Standard Test Method for Evaluation of Heavy-Duty Engine Oils under High Output Conditions-Caterpillar C13 Test Procedure

SIGNIFICANCE AND USE
5.1 This test method assesses the performance of an engine oil with respect to control of piston deposits and maintenance of oil consumption under heavy-duty operating conditions selected to accelerate deposit formation in a turbocharged, intercooled four-stroke-cycle diesel engine equipped with a combustion system that minimizes federally controlled exhaust gas emissions.  
5.2 The results from this test method may be compared against specification requirements to ascertain acceptance.  
5.3 The design of the test engine used in this test method is representative of many, but not all, diesel engines. This factor, along with the accelerated operating conditions, needs to be considered when comparing test results against specification requirements.
SCOPE
1.1 The test method covers a heavy-duty engine test procedure under high output conditions to evaluate engine oil performance with regard to piston deposit formation, piston ring sticking and oil consumption control in a combustion environment designed to minimize exhaust emissions. This test method is commonly referred to as the Caterpillar C13 Heavy-Duty Engine Oil Test.3  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Exceptions-Where there are no SI equivalent such as screw threads, National Pipe Treads (NPT), and tubing sizes.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See Annex A1 for general safety precautions.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
30-Jun-2023
Current Stage
Ref Project

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ASTM D7549-23 - Standard Test Method for Evaluation of Heavy-Duty Engine Oils under High Output Conditions—Caterpillar C13 Test Procedure
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Frequently Asked Questions

ASTM D7549-23 is a standard published by ASTM International. Its full title is "Standard Test Method for Evaluation of Heavy-Duty Engine Oils under High Output Conditions-Caterpillar C13 Test Procedure". This standard covers: SIGNIFICANCE AND USE 5.1 This test method assesses the performance of an engine oil with respect to control of piston deposits and maintenance of oil consumption under heavy-duty operating conditions selected to accelerate deposit formation in a turbocharged, intercooled four-stroke-cycle diesel engine equipped with a combustion system that minimizes federally controlled exhaust gas emissions. 5.2 The results from this test method may be compared against specification requirements to ascertain acceptance. 5.3 The design of the test engine used in this test method is representative of many, but not all, diesel engines. This factor, along with the accelerated operating conditions, needs to be considered when comparing test results against specification requirements. SCOPE 1.1 The test method covers a heavy-duty engine test procedure under high output conditions to evaluate engine oil performance with regard to piston deposit formation, piston ring sticking and oil consumption control in a combustion environment designed to minimize exhaust emissions. This test method is commonly referred to as the Caterpillar C13 Heavy-Duty Engine Oil Test.3 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.2.1 Exceptions-Where there are no SI equivalent such as screw threads, National Pipe Treads (NPT), and tubing sizes. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See Annex A1 for general safety precautions. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE 5.1 This test method assesses the performance of an engine oil with respect to control of piston deposits and maintenance of oil consumption under heavy-duty operating conditions selected to accelerate deposit formation in a turbocharged, intercooled four-stroke-cycle diesel engine equipped with a combustion system that minimizes federally controlled exhaust gas emissions. 5.2 The results from this test method may be compared against specification requirements to ascertain acceptance. 5.3 The design of the test engine used in this test method is representative of many, but not all, diesel engines. This factor, along with the accelerated operating conditions, needs to be considered when comparing test results against specification requirements. SCOPE 1.1 The test method covers a heavy-duty engine test procedure under high output conditions to evaluate engine oil performance with regard to piston deposit formation, piston ring sticking and oil consumption control in a combustion environment designed to minimize exhaust emissions. This test method is commonly referred to as the Caterpillar C13 Heavy-Duty Engine Oil Test.3 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.2.1 Exceptions-Where there are no SI equivalent such as screw threads, National Pipe Treads (NPT), and tubing sizes. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See Annex A1 for general safety precautions. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D7549-23 is classified under the following ICS (International Classification for Standards) categories: 75.100 - Lubricants, industrial oils and related products. The ICS classification helps identify the subject area and facilitates finding related standards.

ASTM D7549-23 has the following relationships with other standards: It is inter standard links to ASTM D445-24, ASTM D613-24, ASTM D975-23a, ASTM D4175-23a, ASTM D86-23a, ASTM D86-23ae1, ASTM D445-23, ASTM D4175-23e1, ASTM D93-20, ASTM D5453-19a, ASTM D975-19, ASTM D975-18a, ASTM D5185-18, ASTM D975-17a, ASTM D613-17c. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

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Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D7549 − 23
Standard Test Method for
Evaluation of Heavy-Duty Engine Oils under High Output
Conditions—Caterpillar C13 Test Procedure
This standard is issued under the fixed designation D7549; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
Any properly equipped laboratory, without outside assistance, can use the test procedure described
in this test method. The ASTM Test Monitoring Center (TMC) provides calibration and an
assessment of the test results obtained on those oils by the laboratory. By this means the laboratory
will know whether its use of the test method gives results statistically similar to those obtained by
other laboratories. Furthermore, various agencies require that a laboratory utilizes the TMC services
in seeking qualification of oils against specifications. For example, the U.S. Army has such a
requirement in some of its engine oil specifications. Accordingly, this test method is written for those
laboratories that use the TMC services. Laboratories that choose not to use these services should
ignore those portions of the test method that refer to the TMC. Information letters issued periodically
by the TMC may modify this test method. In addition the TMC may issue supplementary memoranda
related to the test method.
ASTM International policy is to encourage the development of test procedures based on generic
equipment. It is recognized that there are occasions where critical/sole-source equipment has been
approved by the technical committee (surveillance panel/task force) and is required by the test
procedure. The technical committee that oversees the test procedure is encouraged to clearly identify
if the part is considered critical in the test procedure. If a part is deemed to be critical, ASTM
encourages alternative suppliers to be given the opportunity for consideration of supplying the critical
part/component providing they meet the approval process set forth by the technical committee.
An alternative supplier can start the process by initiating contact with the technical committee
(current chairs shown on ASTM TMC website). The supplier should advise on the details of the part
that is intended to be supplied. The technical committee will review the request and determine
feasibility of an alternative supplier for the requested replacement critical part. In the event that a
replacement critical part has been identified and proven equivalent, the sole-source supplier footnote
shall be removed from the test procedure.
1. Scope* performance with regard to piston deposit formation, piston
ring sticking and oil consumption control in a combustion
1.1 The test method covers a heavy-duty engine test proce-
environment designed to minimize exhaust emissions. This test
dure under high output conditions to evaluate engine oil
method is commonly referred to as the Caterpillar C13
Heavy-Duty Engine Oil Test.
This test method is under the jurisdiction of ASTM Committee D02 on
1.2 The values stated in SI units are to be regarded as
Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of
standard. No other units of measurement are included in this
Subcommittee D02.B0 on Automotive Lubricants.
standard.
Current edition approved July 1, 2023. Published July 2023. Originally published
in 2009. Last previous edition approved in 2021 as D7549 – 21. DOI: 10.1520/
1.2.1 Exceptions—Where there are no SI equivalent such as
D7549-23.
screw threads, National Pipe Treads (NPT), and tubing sizes.
The ASTM Test Monitoring Center will update changes in this test method by
means of Information Letters. This edition includes all information letters through
No. 23-1. Information Letters may be obtained by from the ASTM Test Monitoring Caterpillar Inc., Engine System Technology Development, PO Box 610,
Center, 203 Armstrong Drive, Freeport, PA 16229, Attention: Director. Mossville, IL 61552-0610.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D7549 − 23
1.3 This standard does not purport to address all of the D4739 Test Method for Base Number Determination by
safety concerns, if any, associated with its use. It is the Potentiometric Hydrochloric Acid Titration
responsibility of the user of this standard to establish appro- D5185 Test Method for Multielement Determination of
priate safety, health, and environmental practices and deter- Used and Unused Lubricating Oils and Base Oils by
mine the applicability of regulatory limitations prior to use. Inductively Coupled Plasma Atomic Emission Spectrom-
See Annex A1 for general safety precautions. etry (ICP-AES)
1.4 This international standard was developed in accor- D5186 Test Method for Determination of the Aromatic
dance with internationally recognized principles on standard- Content and Polynuclear Aromatic Content of Diesel
ization established in the Decision on Principles for the Fuels By Supercritical Fluid Chromatography
Development of International Standards, Guides and Recom- D5453 Test Method for Determination of Total Sulfur in
mendations issued by the World Trade Organization Technical Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel
Barriers to Trade (TBT) Committee. Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
D5967 Test Method for Evaluation of Diesel Engine Oils in
2. Referenced Documents
T-8 Diesel Engine
D6078 Test Method for Evaluating Lubricity of Diesel Fuels
2.1 ASTM Standards:
by the Scuffing Load Ball-on-Cylinder Lubricity Evalua-
D86 Test Method for Distillation of Petroleum Products and
tor (SLBOCLE) (Withdrawn 2021)
Liquid Fuels at Atmospheric Pressure
D6681 Test Method for Evaluation of Engine Oils in a High
D93 Test Methods for Flash Point by Pensky-Martens
Speed, Single-Cylinder Diesel Engine—Caterpillar 1P
Closed Cup Tester
Test Procedure
D97 Test Method for Pour Point of Petroleum Products
D6987/D6987M Test Method for Evaluation of Diesel En-
D130 Test Method for Corrosiveness to Copper from Petro-
gine Oils in T-10 Exhaust Gas Recirculation Diesel
leum Products by Copper Strip Test
Engine (Withdrawn 2022)
D235 Specification for Mineral Spirits (Petroleum Spirits)
E29 Practice for Using Significant Digits in Test Data to
(Hydrocarbon Dry Cleaning Solvent)
Determine Conformance with Specifications
D445 Test Method for Kinematic Viscosity of Transparent
E178 Practice for Dealing With Outlying Observations
and Opaque Liquids (and Calculation of Dynamic Viscos-
ity)
2.2 Other ASTM Document:
D482 Test Method for Ash from Petroleum Products ASTM Deposit Rating Manual 20 (formerly CRC Manual
D524 Test Method for Ramsbottom Carbon Residue of
20)
Petroleum Products
D613 Test Method for Cetane Number of Diesel Fuel Oil
3. Terminology
D664 Test Method for Acid Number of Petroleum Products
3.1 Definitions:
by Potentiometric Titration
3.1.1 blind reference oil, n—a reference oil, the identity of
D975 Specification for Diesel Fuel
which is unknown by the test facility.
D976 Test Method for Calculated Cetane Index of Distillate
3.1.1.1 Discussion—This is a coded reference oil that is
Fuels
submitted by a source independent of the test facility. D4175
D1319 Test Method for Hydrocarbon Types in Liquid Petro-
3.1.2 blowby, n—in internal combustion engines, the com-
leum Products by Fluorescent Indicator Adsorption
bustion products and unburned air-and-fuel mixture that enter
D2274 Test Method for Oxidation Stability of Distillate Fuel
the crankcase. D4175
Oil (Accelerated Method)
D2622 Test Method for Sulfur in Petroleum Products by
3.1.3 calibrate, v—to determine the indication or output of a
Wavelength Dispersive X-ray Fluorescence Spectrometry
measuring device with respect to that of a standard. D4175
D2709 Test Method for Water and Sediment in Middle
3.1.4 heavy duty, adj—in internal combustion engine
Distillate Fuels by Centrifuge
operation, characterized by average speeds, power output, and
D3524 Test Method for Diesel Fuel Diluent in Used Diesel
internal temperatures that are close to the potential maximums.
Engine Oils by Gas Chromatography
D4175
D4052 Test Method for Density, Relative Density, and API
3.1.5 heavy-duty engine, n—in internal combustion engine
Gravity of Liquids by Digital Density Meter
types, one that is designed to allow operation continuous at or
D4175 Terminology Relating to Petroleum Products, Liquid
close to its peak output.
Fuels, and Lubricants
3.1.5.1 Discussion—This type of engine is typically in-
D4294 Test Method for Sulfur in Petroleum and Petroleum
stalled in large trucks and buses as well as farm, industrial, and
Products by Energy Dispersive X-ray Fluorescence Spec-
construction equipment. D4175
trometry
4 5
For referenced ASTM standards, visit the ASTM website, www.astm.org, or The last approved version of this historical standard is referenced on
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM www.astm.org.
Standards volume information, refer to the standard’s Document Summary page on For Stock #TMCMNL20, visit the ASTM website, www.astm.org, or contact
the ASTM website. ASTM International Customer Service at service@astm.org.
D7549 − 23
3.1.6 non-reference oil, n—any oil other than a reference oil, 3.3.16 OC—oil consumption
such as a research formulation, commercial oil, or candidate
3.3.17 P/N—part number
oil. D4175
3.3.18 QI—quality index
3.1.7 non-standard test, n—a test that is not conducted in
3.3.19 RPTGC—reference relative top groove carbon pro-
conformance with the requirements in the standard test
file
method, such running on an uncalibrated test stand, using
3.3.20 SDTGCO—standard deviation top groove carbon
different test equipment, applying different equipment assem-
outlier
bly procedures, or using modified operating conditions. D4175
3.3.21 TGC—top groove carbon
3.1.8 reference oil, n—an oil of known performance
characteristics, used as a basis for comparison. 3.3.22 ULSD—ultra low sulfur diesel
3.1.8.1 Discussion—Reference oils are used to calibrate
4. Summary of Test Method
testing facilities, to compare the performance of other oils, or
4.1 This test method uses a Caterpillar production C13
to evaluate other materials (such as seals) that interact with
diesel engine (see Annex A3 for ordering information and list
oils. D4175
of engine build parts). Test operation includes a 60 min engine
3.1.9 test oil, n—any oil subjected to evaluation in an
warm-up and break-in, followed by a 4 h cool down and valve
established procedure.
lash adjustment. After the valve lash adjustment and any other
3.1.9.1 Discussion—It can be any oil selected by the labo-
needed adjustments, a 500 h test is begun. The engine is
ratory conducting the test. It could be an experimental product
operated under steady-state, rated-power conditions known to
or a commercially available oil. Often, it is an oil that is a
generate excessive piston deposits or oil consumption or both
candidate for approval against engine oil specifications (such
in field service. Report the total engine oil consumption as the
as manufacturers’ or military specifications, and so forth).
sum of the measured volumes in 50 h increments.
D4175
4.2 Equip the test stand with the appropriate instrumentation
3.1.10 wear, n—the loss of material from a surface, gener-
to control engine speed, fuel flow, and other operating param-
ally occurring between two surfaces in relative motion, and
eters.
resulting from mechanical or chemical action or a combination
4.3 Determine the engine oil performance by assessing
of both.
piston deposits and ring sticking, and oil consumption.
3.2 Definitions of Terms Specific to This Standard:
4.3.1 Prior to each test, clean and assemble the engine with
3.2.1 overhead, n—in internal combustion engines, the
new cylinder liners, pistons, piston rings, bearings and certain
components of the valve train located in or above the cylinder
valve train components. All aspects of the assembly are
head.
specified. After the test, dismantle the engine and examine and
3.2.2 tote, n—a container, smaller in capacity than a gallon.
rate the parts.
3.2.3 valve train, n—in internal combustion engines, the 4.3.2 A sample of engine oil is removed and an oil addition
series of components, such as valves, crossheads, rocker arms, is made at the end of each 50 h period. The volume of the oil
push rods and camshaft that open and close the intake and addition is the sum of the volume of sample plus the volume of
exhaust valves. oil consumed by the engine.
3.3 Abbreviations and Acronyms:
5. Significance and Use
3.3.1 ACERT—Advanced Combustion Emission Reduction
5.1 This test method assesses the performance of an engine
Technology
oil with respect to control of piston deposits and maintenance
3.3.2 ATGC—average top groove carbon
of oil consumption under heavy-duty operating conditions
selected to accelerate deposit formation in a turbocharged,
3.3.3 ATGCO—average top groove carbon offset
intercooled four-stroke-cycle diesel engine equipped with a
3.3.4 CARB—California Air Resources Board
combustion system that minimizes federally controlled exhaust
3.3.5 CAT—acronym for Caterpillar
gas emissions.
3.3.6 CRC—Coordinating Research Council
5.2 The results from this test method may be compared
3.3.7 DACA—Data Acquisition and Control Automation
against specification requirements to ascertain acceptance.
3.3.8 ECM—engine control module
5.3 The design of the test engine used in this test method is
representative of many, but not all, diesel engines. This factor,
3.3.9 EOT—end of test
along with the accelerated operating conditions, needs to be
3.3.10 HC—heavy carbon
considered when comparing test results against specification
3.3.11 IMP—intake manifold pressure
requirements.
3.3.12 LC—light carbon
6. Apparatus
3.3.13 LTMS—Lubricant Test Monitoring System
6.1 Test Engine Configuration:
3.3.14 MC—medium carbon
6.1.1 Test Engine—The test engine is a production 2004
3.3.15 NPT—National Pipe Thread Caterpillar 320 kW C13 engine, designed for heavy duty
D7549 − 23
on-highway truck use. It is an electronically controlled, 6.2.2 Intake Air System—With the exception of the air filter
turbocharged, after-cooled, direct injected, six cylinder diesel and intake air tube, the intake air system is not specified. See
engine with an in-block camshaft and a four-valve per cylinder Fig. X1.1 of a typical configuration. Use a suitable air filter.
arrangement. The engine uses Caterpillar’s ACERT technology Install the intake air tube (Fig. A4.6) at the intake of the
featuring multiple injections per cycle and inlet valve actuation
turbocharger compressor. The intake air tube is a minimum
control. It features a 2004 US EPA emissions configuration 305 mm of straight, nominal 102 mm diameter tubing. The
with electronic control of fuel metering, fuel injection timing
system configuration upstream of the air tube is not specified.
and inlet valve actuation timing. Critical parts that can affect
NOTE 1—Difficulty in achieving or maintaining intake manifold pres-
piston deposit formation are specified for oil test engine use.
sure or intake manifold temperature, or both, may be indicative of
See Annex A3 for source of the test engine and critical and
insufficient or excessive restriction.
non-critical parts.
6.2.3 Charge Air Cooler—In addition to the Caterpillar
6.1.2 Oil Heat Exchanger and Oil Heat System—Replace
supplied charge air cooler which is engine mounted, use
the standard Caterpillar oil heat exchanger core with a stainless
another cooler to simulate the air-to-air charge air cooler used
steal core, Caterpillar P/N 1Y-4026. Additionally install a
in most field applications. A Modine (P/N 1A012865) cooler
remotely mounted heat exchanger. Control the oil temperature
has been found suitable for this use. See A2.1 for instructions
with a dedicated cooling loop and control system which is
on obtaining this cooler. Alternatively, other charge air coolers
separate from the engine coolant (see Annex A12). Ensure that
may be used with the following limitations: (1) the cooler shall
the oil cooler bypass valve is blocked closed.
provide sufficient cooling capacity to control inlet manifold
6.1.3 Oil Pan Modification—Modify the oil pan as shown in
temperatures in the range specified elsewhere in this test
A4.1.
method; (2) the boost air pressure drop across the cooler not
6.1.4 Engine Control Module (ECM)—The ECM defines the
exceed 15 kPa; and (3) the cooler is equipped with a drain
desired engine fuel timing and quantity. It also limits maximum
system to remove condensate continuously from the boost air
engine speed and power. Caterpillar electronic governors are
cooler outlet side. Remove the coolant diverter valve dia-
designed to maintain a speed indicated by the throttle position
phragm for the Caterpillar supplied charge air cooler.
signal. Speed variation drives fuel demand (rack). Rack and
6.2.4 Exhaust System—Install the exhaust tube, see Fig.
engine speed are input to the injection duration and timing
A4.7, at the discharge flange of the turbocharger turbine
maps to determine duration and timing commands for the fuel
injectors. Obtain special oil test engine control software housing. The piping downstream of the exhaust tube is
required, but not specified. Provide a method to control exhaust
(module P/N 250-6775) for correct maps. Contact the Cater-
pillar oil test representative through TMC for installation of pressure.
this software. Use the Caterpillar engine technician (ET)
6.2.5 Fuel System—The fuel supply and filtration system is
service software package, version 2004B or later, to monitor
not specified. See Fig. X1.2 for a typical configuration.
engine parameters, flash software, and to change power and
Determine the fuel consumption rate by measuring the rate of
injector trim values. Use the full dealer version purchased from
fresh fuel flowing into the day tank. Provide a method to
a Caterpillar dealer with a yearly subscription.
control fuel temperature. Return the excess fuel from the
6.1.5 Crankshaft Position Sensor—Sense the crankshaft
engine into the day tank.
position using a primary sensor at the crankshaft gear and as
6.2.6 Coolant System—The system configuration is not
secondary sensor at the camshaft gear. The secondary sensor
specified. See Fig. X1.3 showing a typical configuration
provides position information during cranking and in the event
consisting of a non-ferrous core heat exchanger, a reservoir
of a primary sensor position failure. Calibrate the engine
(expansion tank) and a temperature control valve. Pressurize
control software before starting the timed test operation.
the system by regulating air pressure at the top of the expansion
6.1.6 Air Compressor—Do not use the engine-mounted air
tank. Ensure the system has a sight glass to detect air
compressor for this test method. Remove the air compressor
entrapment.
and install a block-off plate kit in its place (P/N 227-2574 cover
6.2.6.1 System volume is not specified. Avoid a very large
group and P/N 223-3873, plug group) (Fig. A4.5 or equiva-
volume as it may increase the time required for the engine
lent).
coolant to reach operating temperatures.
6.1.6.1 Modify the turbocharger waste-gate for manual
6.2.7 Pressurized Oil Fill System—The oil fill system is not
control by replacing the supplied pressure control with a
specified. A typical system includes an electric pump, a 50 L
manual linkage. See Figs. A4.21-A4.23.
reservoir, and a transfer hose. Fig. A4.24 shows the location of
6.2 Test Stand Configuration:
the pressurized oil fill system.
6.2.1 Engine Mounting—Install the engine so that it is
6.2.8 External Oil System—Configure the oil system ac-
upright and the crankshaft is horizontal.
cording to Fig. A5.1. The capacity of the oil reservoir is (10 to
6.2.1.1 Configure the engine mounting hardware to mini-
13) L. Ensure that the oil return is drawn from the bottom of
mize block distortion when the engine is fastened to the
the oil reservoir Fig. A4.9. Use Viking Pump Model No.
mounts. Excessive block distortion may influence test results.
SG053514. Locate the external oil pumps at an elevation that
is below the pump supply fitting on the oil pan. The nominal oil
pump motor speed is 1725 rpm. Figs. A4.1-A4.4 show the
Trademark of Caterpillar Inc., 100 North East Adams St., Peoria, IL 61629. pump supply and return port locations.
D7549 − 23
A
TABLE 1 Maximum Allowable System Time Responses TABLE 2 Cat ELC Coolant Concentrate and
Premix 50/50 Options
Measurement Time Response
B
Tote,
Container Size 3.8 L 19 L 208 L
Speed 2.0 s
275 g
Temperature 3.0 s
Concentrate P/N 119-5150 . 136-3707 .
Pressure 3.0 s
Premixed 50/50 P/N 101-2844 129-2151 101-2845 222-1534
Flow 45.0 s
A
Trademark of Caterpillar Inc., 100 North East Adams St., Peoria, IL 61629.
B
A small container.
6.2.8.1 Oil Sample Valve Location—Locate the oil sample
valve on the return line from the external oil system to the
7.3 Engine Coolant—Prepare the engine coolant by mixing
engine, and as close as possible to the return pump see Fig.
50 % volume of mineral-free water with 50 % volume of
A4.9 and Fig. A5.1.
Caterpillar brand coolant concentrate (As an option, pre-mixed
6.2.8.2 Unacceptable Oil System Materials—Do not use
coolant is available and may be used directly).
brass or copper fittings because they can adversely influence oil
7.3.1 Table 2 shows Caterpillar part numbers for several
wear metal analyses in the external oil system.
sized containers of concentrate or premixed coolant.
6.2.9 Crankcase Aspiration—Vent the blowby gas at the
7.3.2 The mineral-free water shall have a mineral content
blowby filter housing located at the left front side of the
not exceeding 34.4 mg/kg of total dissolved solids.
cylinder head cover (Fig. A4.10). Use crankcase breather P/N
7.3.3 The coolant mixture may be used for 6 test starts or up
9Y-4357. Use breather spacer P/N 221-3934 or equivalent
to 3400 h. The mixture shall remain at a 50/50 ratio during the
20 mm thick plate with a fully open center. Use a P/N 9Y-1758
course of the test. Verify by using either Caterpillar testers
gasket on each side of the spacer.
5P3514 or 5P0957 or an equivalent tester. Keep the coolant
6.2.10 Blowby Rate—See the general configuration of this
mixture free from contamination.
system in Fig. A4.10. The minimum internal volume of the
7.3.4 Keep the total solids below 5000 mg/kg.
blowby canister is 26.5 L. The inside diameter of the pipe
7.3.5 Maintain a correct additive level. Verify by checking
connecting the breather outlet to the blowby canister is 32 mm.
the coolant using Caterpillar test kit P/N 8T5296.
Incline the pipe downward to the canister. The hose connecting
7.4 Solvents and Cleaners Required: (Warning—Use ad-
the blowby canister to the flow rate measuring device is not
equate safety precautions with all solvents and cleaners.)
specified but shall match closely to the inlet of the device. The
7.4.1 Solvent—Use mineral spirits meeting Specification
flow rate measurement device is not specified. The J-TEC
8 D235, Type II, Class C requirements for aromatic content (0 %
Associates, Inc. Model No. YF563C does give satisfactory
to 2 % by vol), flash point (61 °C, min), and color (not darker
results under the conditions specified in this test method.
than +25 on Saybolt Scale or 25 on Pt-Co Scale). Obtain a
6.3 System Time Responses—The maximum allowable sys-
Certificate of Analysis for each batch of solvent from the
tem time responses are shown in Table 1. Determine system
supplier. (Warning—Combustible. Health Hazard.)
time responses in accordance with the Data Acquisition and
7.4.2 Pentane—Used for rinsing and cleaning components
Control Automation II (DACA II) Task Force Report.
before measurement. (Warning—Flammable. Health hazard.)
7.4.3 Heptane—Used for rinsing and cleaning components
6.4 Oil Sample Containers—Preferably use high-density
before measurement. (Warning—Flammable. Health hazard.)
polyethylene containers for oil samples. (Warning—Avoid
7.4.4 WD-40 —Used for rinsing and cleaning components
using glass containers which may break and cause injury or
before measurement. (Warning—Flammable. Health hazard.)
exposure to hazardous materials.)
7.4.5 Degreasing Solvent—EnSolv , a proprietary n-propyl
7. Engine Liquids and Cleaning Solvent
bromide based solvent that can be used for cleaning the second
rings. (Warning—Health hazard.)
7.1 Test Oil—Approximately 150 L of test oil is required to
complete the test.
8. Preparation of Apparatus
7.2 Test Fuel—Approximately 45 000 L of Chevron Philips
8.1 Cleaning of Parts:
PC-10 ultra low sulfur diesel fuel is required to complete the
test. Fuel property tolerances are shown in Annex A6.
WD-40 is a registered trademark of the WD-40 Company 9715 Businesspark
Ave., San Diego, CA 92131 USA, http://www.wd40.com. WD-40 is available from
The sole source of supply of the apparatus known to the committee at this time local retailers. The sole source of supply of this product known to the committee at
is J-TEC Associates, Inc., 5005 Blairs Forest Lane NE, Suite L, Cedar Rapids, IA this time is the WD-40 Company. If you are aware of alternative suppliers, please
52402, www.j-tecassociates.com. If you are aware of alternative suppliers, please provide this information to ASTM International Headquarters. Your comments will
provide this information to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of the responsible technical committee,
receive careful consideration at a meeting of the responsible technical committee, which you may attend.
which you may attend. EnSolv is a registered trademark of and is available from Enviro Tech
The sole source of supply of the apparatus known to the committee at this time International, Inc., 2525 West LeMoyne Ave., Melrose Park, IL 60160, http://
is Chevron Phillips Chemical Company LP, 10001 Six Pines Drive, Suite 4036B, www.ensolv.com. The sole source of supply of the EnSolv known to the committee
The Woodlands, TX 77387-4910, www.cpchem.com. If you are aware of alternative at this time is Enviro Tech International, Inc. If you are aware of alternative
suppliers, please provide this information to ASTM International Headquarters. suppliers, please provide this information to ASTM International Headquarters.
Your comments will receive careful consideration at a meeting of the responsible Your comments will receive careful consideration at a meeting of the responsible
1 1
technical committee, which you may attend. technical committee, which you may attend.
D7549 − 23
8.1.1 General—Preparation of test engine components spe- 8.2.6 Piston Cooling Tubes—Target the piston cooling
cific to the Caterpillar C13 test are indicated in this section. tubes. Contact TMC for directions.
Use the Caterpillar Service Manual Form SEN R 9700 8.2.7 New Parts—The following new parts are included in
(Annex A7) for the preparation of other components (except the Engine Build Parts List. They are not reusable, except as
for the piston second ring—see 8.2.7). Take precautions to noted in 10.3.3. Clean the parts prior to use. For piston second
protect rusting of iron components. Use of an engine parts rings and cylinder liners, clean with WD-40 and wipe with a
washer followed by a solvent wash is permitted. clean rag. After wiping the parts, rinse them with pentane or
8.1.2 Engine Block—Disassemble the engine, including re- heptane. Finally, coat the second rings and cylinder liners with
moval of the crankshaft, camshaft, piston cooling tubes, oil build-up oil. During a test, a replacement of any of the new
pump, and oil gallery plugs. Thoroughly clean the surfaces and parts listed below will invalidate the test.
oil passages (galleries). Use a nylon brush to clean the oil 8.2.7.1 Pistons.
passages. Removal of camshaft bearings is optional. 8.2.7.2 Piston rings (top, second and oil).
8.1.3 Cylinder Head, Intake System and Duct—Disassemble 8.2.7.3 Cylinder liners.
and clean these components before each test. Scrub with a 8.2.7.4 Valves (intake, exhaust).
nylon brush and solvent. Use of an engine parts washer 8.2.7.5 Valve guides.
followed by a solvent wash is permitted. 8.2.7.6 Valve seats.
8.1.4 Rocker Cover and Oil Pan—Clean the Rocker Cover 8.2.7.7 Connecting rod bearings, main bearings and thrust
and Oil Pan. Use a nylon brush, as necessary, to remove plate.
deposits.
8.3 Operational Measurements:
8.1.5 External Oil System—Flush the internal surfaces of
8.3.1 Units and Formats—See Annex A8.
the oil lines and the external reservoir with solvent. Repeat
8.3.2 Instrumentation Calibration:
until the solvent drains cleanly. Flush the solvent through the
8.3.2.1 Fuel Consumption Rate Measurement—Calibrate
oil pumps until the solvent drains cleanly, then air dry.
the fuel consumption rate measurement system before each
8.1.6 High Pressure Turbocharger—Carefully remove the
reference oil test sequence and within six months after comple-
turbine housing from the turbocharger and clean the waste-gate
tion of the last successful calibration test. Temperature-
valve with solvent and a soft wire brush.
compensate volumetric systems, and calibrate them against a
8.1.7 Cam Follower Assembly—Take the cam follower as-
standard mass flow device. The flowmeter on the test stand
sembly apart and inspect the bushings and pins. Replace the
shall agree within 0.2 % of the calibration standard, that
parts as necessary.
standard itself being calibrated against a national standard.
8.2 Engine Assembly: 8.3.2.2 Temperature Measurement Calibration—Calibrate
8.2.1 General—Except as noted in this section, use the the temperature measurement systems before each reference oil
procedures described in the Caterpillar Service Manual Form test sequence and within six months after completion of the last
SEN R 9700 (Annex A7). Assemble the engine with the successful calibration test. Each temperature measurement
components shown in the Engine Build Parts List (Annex A3). system shall agree within 60.5 °C of the laboratory calibration
8.2.2 Parts Reuse and Replacement—Reuse engine standard, that standard itself being calibrated against a national
components, except as noted in 8.2.7, and provided that they standard.
meet production tolerances as described in the Caterpillar 8.3.2.3 Pressure Measurement Calibration—Calibrate the
Service Manual. pressure measurement systems before each reference oil test
8.2.3 Build-up Oils—For the head, main caps, and rod bolts, sequence and within six months after completion of the last
use Exxon Mobil 600N engine oil as the build-up oil. For the successful calibration test. Confirm the calibration standard
rest of the engine build, use Mobil EF-411 engine oil or test against a national standard.
oil to lubricate the parts. If test oil is used, the engine build is 8.3.3 Temperature Measurement Locations:
valid only for the respective test oil. 8.3.3.1 General—See Table A14.1. The measurement
8.2.4 Coolant Thermostat—Lock the engine coolant ther- equipment is not specified. Install the sensors such that the tip
mostat open. is located midstream of the flow unless otherwise indicated.
8.2.5 Fuel Injectors—Use P/N 239-4908 fuel injectors. If The accuracy and measurement of the temperature measure-
fuel injectors are reused, exercise caution to avoid mechanical ment sensors and the complete measurement system shall
damage to or contamination of the nozzles. Dedicate the follow the guidelines in ASTM Research Report RR:D02-
injectors to a particular cylinder. Install the injectors according 1218.
to the method described in Caterpillar Service Manual Form 8.3.3.2 Coolant Out Temperature—Install the sensor in the
SENR9700 (Annex A7). Use Mobil EF-411 engine oil as the fitting on the thermostat housing (Fig. A4.12).
build-up oil for the injector o-rings. 8.3.3.3 Coolant In Temperature—Install the sensor on the
right side of the coolant pump intake housing at the 1-in. NPT
port (Fig. A4.13).
Available from a Caterpillar parts distributor.
The sole source of supply of the apparatus known to the committee at this time
is ExxonMobil Corporation, 3225 Gallows Road, Fairfax, VA 22037, www.exxon-
mobil.com. If you are aware of alternative suppliers, please provide this information Supporting data have been filed at ASTM International Headquarters and may
to ASTM International Headquarters. Your comments will receive careful consid- be obtained by requesting Research Report RR:D02-1218. Contact ASTM Customer
eration at a meeting of the responsible technical committee, which you may attend. Service at service@astm.org.
D7549 − 23
8.3.3.4 Fuel In Temperature—Install the sensor in the fuel 8.3.4.11 Additional Pressures—It is permissible to measure
pump inlet fitting (Fig. A4.15). any additional pressures that may be useful for test operation or
engine diagnostics.
8.3.3.5 Oil Gallery Temperature—Install the sensor at the
⁄4 in. NPT female boss on the right rear of the engine (Fig.
NOTE 3—See Fig. A4.19 and Fig. A4.20 for additional instrument
A4.14).
placement information.
8.3.3.6 Intake Air Temperature—Install the sensor in the
8.3.5 Flow Rate Measurement Locations:
inlet air tube 127 mm upstream of the compressor connection
8.3.5.1 General—The equipment for the blowby rate and
(Fig. A4.6).
fuel rate measurements is not specified. Follow the guidelines
8.3.3.7 Intake Manifold Temperature—Install the sensor at
in ASTM Research Report RR:D02-1218 for the accuracy
the ⁄8 in. NPT female boss on the outside radius of the inlet
and resolution of the flow rate measurement system.
manifold elbow (Fig. A4.16).
8.3.5.2 Blowby—The device used to measure the blowby
8.3.3.8 Exhaust Temperature—Install the sensor in the ex-
flow rate is not specified. See 6.2.10 for blowby measurement
haust tube (Fig. A4.7).
system configuration details.
8.3.3.9 Additional Temperatures—It is permissible to mea-
8.3.5.3 Fuel Flow—Determine the fuel consumption rate by
sure any additional temperatures that may be useful for test
measuring the fuel flowing to the day tank (Fig. X1.2).
operation or engine diagnostics.
8.3.5.4 Coolant Flow—Coolant flow rate measurement is
NOTE 2—Additional exhaust sensor locations, at the exhaust ports and
not a test requirement, but may be useful for diagnostic
pre-turbine (front and rear), are recommended. The detection of changes
purposes. The design and use of a coolant flow measuring
in exhaust temperatures is an important diagnostic feature.
system is optional.
8.3.4 Pressure Measurement Locations:
8.3.6 Humidity Measurement—Measure intake air humidity
8.3.4.1 General—The measurement equipment is not speci-
anywhere in the air intake system between air conditioning and
fied. Follow the guidelines in ASTM Research Report
the turbo inlet.
RR:D02-1218 for the accuracy and resolution of the pressure
measurement sensors and the complete measurement system. If
9. Engine/Stand Calibration and Non-Reference Oil Tests
the laboratory has problems with condensation forming in the
9.1 General—Calibrate the test stand by conducting a test
pressure lines, install a condensation trap at the lowest eleva-
with a blind reference oil. Submit the results to the TMC for
tion of the tubing between the pressure measurement location
determination of acceptance according to the Lubricant Test
and the final pressure sensor for crankcase pressure, intake air
Monitoring System (LTMS).
pressure, and exhaust pressure. Route the tubing to avoid
intermediate loops or low spots before and after the conden-
9.2 New Laboratories and New Test Stands:
sation trap. 9.2.1 New Laboratory—A new laboratory is any laboratory
8.3.4.2 Oil Gallery Pressure—Measure the pressure at the that has never previously calibrated a test stand by this test
⁄4 in. NPT fitting on the right rear of the engine (Fig. A4.14). method.
8.3.4.3 Oil Filter Inlet Pressure—Measure the pressure at 9.2.2 New Test Stand—A new test stand is a test cell and
the plug located on the inlet side of the oil filter assembly (Fig.
support hardware that has never previously been calibrated by
A4.8). this test method. Perform a calibration (9.2.3) to introduce a
8.3.4.4 Inlet Manifold Pressure—Measure the pressure at new test stand.
the ⁄4 in. NPT port on the outside radius of the inlet manifold
9.2.3 New Test Stand Calibration—Calibrate a new test
elbow (Fig. A4.16). stand in accordance with the LTMS.
8.3.4.5 Crankcase Pressure—Measure the pressure by in-
9.3 Stand Calibration Period—The calibration period is 12
stalling a bulkhead fitting in the valve cover, top-front (Fig.
operationally valid (Annex A11) non-reference oil tests or
A4.11).
12 months, whichever comes first, from the EOT date of the
8.3.4.6 Intake Air Pressure—Measure the pressure at a wall
last acceptable reference oil test.
tap on the intake air tube 153 mm upstream of the compressor
9.4 Stand Modification and Calibration Status—Stand cali-
connection (Fig. A4.6).
bration status will be invalidated by conducting any non-
8.3.4.7 Exhaust Pressure—Measure the pressure on the
standard test or modification of the test and control systems, or
exhaust tube (Fig. A4.7).
both. A non-standard test is any test conducted under a
8.3.4.8 Fuel Pressure—Measure the pressure at the fuel
modified procedure, non-procedural hardware, controller set-
filter head (Fig. A4.25).
point modifications, or any combination thereof. If changes are
8.3.4.9 Coolant Pressure—Measure the pressure on top of
contemplated, contact the TMC beforehand to ascertain the
the expansion tank (Fig. X1.3).
effect on the calibration status.
8.3.4.10 Intercooler Delta Pressure—Measure the pressure
9.5 Test Numbering System:
drop across the intercooler. Measure the intercooler inlet
pressure at the elbow outlet of the CAT charge air cooler (Fig. 9.5.1 General—The test number has two parts, X and Y. X
A4.19). Use the intake manifold pressure (8.3.4.4) as the represents the test stand number and Y represents the sequen-
intercooler outlet pressure. The intercooler delta pressure is the tial test stand run number. For example 27-15 indicates test
difference between the intercooler outlet pressure and the stand number 27 and test stand run number 15. The test stand
intercooler inlet pressure. run number, Y will increase sequentially by one for each test
D7549 − 23
start (reference oil or non-reference oil). A letter suffix may intervals between reference oil tests. These extensions shall not
also be necessary (see 9.5.2). exceed one regular calibration period.
9.5.2 Reference Oil Tests—A reference oil test conducted
9.10.3 Reference Oil Test Data Flow—To ensure continuous
subsequent to an unacceptable reference oil test shall include a severity and precision monitoring, calibration tests are con-
letter suffix after Y. The letter suffix shall begin with A and
ducted periodically throughout the year. There may be occa-
incremented alphabetically until acceptable reference oil test is sions when laboratories conduct a large portion of calibration
completed. For example, if two consecutive unacceptable
tests in a short period of time. This could result in an
reference oil tests were conducted and the first number was unacceptably large time frame when very few calibration tests
27-15, the second test number would be 27-16A. A third
are conducted. The TMC can shorten or extend calibration
calibration attempt would have the test number 27-17B. If the periods as needed to provide a consistent flow of reference oil
third test were acceptable, then 27-17B would identify the
test data. Adjustments to calibration periods are made such that
reference oil test in the test report. laboratories incur no net loss (or gain) in calibration status.
9.5.3 Non-Reference Oil Tests—Add no letter suffix to Y for
9.10.4 Special Use of the Reference Oil Calibration
aborted or operationally invalid non-reference oil tests. System—The surveillance panel has the option to use the
reference oil system to evaluate changes that have potential
9.6 Reference Oil Test Acceptance—Determine reference oil
6 impact on test severity and precision. This option is only taken
test acceptance in accordance with the LTMS.
when a program of donated tests is not feasible. The surveil-
9.7 Reference Oil Accountability:
lance panel and the TMC shall develop a detailed plan for the
9.7.1 Keep full accounts of the identification and quantities
test program. This plan requires all reference oil tests in the
of all reference oils used. With the exception of the oil analyses
program to be completed as close to the same time as possible,
required in 11.3, perform no chemical or physical analyses on
so that no laboratory or stand calibration is left in an exces-
reference oils without written permission from the TMC. In
sively long pending status. In order to obtain the integrity of
such an event, include the written confirmation and the
the reference oil monitoring system each reference oil test is
analytical results generated in the reference oil test report.
conducted so as to be interpretable for stand calibration. To
9.7.2 Retain used reference oil samples for 90 days from the
facilitate the required test scheduling, the surveillance panel
EOT date.
may direct the TMC to lengthen and shorten reference oil
9.8 Non-Reference Oil Tests: Last Start Date—When run- calibration periods within laboratories such that the laborato-
ning a non-reference oil test during the calibration period; ries incur no net loss (or gain) in calibration status.
crank the engine prior to the expiration of the calibration period
9.11 Calibration of Piston and Ring Deposit Raters—Each
(9.3).
calendar year, each laboratory shall send at least one Heavy
9.9 Donated Reference Oil Test Programs—The surveil- Duty Diesel Rater to the ASTM Standardized Testing Deposit
lance panel is charged with maintaining effective reference oil
Rating Workshop. Each rater shall rate a minimum of six diesel
test severity and precision monitoring. During times of new pistons and one set of C13 rings. If this schedule is not suitable
parts introductions, new or re-blended reference oil additions, to a particular rater or test laboratory, then make alternative
and procedural revisions, it may be necessary to evaluate the arrangements as soon as possible to have the rater calibrated.
possible effects on severity and precision levels. The surveil-
lance panel may choose to conduct a program of donated 10. Procedure
reference oil tests in those laboratories participating in the
10.1 Engine Installation and Stand Connections—Install the
monitoring system to quantify the effect of a particular change
test engine on the stand and connect the engine to the stand
on severity and precision. Typically the surveillance panel
support equipment.
requests its panel members to volunteer enough reference oil
10.2 Coolant System Fill—Fill the cooling system with
test results to create a robust data set. Broad laboratory
pre-diluted Caterpillar Extended Life Coolant (see 7.3 for part
participation is needed to provide a representative sampling of
numbers and available container sizes). The coolant for non-
the industry. To ensure the quality of the data obtained, donated
reference oil tests may be reused provided the level of
tests are conducted on calibrated test stands. The surveillance
inhibitors is within specification requirements. Use new cool-
panel shall arrange an appropriate number of donated tests and
ant for each reference oil test. Pressurize the cooling system as
ensure completion of the test program in a timely manner.
required by the specification and check for leaks prior to
9.10 Adjustment to Reference Oil Calibration Periods:
adding the test oil.
9.10.1 Procedural Deviations—On occasions when a labo-
10.3 Oil Fill for Break-in and Test:
ratory becomes aware of a significant deviation from the test
10.3.1 Install a new Caterpillar 1R-1808 oil filter.
method, such as
...


This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D7549 − 21 D7549 − 23
Standard Test Method for
Evaluation of Heavy-Duty Engine Oils under High Output
Conditions—Caterpillar C13 Test Procedure
This standard is issued under the fixed designation D7549; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
Any properly equipped laboratory, without outside assistance, can use the test procedure described
in this test method. The ASTM Test Monitoring Center (TMC) provides calibration and an
assessment of the test results obtained on those oils by the laboratory. By this means the laboratory
will know whether its use of the test method gives results statistically similar to those obtained by
other laboratories. Furthermore, various agencies require that a laboratory utilizes the TMC services
in seeking qualification of oils against specifications. For example, the U.S. Army has such a
requirement in some of its engine oil specifications. Accordingly, this test method is written for those
laboratories that use the TMC services. Laboratories that choose not to use these services should
ignore those portions of the test method that refer to the TMC. Information letters issued periodically
by the TMC may modify this test method. In addition the TMC may issue supplementary memoranda
related to the test method.
ASTM International policy is to encourage the development of test procedures based on generic
equipment. It is recognized that there are occasions where critical/sole-source equipment has been
approved by the technical committee (surveillance panel/task force) and is required by the test
procedure. The technical committee that oversees the test procedure is encouraged to clearly identify
if the part is considered critical in the test procedure. If a part is deemed to be critical, ASTM
encourages alternative suppliers to be given the opportunity for consideration of supplying the critical
part/component providing they meet the approval process set forth by the technical committee.
An alternative supplier can start the process by initiating contact with the technical committee
(current chairs shown on ASTM TMC website). The supplier should advise on the details of the part
that is intended to be supplied. The technical committee will review the request and determine
feasibility of an alternative supplier for the requested replacement critical part. In the event that a
replacement critical part has been identified and proven equivalent, the sole-source supplier footnote
shall be removed from the test procedure.
1. Scope*
1.1 The test method covers a heavy-duty engine test procedure under high output conditions to evaluate engine oil performance
This test method is under the jurisdiction of ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of Subcommittee
D02.B0 on Automotive Lubricants.
Current edition approved April 1, 2021July 1, 2023. Published April 2021July 2023. Originally published in 2009. Last previous edition approved in 20192021 as
D7549 – 19.D7549 – 21. DOI: 10.1520/D7549-21.10.1520/D7549-23.
The ASTM Test Monitoring Center will update changes in this test method by means of Information Letters. This edition includes all information letters through No.
20-1.23-1. Information Letters may be obtained by from the ASTM Test Monitoring Center, 6555 Penn Avenue, Pittsburgh, PA 15206-4489, Attention: Administrator.203
Armstrong Drive, Freeport, PA 16229, Attention: Director.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D7549 − 23
with regard to piston deposit formation, piston ring sticking and oil consumption control in a combustion environment designed
to minimize exhaust emissions. This test method is commonly referred to as the Caterpillar C13 Heavy-Duty Engine Oil Test.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.2.1 Exceptions—Where there are no SI equivalent such as screw threads, National Pipe Treads (NPT), and tubing sizes.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of
regulatory limitations prior to use. See Annex A1 for general safety precautions.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2.1 ASTM Standards:
D86 Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure
D93 Test Methods for Flash Point by Pensky-Martens Closed Cup Tester
D97 Test Method for Pour Point of Petroleum Products
D130 Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip Test
D235 Specification for Mineral Spirits (Petroleum Spirits) (Hydrocarbon Dry Cleaning Solvent)
D445 Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
D482 Test Method for Ash from Petroleum Products
D524 Test Method for Ramsbottom Carbon Residue of Petroleum Products
D613 Test Method for Cetane Number of Diesel Fuel Oil
D664 Test Method for Acid Number of Petroleum Products by Potentiometric Titration
D975 Specification for Diesel Fuel
D976 Test Method for Calculated Cetane Index of Distillate Fuels
D1319 Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
D2274 Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)
D2622 Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
D2709 Test Method for Water and Sediment in Middle Distillate Fuels by Centrifuge
D3524 Test Method for Diesel Fuel Diluent in Used Diesel Engine Oils by Gas Chromatography
D4052 Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
D4175 Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
D4294 Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
D4739 Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration
D5185 Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively
Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
D5186 Test Method for Determination of the Aromatic Content and Polynuclear Aromatic Content of Diesel Fuels By
Supercritical Fluid Chromatography
D5453 Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel,
and Engine Oil by Ultraviolet Fluorescence
D5967 Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine
D6078 Test Method for Evaluating Lubricity of Diesel Fuels by the Scuffing Load Ball-on-Cylinder Lubricity Evaluator
(SLBOCLE) (Withdrawn 2021)
D6681 Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1P Test
Procedure
D6987/D6987M Test Method for Evaluation of Diesel Engine Oils in T-10 Exhaust Gas Recirculation Diesel Engine
(Withdrawn 2022)
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E178 Practice for Dealing With Outlying Observations
Caterpillar Inc., Engine System Technology Development, PO Box 610, Mossville, IL 61552-0610.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
The last approved version of this historical standard is referenced on www.astm.org.
D7549 − 23
2.2 Other ASTM Document:
ASTM Deposit Rating Manual 20 (formerly CRC Manual 20)
3. Terminology
3.1 Definitions:
3.1.1 blind reference oil, n—a reference oil, the identity of which is unknown by the test facility.
3.1.1.1 Discussion—
This is a coded reference oil that is submitted by a source independent of the test facility. D4175
3.1.2 blowby, n—in internal combustion engines, the combustion products and unburned air-and-fuel mixture that enter the
crankcase. D4175
3.1.3 calibrate, v—to determine the indication or output of a measuring device with respect to that of a standard. D4175
3.1.4 heavy duty, adj—in internal combustion engine operation, characterized by average speeds, power output, and internal
temperatures that are close to the potential maximums. D4175
3.1.5 heavy-duty engine, n—in internal combustion engine types, one that is designed to allow operation continuous at or close
to its peak output.
3.1.5.1 Discussion—
This type of engine is typically installed in large trucks and buses as well as farm, industrial, and construction equipment. D4175
3.1.6 non-reference oil, n—any oil other than a reference oil, such as a research formulation, commercial oil, or candidate oil.
D4175
3.1.7 non-standard test, n—a test that is not conducted in conformance with the requirements in the standard test method, such
running on an uncalibrated test stand, using different test equipment, applying different equipment assembly procedures, or using
modified operating conditions. D4175
3.1.8 reference oil, n—an oil of known performance characteristics, used as a basis for comparison.
3.1.8.1 Discussion—
Reference oils are used to calibrate testing facilities, to compare the performance of other oils, or to evaluate other materials (such
as seals) that interact with oils. D4175
3.1.9 test oil, n—any oil subjected to evaluation in an established procedure.
3.1.9.1 Discussion—
It can be any oil selected by the laboratory conducting the test. It could be an experimental product or a commercially available
oil. Often, it is an oil that is a candidate for approval against engine oil specifications (such as manufacturers’ or military
specifications, and so forth). D4175
3.1.10 wear, n—the loss of material from a surface, generally occurring between two surfaces in relative motion, and resulting
from mechanical or chemical action or a combination of both.
3.2 Definitions of Terms Specific to This Standard:
3.2.1 overhead, n—in internal combustion engines, the components of the valve train located in or above the cylinder head.
3.2.2 tote, n—a container, smaller in capacity than a gallon.
3.2.3 valve train, n—in internal combustion engines, the series of components, such as valves, crossheads, rocker arms, push rods
and camshaft that open and close the intake and exhaust valves.
3.3 Abbreviations and Acronyms:
For Stock #TMCMNL20, visit the ASTM website, www.astm.org, or contact ASTM International Customer Service at service@astm.org.
D7549 − 23
3.3.1 ACERT—Advanced Combustion Emission Reduction Technology
3.3.2 ATGC—average top groove carbon
3.3.3 ATGCO—average top groove carbon offset
3.3.4 CARB—California Air Resources Board
3.3.5 CAT—acronym for Caterpillar
3.3.6 CRC—Coordinating Research Council
3.3.7 DACA—Data Acquisition and Control Automation
3.3.8 ECM—engine control module
3.3.9 EOT—end of test
3.3.10 HC—heavy carbon
3.3.11 IMP—intake manifold pressure
3.3.12 LC—light carbon
3.3.13 LTMS—Lubricant Test Monitoring System
3.3.14 MC—medium carbon
3.3.15 NPT—National Pipe Thread
3.3.16 OC—oil consumption
3.3.17 P/N—part number
3.3.18 QI—quality index
3.3.19 RPTGC—reference relative top groove carbon profile
3.3.20 SDTGCO—standard deviation top groove carbon outlier
3.3.21 TGC—top groove carbon
3.3.22 ULSD—ultra low sulfur diesel
4. Summary of Test Method
4.1 This test method uses a Caterpillar production C13 diesel engine (see Annex A3 for ordering information and list of engine
build parts). Test operation includes a 60 min engine warm-up and break-in, followed by a 4 h cool down and valve lash
adjustment. After the valve lash adjustment and any other needed adjustments, a 500 h test is begun. The engine is operated under
steady-state, rated-power conditions known to generate excessive piston deposits or oil consumption or both in field service. Report
the total engine oil consumption as the sum of the measured volumes in 50 h increments.
D7549 − 23
4.2 Equip the test stand with the appropriate instrumentation to control engine speed, fuel flow, and other operating parameters.
4.3 Determine the engine oil performance by assessing piston deposits and ring sticking, and oil consumption.
4.3.1 Prior to each test, clean and assemble the engine with new cylinder liners, pistons, piston rings, bearings and certain valve
train components. All aspects of the assembly are specified. After the test, dismantle the engine and examine and rate the parts.
4.3.2 A sample of engine oil is removed and an oil addition is made at the end of each 50 h period. The volume of the oil addition
is the sum of the volume of sample plus the volume of oil consumed by the engine.
5. Significance and Use
5.1 This test method assesses the performance of an engine oil with respect to control of piston deposits and maintenance of oil
consumption under heavy-duty operating conditions selected to accelerate deposit formation in a turbocharged, intercooled
four-stroke-cycle diesel engine equipped with a combustion system that minimizes federally controlled exhaust gas emissions.
5.2 The results from this test method may be compared against specification requirements to ascertain acceptance.
5.3 The design of the test engine used in this test method is representative of many, but not all, diesel engines. This factor, along
with the accelerated operating conditions, needs to be considered when comparing test results against specification requirements.
6. Apparatus
6.1 Test Engine Configuration:
6.1.1 Test Engine—The test engine is a production 2004 Caterpillar 320 kW C13 engine, designed for heavy duty on-highway
truck use. It is an electronically controlled, turbocharged, after-cooled, direct injected, six cylinder diesel engine with an in-block
camshaft and a four-valve per cylinder arrangement. The engine uses Caterpillar’s ACERT technology featuring multiple injections
per cycle and inlet valve actuation control. It features a 2004 US EPA emissions configuration with electronic control of fuel
metering, fuel injection timing and inlet valve actuation timing. Critical parts that can affect piston deposit formation are specified
for oil test engine use. See Annex A3 for source of the test engine and critical and non-critical parts.
6.1.2 Oil Heat Exchanger and Oil Heat System—Replace the standard Caterpillar oil heat exchanger core with a stainless steal
core, Caterpillar P/N 1Y-4026. Additionally install a remotely mounted heat exchanger. Control the oil temperature with a
dedicated cooling loop and control system which is separate from the engine coolant (see Annex A12). Ensure that the oil cooler
bypass valve is blocked closed.
6.1.3 Oil Pan Modification—Modify the oil pan as shown in A4.1.
6.1.4 Engine Control Module (ECM)—The ECM defines the desired engine fuel timing and quantity. It also limits maximum
engine speed and power. Caterpillar electronic governors are designed to maintain a speed indicated by the throttle position signal.
Speed variation drives fuel demand (rack). Rack and engine speed are input to the injection duration and timing maps to determine
duration and timing commands for the fuel injectors. Obtain special oil test engine control software (module P/N 250-6775) for
correct maps. Contact the Caterpillar oil test representative through TMC for installation of this software. Use the Caterpillar
engine technician (ET) service software package, version 2004B or later, to monitor engine parameters, flash software, and to
change power and injector trim values. Use the full dealer version purchased from a Caterpillar dealer with a yearly subscription.
6.1.5 Crankshaft Position Sensor—Sense the crankshaft position using a primary sensor at the crankshaft gear and as secondary
sensor at the camshaft gear. The secondary sensor provides position information during cranking and in the event of a primary
sensor position failure. Calibrate the engine control software before starting the timed test operation.
6.1.6 Air Compressor—Do not use the engine-mounted air compressor for this test method. Remove the air compressor and install
a block-off plate kit in its place (P/N 227-2574 cover group and P/N 223-3873, plug group) (Fig. A4.5 or equivalent).
Trademark of Caterpillar Inc., 100 North East Adams St., Peoria, IL 61629.
D7549 − 23
6.1.6.1 Modify the turbocharger waste-gate for manual control by replacing the supplied pressure control with a manual linkage.
See Figs. A4.21-A4.23.
6.2 Test Stand Configuration:
6.2.1 Engine Mounting—Install the engine so that it is upright and the crankshaft is horizontal.
6.2.1.1 Configure the engine mounting hardware to minimize block distortion when the engine is fastened to the mounts.
Excessive block distortion may influence test results.
6.2.2 Intake Air System—With the exception of the air filter and intake air tube, the intake air system is not specified. See Fig. X1.1
of a typical configuration. Use a suitable air filter. Install the intake air tube (Fig. A4.6) at the intake of the turbocharger compressor.
The intake air tube is a minimum 305 mm of straight, nominal 102 mm diameter tubing. The system configuration upstream of the
air tube is not specified.
NOTE 1—Difficulty in achieving or maintaining intake manifold pressure or intake manifold temperature, or both, may be indicative of insufficient or
excessive restriction.
6.2.3 Charge Air Cooler—In addition to the Caterpillar supplied charge air cooler which is engine mounted, use another cooler
to simulate the air-to-air charge air cooler used in most field applications. A Modine (P/N 1A012865) cooler has been found
suitable for this use. See A2.1 for instructions on obtaining this cooler. Alternatively, other charge air coolers may be used with
the following limitations: (1) the cooler shall provide sufficient cooling capacity to control inlet manifold temperatures in the range
specified elsewhere in this test method; (2) the boost air pressure drop across the cooler not exceed 15 kPa; and (3) the cooler is
equipped with a drain system to remove condensate continuously from the boost air cooler outlet side. Remove the coolant diverter
valve diaphragm for the Caterpillar supplied charge air cooler.
6.2.4 Exhaust System—Install the exhaust tube, see Fig. A4.7, at the discharge flange of the turbocharger turbine housing. The
piping downstream of the exhaust tube is required, but not specified. Provide a method to control exhaust pressure.
6.2.5 Fuel System—The fuel supply and filtration system is not specified. See Fig. X1.2 for a typical configuration. Determine the
fuel consumption rate by measuring the rate of fresh fuel flowing into the day tank. Provide a method to control fuel temperature.
Return the excess fuel from the engine into the day tank.
6.2.6 Coolant System—The system configuration is not specified. See Fig. X1.3 showing a typical configuration consisting of a
non-ferrous core heat exchanger, a reservoir (expansion tank) and a temperature control valve. Pressurize the system by regulating
air pressure at the top of the expansion tank. Ensure the system has a sight glass to detect air entrapment.
6.2.6.1 System volume is not specified. Avoid a very large volume as it may increase the time required for the engine coolant to
reach operating temperatures.
6.2.7 Pressurized Oil Fill System—The oil fill system is not specified. A typical system includes an electric pump, a 50 L reservoir,
and a transfer hose. Fig. A4.24 shows the location of the pressurized oil fill system.
6.2.8 External Oil System—Configure the oil system according to Fig. A5.1. The capacity of the oil reservoir is (10 to 13) L.
Ensure that the oil return is drawn from the bottom of the oil reservoir Fig. A4.9. Use Viking Pump Model No. SG053514. Locate
the external oil pumps at an elevation that is below the pump supply fitting on the oil pan. The nominal oil pump motor speed is
1725 rpm. Figs. A4.1-A4.4 show the pump supply and return port locations.
6.2.8.1 Oil Sample Valve Location—Locate the oil sample valve on the return line from the external oil system to the engine, and
as close as possible to the return pump see Fig. A4.9 and Fig. A5.1.
6.2.8.2 Unacceptable Oil System Materials—Do not use brass or copper fittings because they can adversely influence oil wear
metal analyses in the external oil system.
6.2.9 Crankcase Aspiration—Vent the blowby gas at the blowby filter housing located at the left front side of the cylinder head
cover (Fig. A4.10). Use crankcase breather P/N 9Y-4357. Use breather spacer P/N 221-3934 or equivalent 20 mm thick plate with
a fully open center. Use a P/N 9Y-1758 gasket on each side of the spacer.
D7549 − 23
TABLE 1 Maximum Allowable System Time Responses
Measurement Time Response
Speed 2.0 s
Temperature 3.0 s
Pressure 3.0 s
Flow 45.0 s
6.2.10 Blowby Rate—See the general configuration of this system in Fig. A4.10. The minimum internal volume of the blowby
canister is 26.5 L. The inside diameter of the pipe connecting the breather outlet to the blowby canister is 32 mm. Incline the pipe
downward to the canister. The hose connecting the blowby canister to the flow rate measuring device is not specified but shall
match closely to the inlet of the device. The flow rate measurement device is not specified. The J-TEC Associates, Inc. Model No.
YF563C does give satisfactory results under the conditions specified in this test method.
6.3 System Time Responses—The maximum allowable system time responses are shown in Table 1. Determine system time
responses in accordance with the Data Acquisition and Control Automation II (DACA II) Task Force Report.
6.4 Oil Sample Containers—Preferably use high-density polyethylene containers for oil samples. (Warning—Avoid using glass
containers which may break and cause injury or exposure to hazardous materials.)
7. Engine Liquids and Cleaning Solvent
7.1 Test Oil—Approximately 150 L of test oil is required to complete the test.
7.2 Test Fuel—Approximately 45 000 L of Chevron Philips PC-10 ultra low sulfur diesel fuel is required to complete the test.
Fuel property tolerances are shown in Annex A6.
7.3 Engine Coolant—Prepare the engine coolant by mixing 50 % volume of mineral-free water with 50 % volume of Caterpillar
brand coolant concentrate (As an option, pre-mixed coolant is available and may be used directly).
7.3.1 Table 2 shows Caterpillar part numbers for several sized containers of concentrate or premixed coolant.
7.3.2 The mineral-free water shall have a mineral content not exceeding 34.4 mg/kg of total dissolved solids.
7.3.3 The coolant mixture may be used for 6 test starts or up to 3400 h. The mixture shall remain at a 50/50 ratio during the course
of the test. Verify by using either Caterpillar testers 5P3514 or 5P0957 or an equivalent tester. Keep the coolant mixture free from
contamination.
7.3.4 Keep the total solids below 5000 mg/kg.
7.3.5 Maintain a correct additive level. Verify by checking the coolant using Caterpillar test kit P/N 8T5296.
7.4 Solvents and Cleaners Required: (Warning—Use adequate safety precautions with all solvents and cleaners.)
7.4.1 Solvent—Use mineral spirits meeting Specification D235, Type II, Class C requirements for aromatic content (0 % to 2 %
by vol), flash point (61 °C, min), and color (not darker than +25 on Saybolt Scale or 25 on Pt-Co Scale). Obtain a Certificate of
Analysis for each batch of solvent from the supplier. (Warning—Combustible. Health Hazard.)
7.4.2 Pentane—Used for rinsing and cleaning components before measurement. (Warning—Flammable. Health hazard.)
The sole source of supply of the apparatus known to the committee at this time is J-TEC Associates, Inc., 5005 Blairs Forest Lane NE, Suite L, Cedar Rapids, IA 52402,
www.j-tecassociates.com. If you are aware of alternative suppliers, please provide this information to ASTM International Headquarters. Your comments will receive careful
consideration at a meeting of the responsible technical committee, which you may attend.
The sole source of supply of the apparatus known to the committee at this time is Chevron Phillips Chemical Company LP, 10001 Six Pines Drive, Suite 4036B, The
Woodlands, TX 77387-4910, www.cpchem.com. If you are aware of alternative suppliers, please provide this information to ASTM International Headquarters. Your
comments will receive careful consideration at a meeting of the responsible technical committee, which you may attend.
D7549 − 23
A
TABLE 2 Cat ELC Coolant Concentrate and
Premix 50/50 Options
B
Tote,
Container Size 3.8 L 19 L 208 L
275 g
Concentrate P/N 119-5150 . 136-3707 .
Premixed 50/50 P/N 101-2844 129-2151 101-2845 222-1534
A
Trademark of Caterpillar Inc., 100 North East Adams St., Peoria, IL 61629.
B
A small container.
7.4.3 Heptane—Used for rinsing and cleaning components before measurement. (Warning—Flammable. Health hazard.)
7.4.4 WD-40 —Used for rinsing and cleaning components before measurement. (Warning—Flammable. Health hazard.)
7.4.5 Degreasing Solvent—EnSolv , a proprietary n-propyl bromide based solvent that can be used for cleaning the second rings.
(Warning—Health hazard.)
8. Preparation of Apparatus
8.1 Cleaning of Parts:
8.1.1 General—Preparation of test engine components specific to the Caterpillar C13 test are indicated in this section. Use the
Caterpillar Service Manual Form SEN R 9700 (Annex A7) for the preparation of other components (except for the piston second
ring—see 8.2.7). Take precautions to protect rusting of iron components. Use of an engine parts washer followed by a solvent wash
is permitted.
8.1.2 Engine Block—Disassemble the engine, including removal of the crankshaft, camshaft, piston cooling tubes, oil pump, and
oil gallery plugs. Thoroughly clean the surfaces and oil passages (galleries). Use a nylon brush to clean the oil passages. Removal
of camshaft bearings is optional.
8.1.3 Cylinder Head, Intake System and Duct—Disassemble and clean these components before each test. Scrub with a nylon
brush and solvent. Use of an engine parts washer followed by a solvent wash is permitted.
8.1.4 Rocker Cover and Oil Pan—Clean the Rocker Cover and Oil Pan. Use a nylon brush, as necessary, to remove deposits.
8.1.5 External Oil System—Flush the internal surfaces of the oil lines and the external reservoir with solvent. Repeat until the
solvent drains cleanly. Flush the solvent through the oil pumps until the solvent drains cleanly, then air dry.
8.1.6 High Pressure Turbocharger—Carefully remove the turbine housing from the turbocharger and clean the waste-gate valve
with solvent and a soft wire brush.
8.1.7 Cam Follower Assembly—Take the cam follower assembly apart and inspect the bushings and pins. Replace the parts as
necessary.
8.2 Engine Assembly:
8.2.1 General—Except as noted in this section, use the procedures described in the Caterpillar Service Manual Form SEN R
9700 (Annex A7). Assemble the engine with the components shown in the Engine Build Parts List (Annex A3).
WD-40 is a registered trademark of the WD-40 Company 9715 Businesspark Ave., San Diego, CA 92131 USA, http://www.wd40.com. WD-40 is available from local
retailers. The sole source of supply of this product known to the committee at this time is the WD-40 Company. If you are aware of alternative suppliers, please provide this
information to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of the responsible technical committee, which you may
attend.
EnSolv is a registered trademark of and is available from Enviro Tech International, Inc., 2525 West LeMoyne Ave., Melrose Park, IL 60160, http://www.ensolv.com.
The sole source of supply of the EnSolv known to the committee at this time is Enviro Tech International, Inc. If you are aware of alternative suppliers, please provide this
information to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of the responsible technical committee, which you may
attend.
Available from a Caterpillar parts distributor.
D7549 − 23
8.2.2 Parts Reuse and Replacement—Reuse engine components, except as noted in 8.2.7, and provided that they meet production
tolerances as described in the Caterpillar Service Manual.
8.2.3 Build-up Oils—For the head, main caps, and rod bolts, use Exxon Mobil 600N engine oil as the build-up oil. For the rest
of the engine build, use Mobil EF-411 engine oil or test oil to lubricate the parts. If test oil is used, the engine build is valid only
for the respective test oil.
8.2.4 Coolant Thermostat—Lock the engine coolant thermostat open.
8.2.5 Fuel Injectors—Use P/N 239-4908 fuel injectors. If fuel injectors are reused, exercise caution to avoid mechanical damage
to or contamination of the nozzles. Dedicate the injectors to a particular cylinder. Install the injectors according to the method
described in Caterpillar Service Manual Form SENR9700 (Annex A7). Use Mobil EF-411 engine oil as the build-up oil for the
injector o-rings.
8.2.6 Piston Cooling Tubes—Target the piston cooling tubes. Contact TMC for directions.
8.2.7 New Parts—The following new parts are included in the Engine Build Parts List. They are not reusable, except as noted in
10.3.3. Clean the parts prior to use. For piston second rings and cylinder liners, clean with WD-40 and wipe with a clean rag. After
wiping the parts, rinse them with pentane or heptane. Finally, coat the second rings and cylinder liners with build-up oil. During
a test, a replacement of any of the new parts listed below will invalidate the test.
8.2.7.1 Pistons.
8.2.7.2 Piston rings (top, second and oil).
8.2.7.3 Cylinder liners.
8.2.7.4 Valves (intake, exhaust).
8.2.7.5 Valve guides.
8.2.7.6 Valve seats.
8.2.7.7 Connecting rod bearings, main bearings and thrust plate.
8.3 Operational Measurements:
8.3.1 Units and Formats—See Annex A8.
8.3.2 Instrumentation Calibration:
8.3.2.1 Fuel Consumption Rate Measurement—Calibrate the fuel consumption rate measurement system before each reference oil
test sequence and within six months after completion of the last successful calibration test. Temperature-compensate volumetric
systems, and calibrate them against a standard mass flow device. The flowmeter on the test stand shall agree within 0.2 % of the
calibration standard, that standard itself being calibrated against a national standard.
8.3.2.2 Temperature Measurement Calibration—Calibrate the temperature measurement systems before each reference oil test
sequence and within six months after completion of the last successful calibration test. Each temperature measurement system shall
agree within 60.5 °C of the laboratory calibration standard, that standard itself being calibrated against a national standard.
8.3.2.3 Pressure Measurement Calibration—Calibrate the pressure measurement systems before each reference oil test sequence
and within six months after completion of the last successful calibration test. Confirm the calibration standard against a national
standard.
The sole source of supply of the apparatus known to the committee at this time is ExxonMobil Corporation, 3225 Gallows Road, Fairfax, VA 22037,
www.exxonmobil.com. If you are aware of alternative suppliers, please provide this information to ASTM International Headquarters. Your comments will receive careful
consideration at a meeting of the responsible technical committee, which you may attend.
D7549 − 23
8.3.3 Temperature Measurement Locations:
8.3.3.1 General—See Table A14.1. The measurement equipment is not specified. Install the sensors such that the tip is located
midstream of the flow unless otherwise indicated. The accuracy and measurement of the temperature measurement sensors and the
complete measurement system shall follow the guidelines in ASTM Research Report RR:D02-1218.
8.3.3.2 Coolant Out Temperature—Install the sensor in the fitting on the thermostat housing (Fig. A4.12).
8.3.3.3 Coolant In Temperature—Install the sensor on the right side of the coolant pump intake housing at the 1-in. NPT port (Fig.
A4.13).
8.3.3.4 Fuel In Temperature—Install the sensor in the fuel pump inlet fitting (Fig. A4.15).
8.3.3.5 Oil Gallery Temperature—Install the sensor at the ⁄4 in. NPT female boss on the right rear of the engine (Fig. A4.14).
8.3.3.6 Intake Air Temperature—Install the sensor in the inlet air tube 127 mm upstream of the compressor connection (Fig. A4.6).
8.3.3.7 Intake Manifold Temperature—Install the sensor at the ⁄8 in. NPT female boss on the outside radius of the inlet manifold
elbow (Fig. A4.16).
8.3.3.8 Exhaust Temperature—Install the sensor in the exhaust tube (Fig. A4.7).
8.3.3.9 Additional Temperatures—It is permissible to measure any additional temperatures that may be useful for test operation
or engine diagnostics.
NOTE 2—Additional exhaust sensor locations, at the exhaust ports and pre-turbine (front and rear), are recommended. The detection of changes in exhaust
temperatures is an important diagnostic feature.
8.3.4 Pressure Measurement Locations:
8.3.4.1 General—The measurement equipment is not specified. Follow the guidelines in ASTM Research Report RR:D02-1218
for the accuracy and resolution of the pressure measurement sensors and the complete measurement system. If the laboratory has
problems with condensation forming in the pressure lines, install a condensation trap at the lowest elevation of the tubing between
the pressure measurement location and the final pressure sensor for crankcase pressure, intake air pressure, and exhaust pressure.
Route the tubing to avoid intermediate loops or low spots before and after the condensation trap.
8.3.4.2 Oil Gallery Pressure—Measure the pressure at the ⁄4 in. NPT fitting on the right rear of the engine (Fig. A4.14).
8.3.4.3 Oil Filter Inlet Pressure—Measure the pressure at the plug located on the inlet side of the oil filter assembly (Fig. A4.8).
8.3.4.4 Inlet Manifold Pressure—Measure the pressure at the ⁄4 in. NPT port on the outside radius of the inlet manifold elbow (Fig.
A4.16).
8.3.4.5 Crankcase Pressure—Measure the pressure by installing a bulkhead fitting in the valve cover, top-front (Fig. A4.11).
8.3.4.6 Intake Air Pressure—Measure the pressure at a wall tap on the intake air tube 153 mm upstream of the compressor
connection (Fig. A4.6).
8.3.4.7 Exhaust Pressure—Measure the pressure on the exhaust tube (Fig. A4.7).
8.3.4.8 Fuel Pressure—Measure the pressure at the fuel filter head (Fig. A4.25).
8.3.4.9 Coolant Pressure—Measure the pressure on top of the expansion tank (Fig. X1.3).
Supporting data have been filed at ASTM International Headquarters and may be obtained by requesting Research Report RR:D02-1218. Contact ASTM Customer
Service at service@astm.org.
D7549 − 23
8.3.4.10 Intercooler Delta Pressure—Measure the pressure drop across the intercooler. Measure the intercooler inlet pressure at
the elbow outlet of the CAT charge air cooler (Fig. A4.19). Use the intake manifold pressure (8.3.4.4) as the intercooler outlet
pressure. The intercooler delta pressure is the difference between the intercooler outlet pressure and the intercooler inlet pressure.
8.3.4.11 Additional Pressures—It is permissible to measure any additional pressures that may be useful for test operation or engine
diagnostics.
NOTE 3—See Fig. A4.19 and Fig. A4.20 for additional instrument placement information.
8.3.5 Flow Rate Measurement Locations:
8.3.5.1 General—The equipment for the blowby rate and fuel rate measurements is not specified. Follow the guidelines in ASTM
Research Report RR:D02-1218 for the accuracy and resolution of the flow rate measurement system.
8.3.5.2 Blowby—The device used to measure the blowby flow rate is not specified. See 6.2.10 for blowby measurement system
configuration details.
8.3.5.3 Fuel Flow—Determine the fuel consumption rate by measuring the fuel flowing to the day tank (Fig. X1.2).
8.3.5.4 Coolant Flow—Coolant flow rate measurement is not a test requirement, but may be useful for diagnostic purposes. The
design and use of a coolant flow measuring system is optional.
8.3.6 Humidity Measurement—Measure intake air humidity anywhere in the air intake system between air conditioning and the
turbo inlet.
9. Engine/Stand Calibration and Non-Reference Oil Tests
9.1 General—Calibrate the test stand by conducting a test with a blind reference oil. Submit the results to the TMC for
determination of acceptance according to the Lubricant Test Monitoring System (LTMS).
9.2 New Laboratories and New Test Stands:
9.2.1 New Laboratory—A new laboratory is any laboratory that has never previously calibrated a test stand by this test method.
9.2.2 New Test Stand—A new test stand is a test cell and support hardware that has never previously been calibrated by this test
method. Perform a calibration (9.2.3) to introduce a new test stand.
9.2.3 New Test Stand Calibration—Calibrate a new test stand in accordance with the LTMS.
9.3 Stand Calibration Period—The calibration period is 12 operationally valid (Annex A11) non-reference oil tests or 12 months,
whichever comes first, from the EOT date of the last acceptable reference oil test.
9.4 Stand Modification and Calibration Status—Stand calibration status will be invalidated by conducting any non-standard test
or modification of the test and control systems, or both. A non-standard test is any test conducted under a modified procedure,
non-procedural hardware, controller set-point modifications, or any combination thereof. If changes are contemplated, contact the
TMC beforehand to ascertain the effect on the calibration status.
9.5 Test Numbering System:
9.5.1 General—The test number has two parts, X and Y. X represents the test stand number and Y represents the sequential test
stand run number. For example 27-15 indicates test stand number 27 and test stand run number 15. The test stand run number, Y
will increase sequentially by one for each test start (reference oil or non-reference oil). A letter suffix may also be necessary (see
9.5.2).
9.5.2 Reference Oil Tests—A reference oil test conducted subsequent to an unacceptable reference oil test shall include a letter
suffix after Y. The letter suffix shall begin with A and incremented alphabetically until acceptable reference oil test is completed.
D7549 − 23
For example, if two consecutive unacceptable reference oil tests were conducted and the first number was 27-15, the second test
number would be 27-16A. A third calibration attempt would have the test number 27-17B. If the third test were acceptable, then
27-17B would identify the reference oil test in the test report.
9.5.3 Non-Reference Oil Tests—Add no letter suffix to Y for aborted or operationally invalid non-reference oil tests.
9.6 Reference Oil Test Acceptance—Determine reference oil test acceptance in accordance with the LTMS.
9.7 Reference Oil Accountability:
9.7.1 Keep full accounts of the identification and quantities of all reference oils used. With the exception of the oil analyses
required in 11.3, perform no chemical or physical analyses on reference oils without written permission from the TMC. In such
an event, include the written confirmation and the analytical results generated in the reference oil test report.
9.7.2 Retain used reference oil samples for 90 days from the EOT date.
9.8 Non-Reference Oil Tests: Last Start Date—When running a non-reference oil test during the calibration period; crank the
engine prior to the expiration of the calibration period (9.3).
9.9 Donated Reference Oil Test Programs—The surveillance panel is charged with maintaining effective reference oil test severity
and precision monitoring. During times of new parts introductions, new or re-blended reference oil additions, and procedural
revisions, it may be necessary to evaluate the possible effects on severity and precision levels. The surveillance panel may choose
to conduct a program of donated reference oil tests in those laboratories participating in the monitoring system to quantify the effect
of a particular change on severity and precision. Typically the surveillance panel requests its panel members to volunteer enough
reference oil test results to create a robust data set. Broad laboratory participation is needed to provide a representative sampling
of the industry. To ensure the quality of the data obtained, donated tests are conducted on calibrated test stands. The surveillance
panel shall arrange an appropriate number of donated tests and ensure completion of the test program in a timely manner.
9.10 Adjustment to Reference Oil Calibration Periods:
9.10.1 Procedural Deviations—On occasions when a laboratory becomes aware of a significant deviation from the test method,
such as might arise during an in-house review or a TMC inspection, the laboratory and the TMC shall agree on an appropriate
course of action to remedy the deviation. This action may include the shortening of existing reference oil calibration periods.
9.10.2 Parts and Fuel Shortages—Under special circumstances, such as industry-wide parts or fuel shortages, the surveillance
panel may direct the TMC to extend the time intervals between reference oil tests. These extensions shall not exceed one regular
calibration period.
9.10.3 Reference Oil Test Data Flow—To ensure continuous severity and precision monitoring, calibration tests are conducted
periodically throughout the year. There may be occasions when laboratories conduct a large portion of calibration tests in a short
period of time. This could result in an unacceptably large time frame when very few calibration tests are conducted. The TMC can
shorten or extend calibration periods as needed to provide a consistent flow of reference oil test data. Adjustments to calibration
periods are made such that laboratories incur no net loss (or gain) in calibration status.
9.10.4 Special Use of the Reference Oil Calibration System—The surveillance panel has the option to use the reference oil system
to evaluate changes that have potential impact on test severity and precision. This option is only taken when a program of donated
tests is not feasible. The surveillance panel and the TMC shall develop a detailed plan for the test program. This plan requires all
reference oil tests in the program to be completed as close to the same time as possible, so that no laboratory or stand calibration
is left in an excessively long pending status. In order to obtain the integrity of the reference oil monitoring system each reference
oil test is conducted so as to be interpretable for stand calibration. To facilitate the required test scheduling, the surveillance panel
may direct the TMC to lengthen and shorten reference oil calibration periods within laboratories such that the laboratories incur
no net loss (or gain) in calibration status.
9.11 Calibration of Piston and Ring Deposit Raters—Each calendar year, each laboratory shall send at least one Heavy Duty
Diesel Rater to the ASTM Standardized Testing Deposit Rating Workshop. Each rater shall rate a minimum of six diesel pistons
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