvaja prek avtomatiziranih vrst opreme z optičnim načinom zaznavanja. Ta metoda je alternativa običajni ročni tehniki, opisani v standardu EN 23015. Gre za generično metodo, ki zajema obstoječo avtomatizirano opremo.
Metoda določanja zajema destilatna goriva (avtomobilska in pomorska), parafinsko dizelsko gorivo, metil estre maščobnih kislin in njihove mešanice z vsebnostjo od 7 do 30 % vol.

General Information

Status
Published
Public Enquiry End Date
30-Sep-2018
Publication Date
14-Jul-2019
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
19-Jun-2019
Due Date
24-Aug-2019
Completion Date
15-Jul-2019

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SLOVENSKI STANDARD
SIST EN ISO 22995:2019
01-september-2019
Naftni proizvodi - Ugotavljanje točke zmotnitve - Metoda z avtomatskim
stopenjskim ohlajanjem (ISO 22995:2019)
Petroleum products - Determination of cloud point - Automated step-wise cooling method
(ISO 22995:2019)
Mineralölerzeugnisse - Bestimmung des Cloudpoints - Verfahren mit automatischer
schrittweiser Abkühlung (ISO 22995:2019)
Produits pétroliers - Détermination du point de trouble - Méthode automatique par
refroidissement par paliers (ISO 22995:2019)
Ta slovenski standard je istoveten z: EN ISO 22995:2019
ICS:
75.080 Naftni proizvodi na splošno Petroleum products in
general
SIST EN ISO 22995:2019 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 22995:2019

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SIST EN ISO 22995:2019


EN ISO 22995
EUROPEAN STANDARD

NORME EUROPÉENNE

May 2019
EUROPÄISCHE NORM
ICS 75.080
English Version

Petroleum products - Determination of cloud point -
Automated step-wise cooling method (ISO 22995:2019)
Produits pétroliers - Détermination du point de trouble Mineralölerzeugnisse - Bestimmung des Cloudpoints -
- Méthode automatisée par refroidissement par paliers Verfahren mit automatischer schrittweiser Abkühlung
(ISO 22995:2019) (ISO 22995:2019)
This European Standard was approved by CEN on 2 April 2019.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2019 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 22995:2019 E
worldwide for CEN national Members.

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SIST EN ISO 22995:2019
EN ISO 22995:2019 (E)
Contents Page
European foreword . 3

2

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SIST EN ISO 22995:2019
EN ISO 22995:2019 (E)
European foreword
This document (EN ISO 22995:2019) has been prepared by Technical Committee ISO/TC 28 "Petroleum
and related products, fuels and lubricants from natural or synthetic sources" in collaboration with
Technical Committee CEN/TC 19 “Gaseous and liquid fuels, lubricants and related products of
petroleum, synthetic and biological origin.” the secretariat of which is held by NEN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by November 2019, and conflicting national standards
shall be withdrawn at the latest by November 2019.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 22995:2019 has been approved by CEN as EN ISO 22995:2019 without any modification.

3

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SIST EN ISO 22995:2019

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SIST EN ISO 22995:2019
INTERNATIONAL ISO
STANDARD 22995
First edition
2019-04
Petroleum products — Determination
of cloud point — Automated step-wise
cooling method
Produits pétroliers — Détermination du point de trouble — Méthode
automatisée par refroidissement par paliers
Reference number
ISO 22995:2019(E)
©
ISO 2019

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SIST EN ISO 22995:2019
ISO 22995:2019(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2019
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting
on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address
below or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Fax: +41 22 749 09 47
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii © ISO 2019 – All rights reserved

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SIST EN ISO 22995:2019
ISO 22995:2019(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Reagents and materials . 2
6 Apparatus . 2
7 Sampling . 3
8 Sample preparation . 4
9 Preparation of the apparatus . 4
10 Procedure. 4
11 Expression of result . 4
12 Precision . 5
12.1 General . 5
12.2 Repeatability, r . 5
12.3 Reproducibility, R . 5
13 Test report . 5
Bibliography . 6
© ISO 2019 – All rights reserved iii

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SIST EN ISO 22995:2019
ISO 22995:2019(E)

Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as
...

SLOVENSKI STANDARD
oSIST prEN ISO 22995:2018
01-september-2018
1DIWQLSURL]YRGL'RORþHYDQMHPRWQLãþD0HWRGDDYWRPDWVNHJDVWRSHQMVNHJD
RKODMDQMD ,62',6
Petroleum products - Determination of cloud point - Automated step-wise cooling method
(ISO/DIS 22995:2018)
Mineralölerzeugnisse - Bestimmung des Cloudpoints - Verfahren mit automatischer
schrittweiser Abkühlung (ISO/DIS 22995:2018)
Produits pétroliers - Détermination du point de trouble - Méthode automatique par
refroidissement par palier (ISO/DIS 22995:2018)
Ta slovenski standard je istoveten z: prEN ISO 22995
ICS:
75.080 Naftni proizvodi na splošno Petroleum products in
general
oSIST prEN ISO 22995:2018 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
oSIST prEN ISO 22995:2018

---------------------- Page: 2 ----------------------
oSIST prEN ISO 22995:2018
DRAFT INTERNATIONAL STANDARD
ISO/DIS 22995
ISO/TC 28 Secretariat: NEN
Voting begins on: Voting terminates on:
2018-05-21 2018-08-13
Petroleum products — Determination of cloud point —
Automatic step-wise cooling method
Produits pétroliers — Détermination du point de trouble — Méthode automatique par refroidissement
par palier
ICS: 75.080
THIS DOCUMENT IS A DRAFT CIRCULATED
This document is circulated as received from the committee secretariat.
FOR COMMENT AND APPROVAL. IT IS
THEREFORE SUBJECT TO CHANGE AND MAY
NOT BE REFERRED TO AS AN INTERNATIONAL
STANDARD UNTIL PUBLISHED AS SUCH.
IN ADDITION TO THEIR EVALUATION AS
ISO/CEN PARALLEL PROCESSING
BEING ACCEPTABLE FOR INDUSTRIAL,
TECHNOLOGICAL, COMMERCIAL AND
USER PURPOSES, DRAFT INTERNATIONAL
STANDARDS MAY ON OCCASION HAVE TO
BE CONSIDERED IN THE LIGHT OF THEIR
POTENTIAL TO BECOME STANDARDS TO
WHICH REFERENCE MAY BE MADE IN
Reference number
NATIONAL REGULATIONS.
ISO/DIS 22995:2018(E)
RECIPIENTS OF THIS DRAFT ARE INVITED
TO SUBMIT, WITH THEIR COMMENTS,
NOTIFICATION OF ANY RELEVANT PATENT
RIGHTS OF WHICH THEY ARE AWARE AND TO
©
PROVIDE SUPPORTING DOCUMENTATION. ISO 2018

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oSIST prEN ISO 22995:2018
ISO/DIS 22995:2018(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2018
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting
on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address
below or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Fax: +41 22 749 09 47
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii © ISO 2018 – All rights reserved

---------------------- Page: 4 ----------------------
oSIST prEN ISO 22995:2018
ISO/DIS 22995:2018(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Reagents and material . 2
6 Apparatus . 2
7 Sampling . 3
8 Sample preparation . 4
9 Preparation of the apparatus . 4
10 Procedure. 4
11 Expression of result . 4
12 Precision . 5
12.1 General . 5
12.2 Repeatability, r .5
12.3 Reproducibility, R .5
13 Test report . 5
Bibliography . 6
© ISO 2018 – All rights reserved iii

---------------------- Page: 5 ----------------------
oSIST prEN ISO 22995:2018
ISO/DIS 22995:2018(E)

Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/ patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation on the meaning of ISO specific terms and expressions related to conformity assessment,
as well as information about ISO's adherence to the World Trade Organization (WTO) principles in the
Technical Barriers to Trade (TBT) see the following URL: www .iso .org/ iso/ foreword .html.
The committee responsible for this document is CEN/TC 19 “Gaseous and liquid fuels, lubricants and
related products of petroleum, synthetic and biological origin”, the secretariat of which is held by NEN.
iv © ISO 2018 – All rights reserved

---------------------- Page: 6 ----------------------
oSIST prEN ISO 22995:2018
ISO/DIS 22995:2018(E)

Introduction
This document describes an automatic method for the determination of the cloud point, inspired by
[1]
the manual determination technique described in ISO 3015 . In comparison with that standard, the
scope of the present document has been modified for taking into account FAME, current available
distillate fuels as well as paraffinic diesel fuels, including those containing FAME, flow-improvers or
other additives, intended for use in diesel engines and domestic heating installation
© ISO 2018 – All rights reserved v

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oSIST prEN ISO 22995:2018

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oSIST prEN ISO 22995:2018
DRAFT INTERNA
...

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