Liquid petroleum products - Unleaded petrol - Determination of organic oxygenate compounds and total organically bound oxygen content by gas chromatography using column switching

This European Standard specifies a gas chromatographic method using column switching for the quantitative determination of individual organic oxygenate compounds in the range  0,17 % (m/m) to 15 % (m/m) and total organically bound oxygen up 3,7 % (m/m) in unleaded petrol having a final boiling point not greater than 220° C. NOTE 1: The final boiling point can be measured by using prEN ISO 3405:1998. NOTE 2: For the purposes of this European Standard, the terms "% (m/m)" and "% (V/V)" are used to represent respectively the mass fraction and the volume fraction.

Flüssige Mineralölerzeugnisse - Unverbleite Ottokraftstoffe - Bestimmung sauerstoffhaltiger organischer Verbindungen und des Gesamtgehaltes an organisch gebundenem Sauerstoff mittels Gaschromatographie mit Säulenschaltung

Diese Europäische Norm legt ein Gaschromatographie-Verfahren mit Säulenschaltung zur Bestimmung einzelner organischer sauerstoffhaltiger Bestandteile im Bereich zwischen 0,17% (m/m) und 15 % (m/m) und des Gesamtgehaltes an organisch gebundenem Sauerstoff oberhalb 3,7% (m/m) in unverbleitem Kraftstoff mit einem Siedeendpunkt nicht über 220 °C fest.
ANMERKUNG 1   Der Siedeendpunkt kann mit prEN ISO 3405:1998  gemessen werden.
ANMERKUNG 2   Für die Zwecke dieser Europäischen Norm werden die Begriffe ¿% (m/m)" und ¿%  (V/V)" verwendet, um den Massenanteil respektive den Volumenanteil darzustellen.
Diese Europäische Norm ist anwendbar zur Bestimmung der sauerstoffhaltigen Bestandteile und des Gesamtgehaltes an organisch gebundenem Sauerstoff in unverbleitem Kraftstoff in Übereinstimmung mit den relevanten EU-Richtlinien.
WARNHINWEIS - Die Anwendung dieser Norm kann verbunden sein mit gefährlichen Materialien,Verfahrensweisen und Geräten. Es ist nicht Zweck dieser Norm, alle mit ihrer Anwendung verbundenen Sicherheitsprobleme anzusprechen. Es liegt in der Verantwortlichkeit des Anwenders dieser Norm, vorab angemessene Vorkehrungen hinsichtlich Sicherheit und Gesundheit zu treffen und die Anwendung regulatorischer Einschränkungen zu bestimmen.

Produits pétroliers liquides - Essence sans plomb - Détermination des composés oxygénés organiques et de la teneur totale en oxygène organique par chromatographie en phase gazeuse avec commutation de colonnes

La présente norme européenne prescrit une méthode de chromatographie en phase gazeuse avec commutation de colonne, pour le dosage des composés organiques oxygénés dans le domaine 0,17 % (m/m) à 15 % (m/m) et de l'oxygène total organiquement lié à une teneur maximale de 3,7 % (m/m) dans des essences sans plomb ayant un point d'ébullition final inférieur à 220 °C. NOTE 1: Le point final d'ébullition peut être mesuré en utilisant le prEN ISO 3405:1998. NOTE 2: Pour les besoins de la présente norme européenne, les expressions "% (m/m)" et "% (v/v)" sont utilisées pour désigner respectivement les fractions massiques et les fraction....

Tekoči naftni proizvodi - Neosvinčeni motorni bencin - Določevanje organskih kisikovih spojin in celotnega organsko vezanega kisika s plinsko kromatografijo s preklopom kolon

General Information

Status
Published
Publication Date
21-Mar-2000
Withdrawal Date
29-Sep-2000
ICS
75.160.20 - Liquid fuels
Technical Committee
CEN/TC 19 - Petroleum products, lubricants and related products
Drafting Committee
CEN/TC 19/WG 9 - Chromatographic test methods
Current Stage
9093 - Decision to confirm - Review Enquiry
Start Date
12-Apr-2021
Completion Date
14-Apr-2025
Ref Project
SIST EN 13132:2000 - Liquid petroleum products - Unleaded petrol - Determination of organic oxygenate compounds and total organically bound oxygen content by gas chromatography using column switching

Overview

EN 13132:2000 is a CEN European Standard for analysis of liquid petroleum products (unleaded petrol). It specifies a gas chromatographic method using column switching to quantify individual organic oxygenate compounds (such as alcohols and ethers used as petrol oxygenates) and to determine total organically bound oxygen in petrol. The method applies to samples with a final boiling point not greater than 220 °C and reports concentrations in mass or volume fractions.

Key topics and requirements

  • Analytical technique: Gas chromatography (GC) with column switching to separate and quantify organic oxygenates.
  • Quantitative ranges: Individual organic oxygenates measured from 0.17 % (m/m) to 15 % (m/m).
  • Total organically bound oxygen: Determination up to 3.7 % (m/m).
  • Sample scope: Unleaded petrol with a final boiling point ≤ 220 °C (final boiling point can be measured per prEN ISO 3405:1998).
  • Units and notation: The standard clarifies "% (m/m)" as mass fraction and "% (V/V)" as volume fraction.
  • Method focus: Accurate separation and quantification of oxygen-containing additives and contaminants in petrol blends using column switching to improve resolution and analytical throughput.

Applications

EN 13132:2000 is intended for practical use in:

  • Fuel quality control laboratories verifying oxygenate content in unleaded petrol.
  • Refineries and blending terminals monitoring additive concentrations during formulation and shipment.
  • Regulatory and conformity testing where limits on oxygenates or total organically bound oxygen are specified.
  • Environmental and emission testing groups assessing oxygenate-related impacts on combustion and emissions.
  • Standards bodies and certification agencies that need a harmonized GC procedure for inter-laboratory comparability.

Practical benefits include reliable quantification of common petrol oxygenates, support for compliance with fuel specifications, and improved confidence in blending and quality decisions.

Related standards

  • prEN ISO 3405:1998 - referenced for final boiling point determination of petrol samples.

Keywords: EN 13132:2000, unleaded petrol, organic oxygenates, organically bound oxygen, gas chromatography, column switching, fuel analysis, petroleum products standard, CEN.

Frequently Asked Questions

EN 13132:2000 is a standard published by the European Committee for Standardization (CEN). Its full title is "Liquid petroleum products - Unleaded petrol - Determination of organic oxygenate compounds and total organically bound oxygen content by gas chromatography using column switching". This standard covers: This European Standard specifies a gas chromatographic method using column switching for the quantitative determination of individual organic oxygenate compounds in the range 0,17 % (m/m) to 15 % (m/m) and total organically bound oxygen up 3,7 % (m/m) in unleaded petrol having a final boiling point not greater than 220° C. NOTE 1: The final boiling point can be measured by using prEN ISO 3405:1998. NOTE 2: For the purposes of this European Standard, the terms "% (m/m)" and "% (V/V)" are used to represent respectively the mass fraction and the volume fraction.

This European Standard specifies a gas chromatographic method using column switching for the quantitative determination of individual organic oxygenate compounds in the range 0,17 % (m/m) to 15 % (m/m) and total organically bound oxygen up 3,7 % (m/m) in unleaded petrol having a final boiling point not greater than 220° C. NOTE 1: The final boiling point can be measured by using prEN ISO 3405:1998. NOTE 2: For the purposes of this European Standard, the terms "% (m/m)" and "% (V/V)" are used to represent respectively the mass fraction and the volume fraction.

EN 13132:2000 is classified under the following ICS (International Classification for Standards) categories: 75.160.20 - Liquid fuels. The ICS classification helps identify the subject area and facilitates finding related standards.

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Standards Content (Sample)


2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Flüssige Mineralölerzeugnisse - Unverbleite Ottokraftstoffe - Bestimmung sauerstoffhaltiger organischer Verbindungen und des Gesamtgehaltes an organisch gebundenem Sauerstoff mittels Gaschromatographie mit SäulenschaltungProduits pétroliers liquides - Essence sans plomb - Détermination des composés oxygénés organiques et de la teneur totale en oxygene organique par chromatographie en phase gazeuse avec commutation de colonnesLiquid petroleum products - Unleaded petrol - Determination of organic oxygenate compounds and total organically bound oxygen content
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이 기사는 EN 13132:2000이라는 유럽 표준에 대해 논의하며, 여기에는 컬럼 전환을 사용한 가스 크로마토그래피 방법을 통해 무연 휘발유에서 개별 유기 산소 화합물의 양적 결정 및 총 유기 결합 산소 함량을 측정할 수 있다. 이 방법은 무연 휘발유에서 0.17%에서 15%까지의 개별 유기 산소 화합물 및 최대 3.7%의 총 유기 결합 산소 함량을 계량화하는 데 사용될 수 있다. 이 표준은 "% (m/m)"이 질량 분율을 나타내고, "% (V/V)"이 체적 분율을 나타내는 것을 명확히하고 있다. 휘발유의 최종 끓는점은 prEN ISO 3405:1998이라는 다른 표준을 사용하여 측정할 수 있다는 것도 언급되어 있다.

The article discusses a European standard, EN 13132:2000, which outlines a gas chromatographic method using column switching for determining the levels of organic oxygenate compounds in unleaded petrol. The method can be used to quantify individual organic oxygenate compounds ranging from 0.17% to 15% and the total organically bound oxygen content up to 3.7%. The standard also clarifies that "% (m/m)" represents the mass fraction and "% (V/V)" represents the volume fraction. It is noted that the final boiling point of the petrol can be measured using a different standard, prEN ISO 3405:1998.

この記事では、EN 13132:2000というヨーロッパの標準について説明しています。この規格では、カラムスイッチを使用したガスクロマトグラフィー法を用いて、無鉛ガソリン中の個々の有機酸素化合物の定量的な測定ができます。測定範囲は、個々の有機酸素化合物が0.17％から15％の間で、また総有機酸素結合含有量が最大3.7％までです。本標準では、"% (m/m)"が質量分率を表し、"% (V/V)"が体積分率を表すことも明記されています。また、ガソリンの最終沸点は、別の規格であるprEN ISO 3405:1998を使用して測定することができることも注記されています。