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ASTM C1316-01

(Test Method)

Standard Test Method for Nondestructive Assay of Nuclear Material in Scrap and Waste by Passive-Active Neutron Counting Using a 252 Cf Shuffler

Standard Test Method for Nondestructive Assay of Nuclear Material in Scrap and Waste by Passive-Active Neutron Counting Using a 252 Cf Shuffler

SCOPE
1.1 This test method covers the nondestructive assay of scrap and waste for uranium and plutonium content using a  252Cf shuffler. Shuffler measurements provide rapid results and can be applied to a variety of matrix materials in containers as large as 208-litre drums. Corrections are made for the effects of matrix material. This test method has been used to assay items containing uranium, plutonium, or both. Applications of this test method include measurements for safeguards, accountability, TRU, and U waste segregation, disposal, and process control purposes (1,2,3).
1.1.1 This test method uses passive neutron coincidence counting to measure  238Pu,  240Pu, and  242Pu. It has been used to assay items with plutonium contents between 0.03 g and 1000 g. It could be used to measure other spontaneously fissioning isotopes. It specifically describes the approach used with shift register electronics; however, it can be adapted to other electronics.
1.1.2 This test method uses neutron irradiation with a moveable californium source and counting of the delayed neutrons from the induced fissions to measure 235U. It has been used to assay items with 235U contents between 0.1 g and 1000 g. It could be used to assay other fissionable isotopes.
1.2 This test method requires knowledge of the relative isotopic composition to determine the mass of the different elements.
1.3 This test method may give biased results for measurements of containers that include large quantities of hydrogen.
1.4 The techniques described in this test method have been applied to materials other than scrap and waste. These other applications are not addressed in this test method.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.

General Information

Status
Historical
Publication Date
09-Jun-2001
ICS
13.030.30 - Special wastes
17.240 - Radiation measurements
Technical Committee
C26 - Nuclear Fuel Cycle
Drafting Committee
C26.10 - Non Destructive Assay
Current Stage
Ref Project

Relations

Replaces
ASTM C1316-95 - Standard Test Method for Nondestructive Assay of Nuclear Material in Scrap and Waste by Passive-Active Neutron Counting Using a 252 Cf Shuffler
Effective Date
10-Jun-2001
Replaced By
ASTM C1316-08 - Standard Test Method for Nondestructive Assay of Nuclear Material in Scrap and Waste by Passive-Active Neutron Counting Using <sup>252</sup>Cf Shuffler
Effective Date
01-Jun-2008
Referred By
ASTM C1490-14(2023) - Standard Guide for the Selection, Training and Qualification of Nondestructive Assay (NDA) Personnel
Effective Date
10-Jun-2001
Referred By
ASTM C1207-10(2018) - Standard Test Method for Nondestructive Assay of Plutonium in Scrap and Waste by Passive Neutron Coincidence Counting
Effective Date
10-Jun-2001
Referred By
ASTM C1030-10(2018) - Standard Test Method for Determination of Plutonium Isotopic Composition by Gamma-Ray Spectrometry
Effective Date
10-Jun-2001
Referred By
ASTM C1133/C1133M-10(2018) - Standard Test Method for Nondestructive Assay of Special Nuclear Material in Low-Density Scrap and Waste by Segmented Passive Gamma-Ray Scanning
Effective Date
10-Jun-2001
Referred By
ASTM C1592/C1592M-21 - Standard Guide for Making Quality Nondestructive Assay Measurements
Effective Date
10-Jun-2001

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ASTM C1316-01 - Standard Test Method for Nondestructive Assay of Nuclear Material in Scrap and Waste by Passive-Active Neutron Counting Using a 252 Cf ShufflerASTM C1316-01 - Standard Test Method for Nondestructive Assay of Nuclear Material in Scrap and Waste by Passive-Active Neutron Counting Using a 252 Cf Shuffler
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ASTM C1316-01 - Standard Test Method for Nondestructive Assay of Nuclear Material in Scrap and Waste by Passive-Active Neutron Counting Using a 252 Cf Shuffler
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:C1316–01
Standard Test Method for
Nondestructive Assay of Nuclear Material in Scrap and
252
Waste by Passive-Active Neutron Counting Using a Cf
1
Shuffler
This standard is issued under the fixed designation C1316; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
1.1 This test method covers the nondestructive assay of
bility of regulatory limitations prior to use. Specific precau-
scrap and waste for uranium and plutonium content using a
tionary statements are given in Section 8.
252Cf shuffler. Shuffler measurements provide rapid results and
can be applied to a variety of matrix materials in containers as
2. Referenced Documents
largeas208-litredrums.Correctionsaremadefortheeffectsof
2.1 ASTM Standards:
matrix material.This test method has been used to assay items
3
C859 Terminology Relating to Nuclear Materials
containing uranium, plutonium, or both. Applications of this
C986 Guide for Developing Training Programs in the
testmethodincludemeasurementsforsafeguards,accountabil-
3
Nuclear Fuel Cycle
ity, TRU, and U waste segregation, disposal, and process
2 C1009 Guide for Establishing a Quality Assurance Pro-
control purposes (1,2,3).
gram for Analytical Chemistry Laboratories Within the
1.1.1 This test method uses passive neutron coincidence
3
238 240 242
Nuclear Industry
countingtomeasure Pu, Pu,and Pu.Ithasbeenusedto
C1030 Test Method for Determination of Plutonium Isoto-
assay items with plutonium contents between 0.03 g and 1000
3
pic Composition by Gamma-Ray Spectrometry
g. It could be used to measure other spontaneously fissioning
C1068 Guide for Qualification of Measurement Methods
isotopes. It specifically describes the approach used with shift
3
by a Laboratory Within the Nuclear Industry
register electronics; however, it can be adapted to other
C1128 Guide for Preparation of Working Reference Mate-
electronics.
rials for Use in the Analysis of Nuclear Fuel Cycle
1.1.2 This test method uses neutron irradiation with a
3
Materials
moveable californium source and counting of the delayed
235
C1133 Test Method for Nondestructive Assay of Special
neutrons from the induced fissions to measure U. It has been
235 Nuclear Material in Low Density Scrap and Waste by
usedtoassayitemswith Ucontentsbetween0.1gand1000
3
Segmented Passive Gamma-Ray Scanning
g. It could be used to assay other fissionable isotopes.
C1156 Guide for Establishing Calibration for a Measure-
1.2 This test method requires knowledge of the relative
ment Method Used to Analyze Nuclear Fuel Cycle Mate-
isotopic composition to determine the mass of the different
3
rials
elements.
C1207 TestMethodforNondestructiveAssayofPlutonium
1.3 This test method may give biased results for measure-
in Scrap and Waste by Passive Neutron Coincidence
ments of containers that include large quantities of hydrogen.
3
Counting
1.4 The techniques described in this test method have been
C1210 Guide for Establishing a Measurement System
applied to materials other than scrap and waste. These other
Quality Control Program for Analytical Chemistry Labo-
applications are not addressed in this test method.
3
ratories Within the Nuclear Industry
1.5 This standard does not purport to address all of the
C1215 Guide for Preparing and Interpreting Precision and
safety concerns, if any, associated with its use. It is the
Bias Statements in Test Method Standards used in the
3
Nuclear Industry
1
ThistestmethodisunderthejurisdictionofASTMCommitteeC26onNuclear
2.2 ANSI Documents:
Fuel Cycle and is the direct responsibility of Subcommittee C26.10 on Nondestruc-
tive Assay.
Current edition approved June 10, 2001. Published September 2001. Originally
published as C1316–95. Last previous edition C1316–95.
2
The boldface numbers in parentheses refer to a list of references at the end of
3
this test method. Annual Book of ASTM Standards, Vol 12.01.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
C1316
ANSI 15.20 Guide to Calibrating Nondestructive Assay 3.2.14 matrix-specific calibration, n—usesacalibrationma-
4
Systems trix similar to the waste matrix to be measured. No matrix
ANSI N15.36 Nondestructive Assay Measurement Control correction factors are used; this calibration is generally not
4
and Assurance appropriate for other matrices.
3.2.15 neutron absorbers, n—materials that have relatively
3. Terminology
largea
...

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SCOPE
1.1 This test method covers the determination of the amount of draindown in an uncompacted asphalt mixture sample when the sample is held at elevated temperatures comparable to those encountered during the production, storage, transport, and placement of the mixture. The test is particularly applicable to mixtures such as porous asphalt (open-graded friction course) and stone matrix asphalt (SMA).  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
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  • Standard
    3 pages
    English language
    sale 15% off