Photography - Processing chemicals - Specifications for sodium tetraborate decahydrate

Cancels and replaces the first edition (1976). Establishes criteria for the purity of photographic-grade sodium tetraborate decahydrat and specifies the tests to be used to determine the purity.

Photographie — Produits chimiques de traitement — Spécifications relatives au tétraborate de sodium décahydraté

General Information

Status
Published
Publication Date
07-Dec-1994
Technical Committee
ISO/TC 42 - Photography
Drafting Committee
ISO/TC 42 - Photography
Current Stage
9093 - International Standard confirmed
Start Date
05-Jun-2021
Completion Date
13-Dec-2025

Relations

Effective Date
15-Apr-2008

Overview

ISO 3621:1994 - Photography - Processing chemicals - Specifications for sodium tetraborate decahydrate - defines purity criteria and test methods for photographic‑grade sodium tetraborate decahydrate (Na2B4O7·10H2O). This second edition (1994) cancels and replaces the 1976 edition and is part of a series of ISO standards that set minimum quality and analytical requirements for photographic chemicals used in film and paper processing.

Key topics and requirements

  • Scope and intent: Establishes chemical and physical requirements that correlate with undesirable photographic effects; tests are performed on samples “as received.”
  • Physical form & storage:
    • White crystalline powder or granules; relative molecular mass 381.37.
    • Store in a closed container at room temperature.
  • Mandatory purity limits (summary from Table 1):
    • Assay (Na2B4O7·10H2O): ≥ 99.0% (m/m)
    • Heavy metals (as Pb): ≤ 0.002% (m/m)
    • Iron (Fe): ≤ 0.003% (m/m)
    • pH (20 °C): 9.14 – 9.34
    • Reaction to ammoniacal silver nitrate: To pass test
    • Appearance of 20 g/L solution: Clear and free from insoluble matter except for slight flocculence
  • Analytical methods:
    • Assay based on a 20 g/L test solution and titration procedures (mannitol reaction and NaOH titration) using standardized reagents and apparatus.
    • Heavy metals and iron determinations follow ISO 10349‑5 procedures.
    • Reaction to ammoniacal silver nitrate follows ISO 10349‑9.
    • pH measurement requires a calibrated electronic pH‑meter at 20 °C.
  • Safety and laboratory practice: Uses potentially caustic/toxic reagents; follow ISO 10349‑1 guidance and standard laboratory safety (glasses, gloves, ventilation).

Applications and users

ISO 3621:1994 is intended for:

  • Photographic chemical manufacturers and suppliers for product specification and quality control.
  • Analytical and quality assurance laboratories performing acceptance testing of photographic-grade chemicals.
  • Photographic processors and film/paper manufacturers seeking materials that will not impair photographic processing or image quality.
  • Regulators and procurement teams specifying minimum purity for processing chemicals.

Practical benefits include ensuring consistent processing performance, minimizing image defects caused by impurities, and simplifying supplier acceptance testing.

Related standards

  • ISO 10349‑1:1992 - General test methods and safety/hazard symbols
  • ISO 10349‑5:1992 - Determination of heavy metals and iron content
  • ISO 10349‑9:1992 - Reaction to ammoniacal silver nitrate

Keywords: ISO 3621, sodium tetraborate decahydrate, photographic chemicals, purity specification, assay, heavy metals, pH, ISO 10349.

Standard

ISO 3621:1994 - Photography -- Processing chemicals -- Specifications for sodium tetraborate decahydrate

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Frequently Asked Questions

ISO 3621:1994 is a standard published by the International Organization for Standardization (ISO). Its full title is "Photography - Processing chemicals - Specifications for sodium tetraborate decahydrate". This standard covers: Cancels and replaces the first edition (1976). Establishes criteria for the purity of photographic-grade sodium tetraborate decahydrat and specifies the tests to be used to determine the purity.

Cancels and replaces the first edition (1976). Establishes criteria for the purity of photographic-grade sodium tetraborate decahydrat and specifies the tests to be used to determine the purity.

ISO 3621:1994 is classified under the following ICS (International Classification for Standards) categories: 37.040.30 - Photographic chemicals. The ICS classification helps identify the subject area and facilitates finding related standards.

ISO 3621:1994 has the following relationships with other standards: It is inter standard links to ISO 3621:1976. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

You can purchase ISO 3621:1994 directly from iTeh Standards. The document is available in PDF format and is delivered instantly after payment. Add the standard to your cart and complete the secure checkout process. iTeh Standards is an authorized distributor of ISO standards.

Standards Content (Sample)


INTERNATIONAL
STANDARD
Second edition
1994-12-15
Photography - Processing chemicals -
Specifications for sodium tetraborate
decahydrate
Photographie - Produits chimiques de traitement - Spkifications relatives au
tktraborate de sodium d&ahydrat&
Reference nufnber
Foreword
ISO (the International Organization for Standardization) is a worldwide
federation of national Standards bodies (ISO member bodies). The work of
preparing International Standards is normally carried out through ISO
technical committees. Esch member body interested in a subject for which
a technical committee has been established has the right to be
represented on that committee. International organizations, governmental
and non-governmental, in liaison with ISO, also take part in the work. ISO 1
collaborates closely with the International Electrotechnical Commission
(IEC) on all matters of electrotechnical standardization.
Draft International Standards adopted by the technical committees are
circulated to the member bodies for voting. Publication as an International
Standard requires approval by at least 75 % sf the member bodies casting
a vote.
International Standard ISO 3621 was prepared by Technical Committee
ISOfIC 42, Photography.
This second edition cancels and replaces the first edition (ISO 3621:1976),
which has been technically revised.
0 ISO 1994
AH rights reserved. Unless otherwise specified, no part of this publication mag/ be reproduced
utilized in any form or by an)g means, electronie or mecha nical, rncluding photocopytng and
0r
mi crof ilm, wlthout permlssi on in writing from the publisher.
International Organization for Standar ,dization
Gase postale 56 0 CH-1 2 11 Geneve 20 0 SwitzerCand
Pnnted in Switzerland
0 ISO
Introduction
0.1 This International Standard is one of a series that establishes criteria
of purity for chemicals used in processing photographic materials. General
test methods and procedures cited in this International Standard are
compiled in Parts 1, 5 and 9 of ISO 10349.
This International Standard is intended for use by individuals with a
working knowledge of analytical techniques, which may not always be the
case. Some of the procedures utilize caustic, toxic or otherwise hazardous
chemicals. Safe laboratory practice for the handling of chemicals requires
the use of safety glasses or goggles, rubber gloves and other protective
apparel such as face masks or aprons where appropriate. Normal pre-
cautions required in the Performance of any Chemical procedure are to be
exercised at all times but care has been taken to provide warnings for
hazardous materials. Hazard warnings designated by a letter enclosed in
angle brackets, < >, are used as a reminder in those Steps detailing
handling operations and are defined in ISO 10349-1. More detailed
information regarding hazards, handling and use of these chemicals may
be available from the manufacturer.
0.2 This International Standard provides Chemical and physical require-
ments for the suitability of a photographit-grade Chemical. The tests
correlate with undesirable photographic effects. Purity requirements are
set as low as possible consistent with these photographic effects. These
criteria are considered the minimum requirements necessary to assure
sufficient purity for use in photographic processing solutions, except that if
the purity of a commonly available grade of Chemical exceeds photographic
processing requirements and if there is no economic penalty in its use, the
purity requirements have been set to take advantage of the availability of
the higher-quality material. Every effort has been made to keep the
number of requirements to a minimum. Inert impurities are limited to
amounts which will not unduly reduce the assay. All tests are performed
on samples “as received” to reflect the condition of materials furnished for
use. Although the ultimate criterion for suitability of such a Chemical is its
successful Performance in an appropriate use test, the shorter, more
economical test methods described in this International Standard are
generally adequate.
Assay procedures have been included in all cases where a satisfactory
method is available. An effective assay requirement serves not only as a
safeguard of Chemical purity but also as a valuable complement to the
identity test. Identity tests have been included whenever a possibility
exists that another Chemical or mixture of chemicals could pass the other
tests.
All requirements listed in clause 4 are mandatory. The physical appearance
of the material and any footnotes are for general information only and are
not part of the requirements.
. . .
Ill
0.3 Efforts have been made to employ tests which are capable of being
run in any normally equipped laboratory and, wherever possible, to avoid
tests which require highly specialized equipment or techniques.
Instrumental methods have been specified only as alternative methods or
alone in those cases where no other satisfactory method is available.
Over the past few years, great improvements have been made in
instrumentation for various analyses. Where such techniques have
equivalent or greater precision, they may be used in place of the tests
described in this International Standard. Correlation of such alternative
procedures with the given method is the responsibility of the User. In case
of disagreement in results, the method called for in the specification shall
prevail. Where a requirement states Yo pass test ”, however, alternative
methods shall not be used.
INTERNATIONAL STANDARD o Iso ISO 3621:1994(E)
Processing chemicals - Specifications for
Photography -
sodium tetraborate decahydrate
ISO 10349-9: 1992, Photograph y - Photographic-
1 Scope
grade chemicals - Test methods - Part 9: Reaction
This International Standard establishes criteria for the
to ammoniacal silver nitra te.
purity of photographit-grade sodium tetraborate deca-
hydrate and specifies the tests to be used to deter-
mine the purity.
3 General
3.1 Physical proper-Ges
2 Normative references
Sodium tetraborate decahydrate, Na2B407.1 OH*O,
exists as either a white crystalline powder or
The following Standards contain provisions which,
granules. lt has a relative molecular mass of 381,37.
through reference in this text, constitute provisions of
this International Standard. At the time of publication,
the editions indicated were valid. All Standards are
3.2 Hazardous properties
subject to revision, and Parties to agreements based
on this International Standard are encouraged to
Sodium tetraborate decahydrate is not hazardous
investigate the possib
...

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