Standard Guide for Radiographic Examination Using Industrial Radiographic Film

SIGNIFICANCE AND USE
4.1 Within the present state of the radiographic art, this guide is generally applicable to available materials, processes, and techniques where industrial radiographic films are used as the recording media.  
4.2 Limitations—This guide does not take into consideration the benefits and limitations of nonfilm radiography such as radioscopy, digital detector arrays, or computed radiography. Refer to Guides E1000, E2736, and E2007.  
4.3 Although reference is made to documents that may be used in the identification and grading, where applicable, of representative discontinuities in common metal castings and welds, no attempt has been made to set standards of acceptance for any material or production process.  
4.4 Radiography will be consistent in image quality (contrast sensitivity and definition) only if all details of techniques, such as geometry, film, filtration, viewing, etc., are obtained and maintained.
SCOPE
1.1 This guide2 covers satisfactory X-ray and gamma-ray radiographic examination as applied to industrial radiographic film recording. It includes statements about preferred practice without discussing the technical background which justifies the preference. A bibliography of several textbooks and standard documents of other societies is included for additional information on the subject.  
1.2 This guide covers types of materials to be examined; radiographic examination techniques and production methods; radiographic film selection, processing, viewing, and storage; maintenance of inspection records; and a list of available reference radiograph documents.  
Note 1: Further information is contained in Guide E999, Practice E1025, Practice E1030/E1030M, and Practice E1032.  
1.3 The use of digital radiography has expanded and follows many of the same general principles of film based radiography but with many important differences. The user is referred to standards for digital radiography [E2597, E2698, E2736, and E2737 for digital detector array (DDA) radiography and E2007, E2033, E2445/E2445M, and E2446 for computed radiography(CR)] if considering the use of digital radiography.  
1.4 Interpretation and Acceptance Standards—Interpretation and acceptance standards are not covered by this guide, beyond listing the available reference radiograph documents for castings and welds. Designation of accept - reject standards is recognized to be within the cognizance of product specifications and generally a matter of contractual agreement between producer and purchaser.  
1.5 Safety Practices—Problems of personnel protection against X-rays and gamma-rays are not covered by this guide. For information on this important aspect of radiography, reference should be made to the current document of the National Committee on Radiation Protection and Measurement, Federal Register, U.S. Energy Research and Development Administration, National Bureau of Standards, and to state and local regulations, if such exist. For specific radiation safety information, refer to NIST Handbook ANSI 43.3, 21 CFR 1020.40, and 29 CFR 1910.1096 or state regulations for agreement states.  
1.6 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system should be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.7 If an NDT agency is used, the agency should be qualified in accordance with Specification E543.  
1.8 Personnel Qualification—If specified in the contractual agreement, personnel performing examinations to this guide should be qualified in accordance with a nationally or internationally recognized NDT personnel qualification practice or standard and certified by the employer or certifying agency, as applicable.  
1.9 This standard does not purport to address all of the safety problems, if any, assoc...

General Information

Status
Published
Publication Date
30-Nov-2022
Technical Committee
E07 - Nondestructive Testing

Relations

Effective Date
01-Feb-2024
Effective Date
15-Dec-2023
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01-Dec-2023
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01-Dec-2019
Effective Date
01-Dec-2019
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01-Mar-2019
Effective Date
01-Feb-2019
Effective Date
15-Jun-2018
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01-Mar-2018
Effective Date
01-Feb-2018
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01-Feb-2018
Effective Date
01-Feb-2018
Effective Date
01-Feb-2018
Effective Date
01-Jan-2018
Effective Date
01-Nov-2017

Overview

ASTM E94/E94M-22: Standard Guide for Radiographic Examination Using Industrial Radiographic Film provides comprehensive guidance for performing X-ray and gamma-ray radiographic examinations with industrial radiographic film. Issued by ASTM International, this standard is widely recognized for helping organizations achieve consistency and quality in nondestructive testing (NDT) using film-based radiographic techniques.

This guide focuses on the use of industrial radiographic film as the recording medium for examining various materials and components. It outlines preferred practices but does not set acceptance criteria for materials or define safety guidelines for radiation protection. Instead, it provides a foundation for optimal radiographic process design, film handling, technique documentation, and interpretation of results.

Key Topics

1. Radiographic Techniques and Image Quality

  • Guidance on selecting X-ray or gamma sources based on material types and thickness
  • Recommendations for source-to-film and object-to-film distances to achieve optimal image quality
  • Use of image quality indicators (IQIs) for assessing radiographic sensitivity and definition
  • Importance of geometric arrangements, filtration, and scatter reduction

2. Film Selection, Processing, and Storage

  • Considerations in selecting appropriate film class based on required radiographic quality and production needs
  • Best practices for film processing to ensure consistent contrast and minimal granularity
  • Guidance on proper handling and storage of exposed and unexposed industrial radiographic films to preserve image integrity

3. Documentation and Records

  • Maintenance of accurate inspection records including technique logs detailing parameters such as source, material, distances, and markers
  • The role of technique files in ensuring traceability, repeatability, and effective communication between radiographic operators and interpreters

4. Limitations and Safety

  • Excludes digital radiography methods (such as computed radiography or digital detector arrays); references other ASTM standards for those applications
  • Does not address safety practices related to radiation protection-users must consult regulatory requirements and dedicated safety standards

Applications

The ASTM E94/E94M-22 standard is a critical reference for industries where industrial radiography is used as a nondestructive examination method. Typical applications include:

  • Inspection of metal castings and welds: Detect internal discontinuities such as voids, cracks, or inclusions
  • Quality assurance in manufacturing: Validate the integrity of critical structural components in aerospace, automotive, power generation, and construction
  • Maintenance and continued service assessment: Evaluate fatigue, corrosion, or degradation in existing infrastructure
  • Documentation of radiographic evidence: Maintain objective, traceable inspection records for regulatory, contractual, and quality audits

By following the practices outlined in ASTM E94/E94M-22, organizations can enhance the reliability, repeatability, and credibility of their radiographic inspection processes, while facilitating communication and contractual agreements between producers and purchasers.

Related Standards

For users requiring more detailed procedures or coverage of digital techniques, ASTM E94/E94M-22 lists numerous related standards, including:

  • ASTM E999 – Guide for Controlling the Quality of Industrial Radiographic Film Processing
  • ASTM E1025 – Practice for Design and Manufacture of Hole-Type Image Quality Indicators (IQI)
  • ASTM E1030/E1030M – Practice for Radiographic Examination of Metallic Castings
  • ASTM E1032 – Practice for Radiographic Examination of Weldments Using Industrial X-Ray Film
  • ASTM E2007 – Guide for Computed Radiography
  • ASTM E2736 – Guide for Digital Detector Array Radiography
  • ASTM E1815 – Test Method for Classification of Film Systems for Industrial Radiography

Professionals are encouraged to consult these and other referenced documents to address specific needs in nondestructive testing and to ensure compliance with local, national, and international requirements.

Keywords: industrial radiographic film, radiographic examination, nondestructive testing, ASTM E94/E94M-22, X-ray radiography, gamma-ray inspection, image quality indicators, film processing, radiographic technique documentation, NDT standards

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Frequently Asked Questions

ASTM E94/E94M-22 is a guide published by ASTM International. Its full title is "Standard Guide for Radiographic Examination Using Industrial Radiographic Film". This standard covers: SIGNIFICANCE AND USE 4.1 Within the present state of the radiographic art, this guide is generally applicable to available materials, processes, and techniques where industrial radiographic films are used as the recording media. 4.2 Limitations—This guide does not take into consideration the benefits and limitations of nonfilm radiography such as radioscopy, digital detector arrays, or computed radiography. Refer to Guides E1000, E2736, and E2007. 4.3 Although reference is made to documents that may be used in the identification and grading, where applicable, of representative discontinuities in common metal castings and welds, no attempt has been made to set standards of acceptance for any material or production process. 4.4 Radiography will be consistent in image quality (contrast sensitivity and definition) only if all details of techniques, such as geometry, film, filtration, viewing, etc., are obtained and maintained. SCOPE 1.1 This guide2 covers satisfactory X-ray and gamma-ray radiographic examination as applied to industrial radiographic film recording. It includes statements about preferred practice without discussing the technical background which justifies the preference. A bibliography of several textbooks and standard documents of other societies is included for additional information on the subject. 1.2 This guide covers types of materials to be examined; radiographic examination techniques and production methods; radiographic film selection, processing, viewing, and storage; maintenance of inspection records; and a list of available reference radiograph documents. Note 1: Further information is contained in Guide E999, Practice E1025, Practice E1030/E1030M, and Practice E1032. 1.3 The use of digital radiography has expanded and follows many of the same general principles of film based radiography but with many important differences. The user is referred to standards for digital radiography [E2597, E2698, E2736, and E2737 for digital detector array (DDA) radiography and E2007, E2033, E2445/E2445M, and E2446 for computed radiography(CR)] if considering the use of digital radiography. 1.4 Interpretation and Acceptance Standards—Interpretation and acceptance standards are not covered by this guide, beyond listing the available reference radiograph documents for castings and welds. Designation of accept - reject standards is recognized to be within the cognizance of product specifications and generally a matter of contractual agreement between producer and purchaser. 1.5 Safety Practices—Problems of personnel protection against X-rays and gamma-rays are not covered by this guide. For information on this important aspect of radiography, reference should be made to the current document of the National Committee on Radiation Protection and Measurement, Federal Register, U.S. Energy Research and Development Administration, National Bureau of Standards, and to state and local regulations, if such exist. For specific radiation safety information, refer to NIST Handbook ANSI 43.3, 21 CFR 1020.40, and 29 CFR 1910.1096 or state regulations for agreement states. 1.6 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system should be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. 1.7 If an NDT agency is used, the agency should be qualified in accordance with Specification E543. 1.8 Personnel Qualification—If specified in the contractual agreement, personnel performing examinations to this guide should be qualified in accordance with a nationally or internationally recognized NDT personnel qualification practice or standard and certified by the employer or certifying agency, as applicable. 1.9 This standard does not purport to address all of the safety problems, if any, assoc...

SIGNIFICANCE AND USE 4.1 Within the present state of the radiographic art, this guide is generally applicable to available materials, processes, and techniques where industrial radiographic films are used as the recording media. 4.2 Limitations—This guide does not take into consideration the benefits and limitations of nonfilm radiography such as radioscopy, digital detector arrays, or computed radiography. Refer to Guides E1000, E2736, and E2007. 4.3 Although reference is made to documents that may be used in the identification and grading, where applicable, of representative discontinuities in common metal castings and welds, no attempt has been made to set standards of acceptance for any material or production process. 4.4 Radiography will be consistent in image quality (contrast sensitivity and definition) only if all details of techniques, such as geometry, film, filtration, viewing, etc., are obtained and maintained. SCOPE 1.1 This guide2 covers satisfactory X-ray and gamma-ray radiographic examination as applied to industrial radiographic film recording. It includes statements about preferred practice without discussing the technical background which justifies the preference. A bibliography of several textbooks and standard documents of other societies is included for additional information on the subject. 1.2 This guide covers types of materials to be examined; radiographic examination techniques and production methods; radiographic film selection, processing, viewing, and storage; maintenance of inspection records; and a list of available reference radiograph documents. Note 1: Further information is contained in Guide E999, Practice E1025, Practice E1030/E1030M, and Practice E1032. 1.3 The use of digital radiography has expanded and follows many of the same general principles of film based radiography but with many important differences. The user is referred to standards for digital radiography [E2597, E2698, E2736, and E2737 for digital detector array (DDA) radiography and E2007, E2033, E2445/E2445M, and E2446 for computed radiography(CR)] if considering the use of digital radiography. 1.4 Interpretation and Acceptance Standards—Interpretation and acceptance standards are not covered by this guide, beyond listing the available reference radiograph documents for castings and welds. Designation of accept - reject standards is recognized to be within the cognizance of product specifications and generally a matter of contractual agreement between producer and purchaser. 1.5 Safety Practices—Problems of personnel protection against X-rays and gamma-rays are not covered by this guide. For information on this important aspect of radiography, reference should be made to the current document of the National Committee on Radiation Protection and Measurement, Federal Register, U.S. Energy Research and Development Administration, National Bureau of Standards, and to state and local regulations, if such exist. For specific radiation safety information, refer to NIST Handbook ANSI 43.3, 21 CFR 1020.40, and 29 CFR 1910.1096 or state regulations for agreement states. 1.6 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system should be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. 1.7 If an NDT agency is used, the agency should be qualified in accordance with Specification E543. 1.8 Personnel Qualification—If specified in the contractual agreement, personnel performing examinations to this guide should be qualified in accordance with a nationally or internationally recognized NDT personnel qualification practice or standard and certified by the employer or certifying agency, as applicable. 1.9 This standard does not purport to address all of the safety problems, if any, assoc...

ASTM E94/E94M-22 is classified under the following ICS (International Classification for Standards) categories: 77.040.20 - Non-destructive testing of metals. The ICS classification helps identify the subject area and facilitates finding related standards.

ASTM E94/E94M-22 has the following relationships with other standards: It is inter standard links to ASTM E1316-24, ASTM E1742/E1742M-23, ASTM E746-23, ASTM E1316-19b, ASTM E1735-19, ASTM E1316-19, ASTM E1032-19, ASTM E3169-18, ASTM E1742/E1742M-18, ASTM E2903-18, ASTM E746-18, ASTM E1025-18, ASTM E2698-18, ASTM E1316-18, ASTM E746-17. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

ASTM E94/E94M-22 is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.

Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E94/E94M − 22
Standard Guide for
Radiographic Examination Using Industrial Radiographic
Film
This standard is issued under the fixed designation E94/E94M; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope* 1.5 Safety Practices—Problems of personnel protection
2 against X-rays and gamma-rays are not covered by this guide.
1.1 This guide covers satisfactory X-ray and gamma-ray
For information on this important aspect of radiography,
radiographic examination as applied to industrial radiographic
reference should be made to the current document of the
film recording. It includes statements about preferred practice
National Committee on Radiation Protection and
withoutdiscussingthetechnicalbackgroundwhichjustifiesthe
Measurement, Federal Register, U.S. Energy Research and
preference. A bibliography of several textbooks and standard
Development Administration, National Bureau of Standards,
documents of other societies is included for additional infor-
and to state and local regulations, if such exist. For specific
mation on the subject.
radiation safety information, refer to NIST Handbook ANSI
1.2 This guide covers types of materials to be examined;
43.3, 21 CFR 1020.40, and 29 CFR 1910.1096 or state
radiographic examination techniques and production methods;
regulations for agreement states.
radiographic film selection, processing, viewing, and storage;
1.6 Units—The values stated in either SI units or inch-
maintenance of inspection records; and a list of available
pound units are to be regarded separately as standard. The
reference radiograph documents.
values stated in each system may not be exact equivalents;
NOTE 1—Further information is contained in Guide E999, Practice
therefore, each system should be used independently of the
E1025, Practice E1030/E1030M, and Practice E1032.
other. Combining values from the two systems may result in
1.3 Theuseofdigitalradiographyhasexpandedandfollows
non-conformance with the standard.
many of the same general principles of film based radiography
1.7 If an NDT agency is used, the agency should be
but with many important differences. The user is referred to
qualified in accordance with Specification E543.
standards for digital radiography [E2597, E2698, E2736, and
1.8 Personnel Qualification—If specified in the contractual
E2737 for digital detector array (DDA) radiography and
agreement, personnel performing examinations to this guide
E2007, E2033, E2445/E2445M, and E2446 for computed
should be qualified in accordance with a nationally or interna-
radiography(CR)]ifconsideringtheuseofdigitalradiography.
tionally recognized NDT personnel qualification practice or
1.4 Interpretation and Acceptance Standards—
standard and certified by the employer or certifying agency, as
Interpretationandacceptancestandardsarenotcoveredbythis
applicable.
guide, beyond listing the available reference radiograph docu-
1.9 This standard does not purport to address all of the
ments for castings and welds. Designation of accept - reject
safety problems, if any, associated with its use. It is the
standards is recognized to be within the cognizance of product
responsibility of the user of this standard to establish appro-
specifications and generally a matter of contractual agreement
priate safety, health, and environmental practices and deter-
between producer and purchaser.
mine the applicability of regulatory limitations prior to use.
(See 1.5.)
This guide is under the jurisdiction ofASTM Committee E07 on Nondestruc-
1.10 This international standard was developed in accor-
tive Testing and is the direct responsibility of Subcommittee E07.01 on Radiology
dance with internationally recognized principles on standard-
(X and Gamma) Method.
Current edition approved Dec. 1, 2022. Published December 2022. Originally
ization established in the Decision on Principles for the
approved in 1952. Last previous edition approved in 2017 as E94/E94M–17. DOI:
Development of International Standards, Guides and Recom-
10.1520/E0094_E0094M-22.
mendations issued by the World Trade Organization Technical
For ASME Boiler and Pressure Vessel Code applications, see related Guide
SE-94 in Section V of that Code. Barriers to Trade (TBT) Committee.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
E94/E94M − 22
2. Referenced Documents E2446Practice for Manufacturing Characterization of Com-
3 puted Radiography Systems
2.1 ASTM Standards:
E2597Practice for Manufacturing Characterization of Digi-
E543Specification forAgencies Performing Nondestructive
tal Detector Arrays
Testing
E2698Practice for Radiographic Examination Using Digital
E746Practice for Determining Relative Image Quality Re-
Detector Arrays
sponse of Industrial Radiographic Imaging Systems
E2736Guide for Digital Detector Array Radiography
E747Practice for Design, Manufacture and Material Group-
E2737Practice for Digital Detector Array Performance
ing Classification of Wire Image Quality Indicators (IQI)
Evaluation and Long-Term Stability
Used for Radiology
E2903Test Method for Measurement of the Effective Focal
E801Practice for Controlling Quality of Radiographic Ex-
Spot Size of Mini and Micro Focus X-ray Tubes
amination of Electronic Devices
E3169Guide for Digital Imaging and Communication in
E999Guide for Controlling the Quality of Industrial Radio-
Nondestructive Evaluation (DICONDE)
graphic Film Processing
2.2 ANSI Standard:
E1000Guide for Radioscopy
ANSI/I3A/PIMAIT 2.26Determination of Safelight Condi-
E1025 Practice for Design, Manufacture, and Material
tions
Grouping Classification of Hole-Type Image Quality In-
2.3 Federal Standards:
dicators (IQI) Used for Radiography
Title21,CodeofFederalRegulations(CFR)1020.40,Safety
E1030/E1030MPractice for Radiographic Examination of
Requirements of Cabinet X-Ray Systems
Metallic Castings
Title 29,Code of Federal Regulations (CFR) 1910.96, Ion-
E1032PracticeforRadiographicExaminationofWeldments
izing Radiation (X-Rays, RF, etc.)
Using Industrial X-Ray Film
2.4 ISO Standards:
E1079Practice for Calibration of Transmission Densitom-
ISO 14096-2Non-destructive Testing — Qualification of
eters
Radiographic Film Digitization Systems — Part 2: Mini-
E1165Test Method for Measurement of Focal Spots of
mum Requirements
Industrial X-Ray Tubes by Pinhole Imaging
ISO 18901Imaging Materials — Processed Silver-Gelatin-
E1254Guide for Storage of Radiographs and Unexposed
typeBlack-and-whiteFilms—SpecificationsforStability
Industrial Radiographic Films
ISO 18902Imaging Materials — Processed Imaging Mate-
E1316Terminology for Nondestructive Examinations
rials — Albums, Framing and Storage Materials
E1390Specification for Illuminators Used for Viewing In-
ISO 18917Photography—Determination of Residual Thio-
dustrial Radiographs
sulphate and Other Related Chemicals in Processed Pho-
E1453Guide for Storage of Magnetic Tape Media that
tographic Materials—Methods Using Iodine-amylose,
Contains Analog or Digital Radioscopic Data
Methylene Blue and Silver Sulfide
E1475Guide for Data Fields for Computerized Transfer of
Digital Radiological Examination Data 2.5 Other Document:
E1735Practice for Determining Relative Image Quality NBS HandbookANSI N43.3 General Radiation Safety In-
Response of Industrial Radiographic Imaging Systems stallations Using NonMedical X-Ray and Sealed Gamma-
from4to25MeV Ray Sources up to 10 MeV
E1742/E1742MPractice for Radiographic Examination
3. Terminology
E1815Test Method for Classification of Film Systems for
Industrial Radiography
3.1 Definitions—For definitions of terms used in this guide,
E1817Practice for Controlling Quality of Radiological Ex-
refer to Terminology E1316.
amination by Using Representative Quality Indicators
4. Significance and Use
(RQIs)
E1936Reference Radiograph for Evaluating the Perfor-
4.1 Within the present state of the radiographic art, this
mance of Radiographic Digitization Systems
guide is generally applicable to available materials, processes,
E2007Guide for Computed Radiography
and techniques where industrial radiographic films are used as
E2033Practice for Radiographic Examination Using Com-
the recording media.
puted Radiography (Photostimulable Luminescence
4.2 Limitations—Thisguidedoesnottakeintoconsideration
Method)
the benefits and limitations of nonfilm radiography such as
E2339Practice for Digital Imaging and Communication in
Nondestructive Evaluation (DICONDE)
E2445/E2445MPractice for Performance Evaluation and 4
Available fromAmerican National Standards Institute (ANSI), 25 W. 43rd St.,
Long-Term Stability of Computed Radiography Systems 4th Floor, New York, NY 10036.
AvailablefromU.S.GovernmentPrintingOfficeSuperintendentofDocuments,
732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401.
Available from International Organization for Standardization (ISO), ISO
For referenced ASTM standards, visit the ASTM website, www.astm.org, or Central Secretariat, Chemin de Blandonnet 8, CP 401, 1214 Vernier, Geneva,
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Switzerland, https://www.iso.org.
Standards volume information, refer to the standard’s Document Summary page on Available from National Technical Information Service (NTIS), U.S. Depart-
the ASTM website. ment of Commerce, 5301 Shawnee Rd, Alexandria, VA 22312.
E94/E94M − 22
radioscopy, digital detector arrays, or computed radiography. raphy is 2% (2-2T when using hole type IQI) unless a higher
Refer to Guides E1000, E2736, and E2007. or lower quality is agreed upon between the purchaser and the
supplier. The level of inspection specified should be based on
4.3 Although reference is made to documents that may be
the service requirements of the product. Great care should be
used in the identification and grading, where applicable, of
taken in specifying quality levels 2-1T, 1-1T, and 1-2T by first
representative discontinuities in common metal castings and
determining that these quality levels can be maintained in
welds,noattempthasbeenmadetosetstandardsofacceptance
production radiography.
for any material or production process.
6.3 If IQIs of material radiographically similar to that being
4.4 Radiography will be consistent in image quality (con-
examined are not available, IQIs of the required dimensions
trast sensitivity and definition) only if all details of techniques,
but of a lower-absorption material may be used.
such as geometry, film, filtration, viewing, etc., are obtained
and maintained. 6.4 The quality level required using wire IQIs should be
equivalent to the 2-2T level of Practice E1025 unless a higher
5. Equipment and Configuration
or lower quality level is agreed upon between purchaser and
5.1 Toobtainqualityradiographs,itisnecessarytoconsider
supplier. Table 4 of Practice E747 provides a list of various
asaminimumthefollowinglistofitems.Detailedinformation
hole-type IQIs and the corresponding diameter of the wires to
on each item is further described in this guide.
achievetheEquivalentPenetrameterSensitivity(EPS)withthe
5.1.1 Radiation source (X-ray or gamma),
applicable1T,2T,and4TholesintheplaqueIQI.AppendixX1
5.1.2 Energy selection,
of Practice E747 gives the equation for calculating other
5.1.3 Source size (X-ray focal spot dimension or gamma
equivalencies, if needed.
source size),
7. Energy Selection
5.1.4 Ways and means to eliminate scattered radiation,
5.1.5 Film system class,
7.1 X-rayenergyaffectsimagequality.Ingeneral,thelower
5.1.6 Source-to-film and object-to-film distance,
the energy of the source utilized the higher the achievable
5.1.7 Image quality indicators (IQIs),
radiographic contrast, however, other variables such as exces-
5.1.8 Screens and filters,
sive dose geometry and scatter conditions may override the
5.1.9 Geometry of part or component configuration,
potential advantage of higher contrast. For a particular energy,
5.1.10 Identification and location markers, and
a range of thicknesses which are a multiple of the half value
5.1.11 Radiographic quality level.
layer, may be radiographed to an acceptable quality level
utilizing a particular X-ray machine or gamma ray source. In
6. Radiographic Quality Level
allcases,thespecifiedIQI(penetrameter)qualitylevelmustbe
6.1 Image Quality Indicators (IQIs) are devices placed
shown on the radiograph. In general, satisfactory results can
within a radiographic set-up to indicate that a certain contrast
normally be obtained for X-ray energies between 100 kV to
sensitivity and definition has been achieved. IQIs demonstrat-
500 kV in a range between 2.5 to 10 half value layers (HVL)
ingtherequiredsensitivityleveldonotguaranteethatasimilar
ofmaterialthickness(seeTable1).Thisrangemaybeextended
size flaw in a part will be detected but indicate that the
by as much as a factor of 2 in some situations for X-ray
radiographic quality has been met. Information on the design
energies in the 1 to 25 MVrange primarily because of reduced
and manufacture of image quality indicators (IQIs) can be
scatter.
found in Practices E747, E801, E1025, and E1742/E1742M.
8. Radiographic Equivalence Factors
6.2 Radiographic quality level is usually expressed in
percentofpartthicknessanddiameteroffeaturetobedetected. 8.1 Theradiographicequivalencefactorofamaterialisthat
If a single percent number is given, the feature diameter is factor by which the thickness of the material must be multi-
assumedtobetwicethegivenpercentthicknessofthepart.For pliedtogivethethicknessofa“standard”material(oftensteel)
example, if 2% is given for one inch [25.4 mm] thick part, the which has the same absorption. Radiographic equivalence
featurediameteris2×0.02×1in.[25.4mm]or0.04in.[1.016
mm]. Image quality levels using hole-type IQIs (see Practice
TABLE 1 Typical Steel HVL Thickness in Inches [mm] for
E1025)aredesignatedbyatwopartexpression X-YT.Thefirst
Common Energies
partoftheexpression XreferstotheIQIthicknessexpressedas
Thickness,
kV/MV
a percentage of the specimen thickness.The second part of the
Inches [mm]
expression YT refers to the diameter of the hole and is 120 kV 0.10 [2.5]
150 kV 0.14 [3.6]
expressed as a multiple of the IQI thickness, T. The image
200 kV 0.20 [5.1]
quality level 2-2T means that the IQI thickness T is 2% of the
250 kV 0.25 [6.4]
specimen thickness and that the diameter of the IQI imaged 400 kV (Se 75) 0.35 [8.9]
750 kV (Ir 192) 0.51 [12.5]
hole is 2 times the IQI thickness. If using wire IQIs, the wire
1 MV 0.57 [14.5]
set and wire number are designated. Correspondence between
2 MV (Co 60) 0.80 [20.3]
hole-type and wire-type IQIs is given in Practice E747. Hole- 4 MV 1.00 [25.4]
6 MV 1.15 [29.2]
and wire-type IQIs are the major types used for industrial
10 MV 1.25 [31.8]
radiography. Other types may also be used (for example, see
16 MV and higher 1.30 [33.0]
Practice E1817). The quality level usually required for radiog-
E94/E94M − 22
factors of several of the more common metals are given in 10.2.1 Decreasing scattered radiation, thus increasing con-
Table 2, with steel arbitrarily assigned a factor of 1.0. trast.
Example:To radiograph 1.0 in. [25.4 mm] of aluminum at 220 10.2.2 Decreasing undercutting, thus increasing contrast.
kV, multiply 1.0 by the 0.18 (equivalence factor for aluminum 10.2.3 Decreasing contrast of parts of varying thickness,
at 220 kV) and this indicates that 1.0 in. [25.4 mm] of thereby increasing radiographic latitude.
aluminum is equivalent to 0.18 in. [4.57 mm] of steel when
10.3 Location—Usually the filter will be placed in one of
using 220 kV.
the following two locations:
The factors may be used:
10.3.1 As close as possible to the radiation source, which
8.1.1 To determine the practical thickness limits for radia-
minimizes the size of the filter and also the contribution of the
tion sources for materials other than steel, and
filter itself to scattered radiation to the film.
8.1.2 To determine exposure for one metal from exposure
10.3.2 Betweenthespecimenandthefilminordertoabsorb
techniques for other metals.
preferentially the scattered radiation from the specimen. It
should be noted that lead foil and other metallic screens (see
9. Film
13.1) fulfill this function.
9.1 Various industrial radiographic films are available to
10.4 Thickness and Filter Material—The thickness and
meet the needs of production radiographic work. However,
material of the filter will vary depending upon the following:
definite rules on the selection of film are difficult to formulate
10.4.1 The material radiographed.
because the choice depends on individual user requirements.
10.4.2 Thickness of the material radiographed.
Some user requirements are as follows: radiographic quality
10.4.3 Variation of thickness of the material radiographed.
levels, exposure times, and various cost factors. Several
10.4.4 Energy spectrum of the radiation used.
methods are available for assessing image quality levels (see
10.4.5 The improvement desired (increasing or decreasing
Practices E746, E747, and E801). Information about specific
contrast). Filter thickness and material can be calculated or
products can be obtained from the manufacturers.
determined empirically.
9.2 Various industrial radiographic films are manufactured
11. Masking and Collimation
tomeetqualitylevelandproductionneeds.TestMethodE1815
provides a method for film manufacturer classification of film
11.1 Masking or blocking (surrounding specimens or cov-
systems.Afilm system consists of the film and associated film
ering thin sections with an absorptive material) is helpful in
processingsystem.Usersmayobtainaclassificationtablefrom
reducing scattered radiation. Such a material can also be used
the film manufacturer for the film system used in production
to equalize the absorption of different sections, but the loss of
radiography.Achoice of film class can be made as provided in
detail may be high in the thinner sections.
Test Method E1815. Additional specific details regarding
11.2 Collimating the beam by restricting its size with heavy
classification of film systems are provided in Test Method
metalbeamblockerstoonlythatareaneededtoexposethearea
E1815. ISO 18901, ISO 18902, and ISO 18917 provide
of interest is helpful in restricting scatter from areas in the part
specific details and requirements for film manufacturing.
outside the area of interest and the surrounding environment,
includingairscatter.Collimatorsareusuallyplacedclosetothe
10. Filters
source to minimize size and weight; however, collimators may
10.1 Definition—Filters are uniform layers of material
be placed anywhere in the beam to help with scatter control.
placed between the radiation source and the film.
12. Back-Scatter Protection
10.2 Purpose—The purpose of filters is to absorb the softer
components of the primary radiation, thus resulting in one or 12.1 Effects of back-scattered radiation can be reduced by
several of the following practical advantages: confining the radiation beam to the smallest practical cross
TABLE 2 Approximate Radiographic Equivalence Factors for Several Metals (Relative to Steel)
kV / MV
Metal
192 60 75
100 kV 150 kV 220 kV 250 kV 400 kV 1 MV 2 MV 4 to 25 MV Ir Co Se
Magnesium 0.05 0.05 0.08
Aluminum 0.08 0.12 0.18 0.35 0.35 0.5
Aluminum alloy 0.10 0.14 0.18 0.35 0.35 0.5
Titanium 0.54 0.54 0.71 0.9 0.9 0.9 0.9 0.9 0.6
Iron/all steels 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0
Copper 1.5 1.5 1.4 1.4 1.4 1.1 1.1 1.2 1.1 1.1 1.4
Zinc 1.4 1.3 1.3 1.2 1.1 1.0 1.2
Brass 1.4 1.3 1.3 1.2 1.1 1.0 1.1 1.0 1.3
Inconel X 1.4 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3
Monel 1.7 1.2 1.1
Zirconium 2.4 2.3 2.0 1.7 1.5 1.0 1.0 1.0 1.2 1.0 1.6
Lead 14.0 14.0 12.0 5.0 2.5 2.7 4.0 2.3 8.0
Hafnium 14.0 12.0 9.0 3.0 11.0
Uranium 20.0 16.0 12.0 4.0 3.9 12.6 3.4 14.0
E94/E94M − 22
section and by placing lead behind the film. In some cases, 13.2.3 Gold, tantalum, or other heavy metal screens may be
eitherorboththebackleadscreenandtheleadcontainedinthe used in cases where lead cannot be used.
back of the cassette or film holder will furnish adequate
13.3 Fluorescent Screens—Fluorescentscreensmaybeused
protection against back-scattered radiation. In other instances,
as required providing the required image quality is achieved.
this should be supplemented by additional lead shielding
Proper selection of the fluorescent screen is required to
behind the cassette or film holder.
minimize image unsharpness. Technical information about
12.2 If there is any question about the adequacy of protec- specific fluorescent screen products can be obtained from the
tion from back-scattered radiation, a characteristic symbol manufacturers. Good film-screen contact and screen cleanli-
(frequentlya ⁄8-in.[3.2-mm]thickletter B)shouldbeattached ness are required for successful use of fluorescent screens.
to the back of the cassette or film holder, and a radiograph Additional information on the use of fluorescent screens is
made in the normal manner. If the image of this symbol provided in Appendix X1.
appears on the radiograph with a lower optical density than
13.4 Screen Care—All screens should be handled carefully
background, it is an indication that protection against back-
to avoid dents and scratches, dirt, or grease on active surfaces.
scattered radiation is insufficient and that additional precau-
Grease and lint may be removed from lead screens with a
tions should be taken.
solvent. Fluorescent screens should be cleaned in accordance
with the recommendations of the manufacturer. Screens show-
13. Screens
ing evidence of physical damage should be discarded.
13.1 Metallic Foil Screens:
13.1.1 Lead foil screens are commonly used in direct
14. Radiographic Image Quality
contact with the films, and, depending upon their thickness,
14.1 Radiographic Image Quality is a qualitative term used
and composition of the specimen material, will exhibit an
to describe the capability of a radiograph to show flaws in the
intensifying action at as low as 90 kV. In addition, any screen
area under examination. There are three fundamental compo-
used in front of the film acts as a filter (Section 10)to
nents of radiographic image quality as shown in Fig. 1. Each
preferentially absorb scattered radiation arising from the
component is an important attribute when considering a
specimen, thus improving radiographic quality. The selection
specific radiographic technique or application and will be
of lead screen thickness, or for that matter, any metallic screen
briefly discussed below.
thickness, is subject to the same considerations as outlined in
10.4. Lead screens lessen the scatter reaching the film regard- 14.2 Radiographic Contrast between two areas of a radio-
less of whether the screens permit a decrease or necessitate an graph is the difference between the optical densities of those
areas. The degree of radiographic contrast is dependent upon
increaseintheradiographicexposure.Toavoidimageunsharp-
ness due to screens, there should be intimate contact between both subject contrast and film contrast as illustrated in Fig. 1.
the lead screen and the film during exposure. 14.2.1 Subject Contrast is the ratio of X-ray or gamma-ray
13.1.2 Lead foil screens of appropriate thickness should be intensities transmitted by two selected portions of a specimen.
Subject contrast is dependent upon the nature of the specimen
usedwhenevertheyimproveradiographicqualityorpenetram-
eter sensitivity, or both.The thickness of the front lead screens (materialtypeandthickness),theenergy(spectralcomposition,
hardness, or wavelengths) of the radiation used and the
should be selected with care to avoid excessive filtration in the
radiography of thin or light alloy materials, particularly at the intensity and distribution of scattered radiation. It is indepen-
dent of time, milliamperage or source strength (curies), source
lower kilovoltages. In general, there is no exposure advantage
totheuseof0.005in.[0.13mm]infrontandbackleadscreens distance and the characteristics of the film system.
14.2.2 Film Contrast refers to the slope (steepness) of the
below 125 kVin the radiography of ⁄4-in. [6.35-mm] or lesser
thickness steel. As the kilovoltage is increased to penetrate film system characteristic curve. Film contrast is dependent
thicker sections of steel, however, there is a significant expo- upon the type of film, the processing it receives, and the
sureadvantage.Inadditiontointensifyingaction,thebacklead amount of optical density. It also depends upon whether the
screens are used as protection against back-scattered radiation film was exposed with lead screens (or without) or with
(see Section 12) and their thickness is only important for this fluorescent screens. Film contrast is independent, for most
function. As exposure energy is increased to penetrate greater practical purposes, of the wavelength and distribution of the
thicknesses of a given subject material, it is customary to radiationreachingthefilmand,henceisindependentofsubject
increase lead screen thickness. For radiography using radioac- contrast. For further information, consult Test Method E1815.
tive sources, the minimum thickness of the front lead screen
14.3 Film System Granularity is the objective measurement
should be 0.005 in. [0.13 mm] for iridium-192, and 0.010 in.
of the local variation in optical density that produce the
[0.25 mm] for cobalt-60.
sensation of graininess on the radiographic film (for example,
13.2 Other Metallic Screen Materials: measured with a densitometer with a small aperture of
13.2.1 Lead oxide screens perform in a similar manner to ≤0.0039 in. [0.1mm]). Graininess is the subjective perception
lead foil screens except that their equivalence in lead foil of a mottled pattern apparent to a viewer who sees small local
thickness approximates 0.0005 in. [0.013 mm]. optical density variations in an area of overall uniform optical
13.2.2 Copper screens have somewhat less absorption and density (that is, the visual impression of irregularity of silver
intensification than lead screens, but may provide somewhat deposit in a processed radiograph). The degree of granularity
better radiographic sensitivity with higher energy above 1 MV. will not affect the overall spatial radiographic resolution
E94/E94M − 22
Radiographic Image Quality
Radiographic Contrast Radiographic Definition
Film System
Subject Film Inherent Geometric
Granularity
Contrast Contrast Unsharpness Unsharpness
Affected by: Affected by:  Grain size and distribution within
Affected by: Affected by:
 Absorption differences in  Type of film the film emulsion  Degree of screen-film contact  Focal spot or source
specimen (thickness,  Degree of development (type of  Processing conditions (type and  Total film thickness physical size
composition, density) developer, time, temperature and activity of developer, temperature of  Single or  Source-to-film distance
 Radiation wavelength activity of developer, degree of developer, etc.) double emulsion coatings  Specimen-to-film
 Scattered radiation agitation)  Type of screens (that is,  Radiation quality distance
 Optical density (that is, the fluorescent, metal, or none)  Type and thickness of screens  Abruptness of thick-
greater the optical density, the  Radiation quality (that is, energy (fluorescent, metal, or none) ness changes in
greater the resultant contrast) level, filtration, etc.) specimen
 Type of screens (that is,  Exposure quanta (that is,  Motion of specimen or
fluorescent, lead or none) intensity, dose, etc.) radiation source
The contrast increases approxi- The granularity increases approxi-
mately linearly with the optical den- mately with the square root of the
sity above fog and base optical density above fog and base
Reduced or enhanced by:
 Masks and diaphragms
 Filters
 Lead screens
• Potter-Bucky diaphragms
FIG. 1 Variables of Radiographic Image Quality
Example:
(expressedinlinepairspermm,etc.)oftheresultantimageand
Given:
is usually independent of exposure geometry arrangements.
Source-object distance (d )=40 in.,
o
Granularity is affected by the applied screens, screen-film
Source size (F) =500 mils, and
contact, and film processing conditions. For further informa-
Source side of specimen to film distance (t) =1.5 in.
tion on detailed perceptibility, consult Test Method E1815.
Drawastraightline(dashedinFig.3)between500milsonthe Fscaleand
1.5 in. on the t scale. Note the point on intersection (P) of this line with
14.4 Radiographic Definition refers to the sharpness of the
the pivot line. Draw a straight line (solid in Fig. 3) from 40 in. on the d
o
image (both the image outline as well as image detail).
scale through point P and extend to the U scale. Intersection of this line
g
Radiographic definition is dependent upon the inherent un- with the U scale gives geometrical unsharpness in mils, which in the
g
example is 19 mils.
sharpness of the film system and the geometry of the radio-
graphic exposure arrangement (geometric unsharpness) as Inasmuch as the source size, F, is usually fixed for a given
illustrated in Fig. 1. radiationsource,thevalueof U isessentiallycontrolledbythe
g
14.4.1 Inherent Unsharpness (U ) is the degree of visible simple d /t ratio.
i o
detailresultingfromgeometricalaspectswithinthefilm-screen Geometric unsharpness (U ) can have a significant effect on
g
system, that is, screen-film contact, screen thickness, total thequalityoftheradiograph;therefore,source-to-film-distance
thickness of the film emulsions, whether single or double- (SFD) selection is important. The geometric unsharpness
...


This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E94/E94M − 17 E94/E94M − 22
Standard Guide for
Radiographic Examination Using Industrial Radiographic
Film
This standard is issued under the fixed designation E94/E94M; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope Scope*
1.1 This guide covers satisfactory X-ray and gamma-ray radiographic examination as applied to industrial radiographic film
recording. It includes statements about preferred practice without discussing the technical background which justifies the
preference. A bibliography of several textbooks and standard documents of other societies is included for additional information
on the subject.
1.2 This guide covers types of materials to be examined; radiographic examination techniques and production methods;
radiographic film selection, processing, viewing, and storage; maintenance of inspection records; and a list of available reference
radiograph documents.
NOTE 1—Further information is contained in Guide E999, Practice E1025, Test Methods Practice E1030E1030/E1030M, and Practice E1032.
1.3 The use of digital radiography has expanded and follows many of the same general principles of film based radiography but
with many important differences. The user is referred to standards for digital radiography [E2597, E2698, E2736, and E2737 for
digital detector array (DDA) radiography and E2007, E2033, E2445/E2445M, and E2446 for computed radiography(CR)] if
considering the use of digital radiography.
1.4 Interpretation and Acceptance Standards—Interpretation and acceptance standards are not covered by this guide, beyond
listing the available reference radiograph documents for castings and welds. Designation of accept - reject standards is recognized
to be within the cognizance of product specifications and generally a matter of contractual agreement between producer and
purchaser.
1.5 Safety Practices—Problems of personnel protection against X rays and gamma rays X-rays and gamma-rays are not covered
by this document.guide. For information on this important aspect of radiography, reference should be made to the current document
of the National Committee on Radiation Protection and Measurement, Federal Register, U.S. Energy Research and Development
Administration, National Bureau of Standards, and to state and local regulations, if such exist. For specific radiation safety
information, refer to NIST Handbook ANSI 43.3, 21 CFR 1020.40, and 29 CFR 1910.1096 or state regulations for agreement
states.
This guide is under the jurisdiction of ASTM Committee E07 on Nondestructive Testing and is the direct responsibility of Subcommittee E07.01 on Radiology (X and
Gamma) Method.
Current edition approved June 1, 2017Dec. 1, 2022. Published August 2017December 2022. Originally approved in 1952. Last previous edition approved in 20102017
as E94 - 04E94/E94M – 17.(2010). DOI: 10.1520/E0094_E0094M-17.10.1520/E0094_E0094M-22.
For ASME Boiler and Pressure Vessel Code applications, see related Guide SE-94 in Section V of that Code.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
E94/E94M − 22
1.6 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in
each system may not be exact equivalents; therefore, each system should be used independently of the other. Combining values
from the two systems may result in non-conformance with the standard.
1.7 If an NDT agency is used, the agency should be qualified in accordance with Specification E543.
1.8 Personnel Qualification—If specified in the contractual agreement, personnel performing examinations to this guide should
be qualified in accordance with a nationally or internationally recognized NDT personnel qualification practice or standard and
certified by the employer or certifying agency, as applicable.
1.9 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of
regulatory limitations prior to use. (See 1.5.)
1.10 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2.1 ASTM Standards:
E543 Specification for Agencies Performing Nondestructive Testing
E746 Practice for Determining Relative Image Quality Response of Industrial Radiographic Imaging Systems
E747 Practice for Design, Manufacture and Material Grouping Classification of Wire Image Quality Indicators (IQI) Used for
Radiology
E801 Practice for Controlling Quality of Radiographic Examination of Electronic Devices
E999 Guide for Controlling the Quality of Industrial Radiographic Film Processing
E1000 Guide for Radioscopy
E1025 Practice for Design, Manufacture, and Material Grouping Classification of Hole-Type Image Quality Indicators (IQI)
Used for Radiography
E1030E1030/E1030M Practice for Radiographic Examination of Metallic Castings
E1032 Practice for Radiographic Examination of Weldments Using Industrial X-Ray Film
E1079 Practice for Calibration of Transmission Densitometers
E1165 Test Method for Measurement of Focal Spots of Industrial X-Ray Tubes by Pinhole Imaging
E1254 Guide for Storage of Radiographs and Unexposed Industrial Radiographic Films
E1316 Terminology for Nondestructive Examinations
E1390 Specification for Illuminators Used for Viewing Industrial Radiographs
E1453 Guide for Storage of Magnetic Tape Media that Contains Analog or Digital Radioscopic Data
E1475 Guide for Data Fields for Computerized Transfer of Digital Radiological Examination Data
E1735 Practice for Determining Relative Image Quality Response of Industrial Radiographic Imaging Systems from 4 to 25
MeV
E1742E1742/E1742M Practice for Radiographic Examination
E1815 Test Method for Classification of Film Systems for Industrial Radiography
E1817 Practice for Controlling Quality of Radiological Examination by Using Representative Quality Indicators (RQIs)
E1936 Reference Radiograph for Evaluating the Performance of Radiographic Digitization Systems
E2007 Guide for Computed Radiography
E2033 Practice for Radiographic Examination Using Computed Radiography (Photostimulable Luminescence Method)
E2339 Practice for Digital Imaging and Communication in Nondestructive Evaluation (DICONDE)
E2445/E2445M Practice for Performance Evaluation and Long-Term Stability of Computed Radiography Systems
E2446 Practice for Manufacturing Characterization of Computed Radiography Systems
E2597 Practice for Manufacturing Characterization of Digital Detector Arrays
E2698 Practice for Radiographic Examination Using Digital Detector Arrays
E2736 Guide for Digital Detector Array Radiography
E2737 Practice for Digital Detector Array Performance Evaluation and Long-Term Stability
E2903 Test Method for Measurement of the Effective Focal Spot Size of Mini and Micro Focus X-ray Tubes
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
E94/E94M − 22
E3169 Guide for Digital Imaging and Communication in Nondestructive Evaluation (DICONDE)
2.2 ANSI Standards:Standard:
PH1.41 Specifications for Photographic Film Archival Records, Silver Type
PH2.22ANSI/I3A/PIMA IT 2.26 Photography (Sensitometry)—Determination Determination of Safelight Conditions
T9.1 Imaging Media (Film)—Silver-Gelatin Type Specifications for Stability
T9.2 Imaging Media—Photographic Processed Films, Plates, and Paper Filing Enclosures and Storage Containers
2.3 Federal Standards:
Title 21, Code of Federal Regulations (CFR) 1020.40, Safety Requirements of Cabinet X-Ray Systems
Title 29, Code of Federal Regulations (CFR) 1910.96, Ionizing Radiation (X-Rays, RF, etc.)
2.4 ISO Standards:
ISO 14096-2 Non-destructive Testing — Qualification of Radiographic Film Digitization Systems — Part 2: Minimum
Requirements
ISO 18901 Imaging Materials — Processed Silver-Gelatin-type Black-and-white Films — Specifications for Stability
ISO 18902 Imaging Materials — Processed Imaging Materials — Albums, Framing and Storage Materials
ISO 18917 Photography—Determination of Residual Thiosulphate and Other Related Chemicals in Processed Photographic
Materials—Methods Using Iodine-amylose, Methylene Blue and Silver Sulfide
2.5 Other Document:
ISO 18917 Photography—Determination of residual thiosulphate and other related chemicals in processed photographic
materials—Methods using iodine-amylose, methylene blue and silver sulfide
NBS Handbook ANSI N43.3 General Radiation Safety Installations Using NonMedical X-Ray and Sealed Gamma-Ray Sources
up to 10 MeV
3. Terminology
3.1 Definitions—For definitions of terms used in this guide, refer to Terminology E1316.
4. Significance and Use
4.1 Within the present state of the radiographic art, this guide is generally applicable to available materials, processes, and
techniques where industrial radiographic films are used as the recording media.
4.2 Limitations—This guide does not take into consideration the benefits and limitations of nonfilm radiography such as
fluoroscopy,radioscopy, digital detector arrays, or computed radiography. Refer to Guides E1000, E2736, and E2007.
4.3 Although reference is made to documents that may be used in the identification and grading, where applicable, of
representative discontinuities in common metal castings and welds, no attempt has been made to set standards of acceptance for
any material or production process.
4.4 Radiography will be consistent in image quality (contrast sensitivity and definition) only if all details of techniques, such as
geometry, film, filtration, viewing, etc., are obtained and maintained.
5. Equipment and Configuration
5.1 To obtain quality radiographs, it is necessary to consider as a minimum the following list of items. Detailed information on
each item is further described in this guide.
5.1.1 Radiation source (X-ray or gamma),
5.1.2 Energy selection,
5.1.3 Source size (X-ray focal spot dimension or gamma source size),
5.1.4 Ways and means to eliminate scattered radiation,
Available from American National Standards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York, NY 10036.
Available from U.S. Government Printing Office Superintendent of Documents, 732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401.
Available from International Organization for Standardization (ISO), ISO Central Secretariat, Chemin de Blandonnet 8, CP 401, 1214 Vernier, Geneva, Switzerland,
https://www.iso.org.
Available from National Technical Information Service (NTIS), U.S. Department of Commerce, 5301 Shawnee Rd, Alexandria, VA 22312.
E94/E94M − 22
5.1.5 Film system class,
5.1.6 Source-to-film and object-to-film distance,
5.1.7 Image quality indicators (IQIs),
5.1.8 Screens and filters,
5.1.9 Geometry of part or component configuration,
5.1.10 Identification and location markers, and
5.1.11 Radiographic quality level.
6. Radiographic Quality Level
6.1 Image Quality Indicators (IQIs) are devices placed within a radiographic set-up to indicate that a certain contrast sensitivity
and definition has been achieved. IQIs demonstrating the required sensitivity level do not guarantee that a similar size flaw in a
part will be detected but indicate that the radiographic quality has been met. Information on the design and manufacture of image
quality indicators (IQIs) can be found in Practices E747, E801, E1025, and E1742E1742/E1742M.
6.2 Radiographic quality level is usually expressed in percent of part thickness and diameter of feature to be detected. If a single
percent number is given, the feature diameter is assumed to be twice the given percent thickness of the part. For example, if 2%
is given for one inch [25.4 mm] thick part, the feature diameter is 2 × 0.02 × 1 in. [25.4 mm] or 0.04 in. [1.016 mm]. Image quality
levels using hole-type IQIs (see Practice E1025) are designated by a two part expression X-YT. The first part of the expression X
refers to the IQI thickness expressed as a percentage of the specimen thickness. The second part of the expression YT refers to the
diameter of the hole and is expressed as a multiple of the IQI thickness, T. The image quality level 2-2T means that the IQI
thickness T is 2% of the specimen thickness and that the diameter of the IQI imaged hole is 2 times the IQI thickness. If using
wire IQIs, the wire set and wire number are designated. Correspondence between hole-type and wire-type IQIs is given in Practice
E747. Hole- and wire-type IQIs are the major types used for industrial radiography. Other types may also be used (for example,
see Practice E1817). The quality level usually required for radiography is 2 % (2-2T when using hole type IQI) unless a higher
or lower quality is agreed upon between the purchaser and the supplier. The level of inspection specified should be based on the
service requirements of the product. Great care should be taken in specifying quality levels 2-1T, 1-1T, and 1-2T by first
determining that these quality levels can be maintained in production radiography.
6.3 If IQIs of material radiographically similar to that being examined are not available, IQIs of the required dimensions but of
a lower-absorption material may be used.
6.4 The quality level required using wire IQIs should be equivalent to the 2-2T level of Practice E1025 unless a higher or lower
quality level is agreed upon between purchaser and supplier. Table 4 of Practice E747 provides a list of various hole-type IQIs and
the corresponding diameter of the wires to achieve the Equivalent Penetrameter Sensitivity (EPS) with the applicable 1T, 2T, and
4T holes in the plaque IQI. Appendix X1 of Practice E747 gives the equation for calculating other equivalencies, if needed.
7. Energy Selection
7.1 X-ray energy affects image quality. In general, the lower the energy of the source utilized the higher the achievable
radiographic contrast, however, other variables such as excessive dose geometry and scatter conditions may override the potential
advantage of higher contrast. For a particular energy, a range of thicknesses which are a multiple of the half value layer, may be
radiographed to an acceptable quality level utilizing a particular X-ray machine or gamma ray source. In all cases, the specified
IQI (penetrameter) quality level must be shown on the radiograph. In general, satisfactory results can normally be obtained for
X-ray energies between 100 kV to 500 kV in a range between 2.5 to 10 half value layers (HVL) of material thickness (see Table
1). This range may be extended by as much as a factor of 2 in some situations for X-ray energies in the 1 to 25 MV range primarily
because of reduced scatter.
8. Radiographic Equivalence Factors
8.1 The radiographic equivalence factor of a material is that factor by which the thickness of the material must be multiplied to
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TABLE 1 Typical Steel HVL Thickness in Inches [mm] for
Common Energies
Thickness,
kV/MV
Inches [mm]
120 kV 0.10 [2.5]
150 kV 0.14 [3.6]
200 kV 0.20 [5.1]
250 kV 0.25 [6.4]
400 kV (Ir 192) 0.35 [8.9]
400 kV (Se 75) 0.35 [8.9]
750 kV (Ir 192) 0.51 [12.5]
1 MV 0.57 [14.5]
2 MV (Co 60) 0.80 [20.3]
4 MV 1.00 [25.4]
6 MV 1.15 [29.2]
10 MV 1.25 [31.8]
16 MV and higher 1.30 [33.0]
give the thickness of a “standard” material (often steel) which has the same absorption. Radiographic equivalence factors of several
of the more common metals are given in Table 2, with steel arbitrarily assigned a factor of 1.0.
Example: To radiograph 1.0 in. [25.4 mm] of aluminum at 220 kV, multiply 1.0 by the 0.18 (equivalence factor for aluminum at
220 kV) and this indicates that 1.0 in. [25.4 mm] of aluminum is equivalent to 0.18 in. [4.57 mm] of steel when using 220 kV.
The factors may be used:
8.1.1 To determine the practical thickness limits for radiation sources for materials other than steel, and
8.1.2 To determine exposure for one metal from exposure techniques for other metals.
9. Film
9.1 Various industrial radiographic films are available to meet the needs of production radiographic work. However, definite rules
on the selection of film are difficult to formulate because the choice depends on individual user requirements. Some user
requirements are as follows: radiographic quality levels, exposure times, and various cost factors. Several methods are available
for assessing image quality levels (see Practices E746, E747, and E801). Information about specific products can be obtained from
the manufacturers.
9.2 Various industrial radiographic films are manufactured to meet quality level and production needs. Test Method E1815
provides a method for film manufacturer classification of film systems. A film system consistconsists of the film and associated
film processing system. Users may obtain a classification table from the film manufacturer for the film system used in production
radiography. A choice of film class can be made as provided in Test Method E1815. Additional specific details regarding
classification of film systems isare provided in Test Method E1815. ANSI Standards PH1.41, ISO 417, T9.1, and T9.2 ISO 18901,
ISO 18902, and ISO 18917 provide specific details and requirements for film manufacturing.
TABLE 2 Approximate Radiographic Equivalence Factors for Several Metals (Relative to Steel)
kVMVkV / MV
Metal
192 60 75
100 kV 150 kV 220 kV 250 kV 400 kV 1 MV 2 MV 4 to 25 MV Ir Co Se
Magnesium 0.05 0.05 0.08
Aluminum 0.08 0.12 0.18 0.35 0.35 0.5
Aluminum alloy 0.10 0.14 0.18 0.35 0.35 0.5
Titanium 0.54 0.54 0.71 0.9 0.9 0.9 0.9 0.9 0.6
Iron/all steels 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0
Copper 1.5 1.6 1.4 1.4 1.4 1.1 1.1 1.2 1.1 1.1 1.4
Copper 1.5 1.5 1.4 1.4 1.4 1.1 1.1 1.2 1.1 1.1 1.4
Zinc 1.4 1.3 1.3 1.2 1.1 1.0 1.2
Brass 1.4 1.3 1.3 1.2 1.1 1.0 1.1 1.0 1.3
Inconel X 1.4 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3
Monel 1.7 1.2 1.1
Zirconium 2.4 2.3 2.0 1.7 1.5 1.0 1.0 1.0 1.2 1.0 1.6
Lead 14.0 14.0 12.0 5.0 2.5 2.7 4.0 2.3 8.0
Hafnium 14.0 12.0 9.0 3.0 11.0
Uranium 20.0 16.0 12.0 4.0 3.9 12.6 3.4 14.0
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10. Filters
10.1 Definition—Filters are uniform layers of material placed between the radiation source and the film.
10.2 Purpose—The purpose of filters is to absorb the softer components of the primary radiation, thus resulting in one or several
of the following practical advantages:
10.2.1 Decreasing scattered radiation, thus increasing contrast.
10.2.2 Decreasing undercutting, thus increasing contrast.
10.2.3 Decreasing contrast of parts of varying thickness, thereby increasing radiographic latitude.
10.3 Location—Usually the filter will be placed in one of the following two locations:
10.3.1 As close as possible to the radiation source, which minimizes the size of the filter and also the contribution of the filter itself
to scattered radiation to the film.
10.3.2 Between the specimen and the film in order to absorb preferentially the scattered radiation from the specimen. It should
be noted that lead foil and other metallic screens (see 13.1) fulfill this function.
10.4 Thickness and Filter Material—The thickness and material of the filter will vary depending upon the following:
10.4.1 The material radiographed.
10.4.2 Thickness of the material radiographed.
10.4.3 Variation of thickness of the material radiographed.
10.4.4 Energy spectrum of the radiation used.
10.4.5 The improvement desired (increasing or decreasing contrast). Filter thickness and material can be calculated or determined
empirically.
11. Masking and Collimation
11.1 Masking or blocking (surrounding specimens or covering thin sections with an absorptive material) is helpful in reducing
scattered radiation. Such a material can also be used to equalize the absorption of different sections, but the loss of detail may be
high in the thinner sections.
11.2 Collimating the beam by restricting its size with heavy metal beam blockers to only that area needed to expose the area of
interest is helpful in restricting scatter from areas in the part outside the area of interest and the surrounding environment, including
air scatter. Collimators are usually placed close to the source to minimize size and weight; however, collimators may be placed
anywhere in the beam to help with scatter control.
12. Back-Scatter Protection
12.1 Effects of back-scattered radiation can be reduced by confining the radiation beam to the smallest practical cross section and
by placing lead behind the film. In some cases, either or both the back lead screen and the lead contained in the back of the cassette
or film holder will furnish adequate protection against back-scattered radiation. In other instances, this shallshould be
supplemented by additional lead shielding behind the cassette or film holder.
12.2 If there is any question about the adequacy of protection from back-scattered radiation, a characteristic symbol (frequently
a ⁄8-in. [3.2-mm] thick letter B) should be attached to the back of the cassette or film holder, and a radiograph made in the normal
manner. If the image of this symbol appears on the radiograph aswith a lighter lower optical density than background, it is an
indication that protection against back-scattered radiation is insufficient and that additional precautions shallshould be taken.
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13. Screens
13.1 Metallic Foil Screens:
13.1.1 Lead foil screens are commonly used in direct contact with the films, and, depending upon their thickness, and composition
of the specimen material, will exhibit an intensifying action at as low as 90 kV. In addition, any screen used in front of the film
acts as a filter (Section 10) to preferentially absorb scattered radiation arising from the specimen, thus improving radiographic
quality. The selection of lead screen thickness, or for that matter, any metallic screen thickness, is subject to the same
considerations as outlined in 10.4. Lead screens lessen the scatter reaching the film regardless of whether the screens permit a
decrease or necessitate an increase in the radiographic exposure. To avoid image unsharpness due to screens, there should be
intimate contact between the lead screen and the film during exposure.
13.1.2 Lead foil screens of appropriate thickness should be used whenever they improve radiographic quality or penetrameter
sensitivity, or both. The thickness of the front lead screens should be selected with care to avoid excessive filtration in the
radiography of thin or light alloy materials, particularly at the lower kilovoltages. In general, there is no exposure advantage to
the use of 0.005 in. [0.13 mm] in front and back lead screens below 125 kV in the radiography of ⁄4-in. [6.35-mm] or lesser
thickness steel. As the kilovoltage is increased to penetrate thicker sections of steel, however, there is a significant exposure
advantage. In addition to intensifying action, the back lead screens are used as protection against back-scattered radiation (see
Section 12) and their thickness is only important for this function. As exposure energy is increased to penetrate greater thicknesses
of a given subject material, it is customary to increase lead screen thickness. For radiography using radioactive sources, the
minimum thickness of the front lead screen should be 0.005 in. [0.13 mm] for iridium-192, and 0.010 in. [0.25 mm] for cobalt-60.
13.2 Other Metallic Screen Materials:
13.2.1 Lead oxide screens perform in a similar manner to lead foil screens except that their equivalence in lead foil thickness
approximates 0.0005 in. (0.013 mm).[0.013 mm].
13.2.2 Copper screens have somewhat less absorption and intensification than lead screens, but may provide somewhat better
radiographic sensitivity with higher energy above 1 MV.
13.2.3 Gold, tantalum, or other heavy metal screens may be used in cases where lead cannot be used.
13.3 Fluorescent Screens—Fluorescent screens may be used as required providing the required image quality is achieved. Proper
selection of the fluorescent screen is required to minimize image unsharpness. Technical information about specific fluorescent
screen products can be obtained from the manufacturers. Good film-screen contact and screen cleanliness are required for
successful use of fluorescent screens. Additional information on the use of fluorescent screens is provided in Appendix X1.
13.4 Screen Care—All screens should be handled carefully to avoid dents and scratches, dirt, or grease on active surfaces. Grease
and lint may be removed from lead screens with a solvent. Fluorescent screens should be cleaned in accordance with the
recommendations of the manufacturer. Screens showing evidence of physical damage should be discarded.
14. Radiographic Image Quality
14.1 Radiographic image qualityImage Quality is a qualitative term used to describe the capability of a radiograph to show flaws
in the area under examination. There are three fundamental components of radiographic image quality as shown in Fig. 1. Each
component is an important attribute when considering a specific radiographic technique or application and will be briefly discussed
below.
14.2 Radiographic contrastContrast between two areas of a radiograph is the difference between the filmoptical densities of those
areas. The degree of radiographic contrast is dependent upon both subject contrast and film contrast as illustrated in Fig. 1.
14.2.1 Subject contrastContrast is the ratio of X-ray or gamma-ray intensities transmitted by two selected portions of a specimen.
Subject contrast is dependent upon the nature of the specimen (material type and thickness), the energy (spectral composition,
hardness, or wavelengths) of the radiation used and the intensity and distribution of scattered radiation. It is independent of time,
milliamperage or source strength (curies), source distance and the characteristics of the film system.
14.2.2 Film contrastContrast refers to the slope (steepness) of the film system characteristic curve. Film contrast is dependent
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Radiographic Image Quality
Radiographic Contrast Radiographic Definition
Film System
Subject Film Inherent Geometric
Granularity
Contrast Contrast Unsharpness Unsharpness
Affected by: Affected by: • Grain size and distribution within Affected by: Affected by:
• Absorption differences in • Type of film the film emulsion • Degree of screen-film contact • Focal spot or source
specimen (thickness, • Degree of development (type of • Processing conditions (type and • Total film thickness physical size
composition, density) developer, time, temperature and activity of developer, temperature of • Single or • Source-to-film distance
• Radiation wavelength activity of developer, degree of developer, etc.) double emulsion coatings • Specimen-to-film
• Scattered radiation agitation) • Type of screens (that is, • Radiation quality distance
• Optical density (that is, the fluorescent, lead or none) • Type and thickness of screens • Abruptness of thick-
greater the optical density, the • Radiation quality (that is, energy (fluorescent, lead or none) ness changes in
greater the resultant contrast) level, filtration, etc. specimen
• Type of screens (that is, • Exposure quanta (that is, • Motion of specimen or
fluorescent, lead or none) intensity, dose, etc.) radiation source
•The contract increases approxi- •The granularity increases approxi-
mately linearly with the new optical mately with the square root of the
density net optical density
Affected by: Affected by: • Grain size and distribution within Affected by: Affected by:
• Absorption differences in • Type of film the film emulsion • Degree of screen-film contact • Focal spot or source
specimen (thickness, • Degree of development (type of • Processing conditions (type and • Total film thickness physical size
composition, density) developer, time, temperature and activity of developer, temperature of • Single or • Source-to-film distance
• Radiation wavelength activity of developer, degree of developer, etc.) double emulsion coatings • Specimen-to-film
• Scattered radiation agitation) • Type of screens (that is, • Radiation quality distance
• Optical density (that is, the fluorescent, metal, or none) • Type and thickness of screens • Abruptness of thick-
greater the optical density, the • Radiation quality (that is, energy (fluorescent, metal, or none) ness changes in
greater the resultant contrast) level, filtration, etc.) specimen
• Type of screens (that is, • Exposure quanta (that is, • Motion of specimen or
fluorescent, lead or none) intensity, dose, etc.) radiation source
•The contrast increases approxi- •The granularity increases approxi-
mately linearly with the optical den- mately with the square root of the
sity above fog and base optical density above fog and base
Reduced or enhanced by:
• Masks and diaphragms
• Filters
• Lead screens
• Potter-Bucky diaphragms
FIG. 1 Variables of Radiographic Image Quality
upon the type of film, the processing it receives, and the amount of optical density. It also depends upon whether the film was
exposed with lead screens (or without) or with fluorescent screens. Film contrast is independent, for most practical purposes, of
the wavelength and distribution of the radiation reaching the film and, hence is independent of subject contrast. For further
information, consult Test Method E1815.
14.3 Film system granularitySystem Granularity is the objective measurement of the local density variations variation in optical
density that produce the sensation of graininess on the radiographic film (for example, measured with a densitometer with a small
aperture of ≤ 0.0039 in. [0.1 mm]). Graininess is the subjective perception of a mottled pattern apparent to a viewer who sees small
local optical density variations in an area of overall uniform optical density (that is, the visual impression of irregularity of silver
deposit in a processed radiograph). The degree of granularity will not affect the overall spatial radiographic resolution (expressed
in line pairs per mm, etc.) of the resultant image and is usually independent of exposure geometry arrangements. Granularity is
affected by the applied screens, screen-film contact, and film processing conditions. For further information on detailed
perceptibility, consult Test Method E1815.
14.4 Radiographic definitionDefinition refers to the sharpness of the image (both the image outline as well as image detail).
Radiographic definition is dependent upon the inherent unsharpness of the film system and the geometry of the radiographic
exposure arrangement (geometric unsharpness) as illustrated in Fig. 1.
14.4.1 Inherent unsharpnessUnsharpness (U ) is the degree of visible detail resulting from geometrical aspects within the
i
film-screen system, that is, screen-film contact, screen thickness, total thickness of the film emulsions, whether single or
double-coated emulsions, quality of radiation used (wavelengths, etc.) and the type of screen. Inherent unsharpness is independent
of exposure geometry arrangements.
14.4.2 Geometric unsharpnessUnsharpness (U ) determin
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