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ASTM D6514-03

(Test Method)

Standard Test Method for High Temperature Universal Oxidation Test for Turbine Oils

Standard Test Method for High Temperature Universal Oxidation Test for Turbine Oils

SIGNIFICANCE AND USE
Degradation of fluid lubricants because of oxidation or thermal breakdown can result in fluid thickening or in the formation of acids or insoluble solids and render the fluid unfit for further use as a lubricant.
This test method can be used for estimating the oxidation stability of oils. It can function as a formulation screening tool, specification requirement, quality control measurement, or as a means of estimating remaining service life. It shall be recognized, however, that correlation between results of this test method and the oxidation stability of an oil in field service can vary markedly with field service conditions and with various oils.
This test method is designed to compliment Test Method D 5846 and is intended for evaluation of fluids which do not degrade significantly within a reasonable period of time at 135°C.
SCOPE
1.1 This test method covers a procedure for evaluating the oxidation of inhibited lubricants in the presence of air, copper, and iron metals.
1.2 This test method was developed and is used to evaluate the high temperature oxidation stability and deposit forming tendency of oils for steam and gas turbines. It has been used for testing other lubricants made with mineral oil and synthetic basestocks for compressors, hydraulic pumps, and other applications, but these have not been used in cooperative testing.
1.3 The values stated in SI units are to be regarded as the standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Identified hazardous chemicals are listed in Section 7. Before using this test method, refer to suppliers' safety labels, Material Safety Data Sheets and other technical literature.

General Information

Status
Historical
Publication Date
09-May-2003
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.09.0C - Oxidation of Turbine Oils
Current Stage
Ref Project

Relations

Replaces
ASTM D6514-02 - Standard Test Method for High Temperature Universal Oxidation Test for Turbine Oils
Effective Date
10-May-2003
Replaced By
ASTM D6514-03(2008) - Standard Test Method for High Temperature Universal Oxidation Test for Turbine Oils
Effective Date
01-Dec-2008
Referred By
ASTM D7155-20 - Standard Practice for Evaluating Compatibility of Mixtures of Turbine Lubricating Oils
Effective Date
10-May-2003
Referred By
ASTM D4871-11(2022) - Standard Guide for Universal Oxidation/Thermal Stability Test Apparatus
Effective Date
10-May-2003

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ASTM D6514-03 - Standard Test Method for High Temperature Universal Oxidation Test for Turbine OilsASTM D6514-03 - Standard Test Method for High Temperature Universal Oxidation Test for Turbine Oils
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ASTM D6514-03 - Standard Test Method for High Temperature Universal Oxidation Test for Turbine Oils
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
An American National Standard
Designation: D 6514 – 03
Standard Test Method for
1
High Temperature Universal Oxidation Test for Turbine Oils
This standard is issued under the fixed designation D 6514; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D 974 Test Method for Acid and Base Number by Color-
Indicator Titration
1.1 This test method covers a procedure for evaluating the
D 3339 Test Method for Acid Number of Petroleum Prod-
oxidation of inhibited lubricants in the presence of air, copper,
ucts by Semi-Micro Color Indicator Titration
and iron metals.
D 4057 Practice for Manual Sampling of Petroleum and
1.2 This test method was developed and is used to evaluate
Petroleum Products
the high temperature oxidation stability and deposit forming
D 4871 Guide for Universal Oxidation/Thermal Stability
tendencyofoilsforsteamandgasturbines.Ithasbeenusedfor
Test Apparatus
testing other lubricants made with mineral oil and synthetic
D 5846 Test Method for Universal Oxidation Test for Hy-
basestocks for compressors, hydraulic pumps, and other appli-
draulic and Turbine Oils Using the Universal Oxidation
cations, but these have not been used in cooperative testing.
Test Apparatus
1.3 The values stated in SI units are to be regarded as the
3
2.2 British Standards:
standard.
BS 1829 Specification for Carbon Steel, alternate to Speci-
1.4 This standard does not purport to address all of the
fication A 510
safety concerns, if any, associated with its use. It is the
4
2.3 Institute of Petroleum Standard:
responsibility of the user of this standard to establish appro-
IP 2546 Practice for Sampling of Petroleum Products;
priate safety and health practices and determine the applica-
Alternate to Practice D 4057
bility of regulatory limitations prior to use. Identified hazard-
5
2.4 ASTM Adjunct
ous chemicals are listed in Section 7. Before using this test
5
ADJD6514 Oxidation Cell Varnish Standard
method, refer to suppliers’ safety labels, Material Safety Data
Sheets and other technical literature.
3. Terminology
2. Referenced Documents 3.1 Definitions of Terms Specific to This Standard:
2
3.1.1 Universal Oxidation Test—the apparatus and proce-
2.1 ASTM Standards:
dures described in Guide D 4871.
A 510 Specification for General Requirements for Wire
Rods and Coarse Round Wire, Carbon Steel
4. Summary of Test Method
B1 Specification for Hard-Drawn Copper Wire
4.1 Afterdeterminingtheviscosityat40°Candacidnumber
D 445 Test Method for Kinematic Viscosity of Transparent
of a sample, a test specimen is stressed at 155°Cfor96h.After
and Opaque Liquids (and the Calculation of Dynamic
cooling, the test specimen is vacuum filtered for the determi-
Viscosity)
nation of the total insolubles formed during the test. Total
D 664 TestMethodforAcidNumberofPetroleumProducts
insolubles are reported as low, medium, or high.
by Potentiometric Titration
4.2 The viscosity and the acid number of the filtrate are
D 943 Test Method for Oxidation Characteristics of Inhib-
determined and compared with the initial values to ascertain
ited Mineral Oils
any increase in those values. Both the change in acid number
and the increase in viscosity at 40°C are reported.
1
This test method is under the jurisdiction of ASTM Committee D02 on
Petroleum Products and Lubricants and is the direct responsibility of D02.09.0C on
3
Oxidation of Turbine Oils. Available from British Standards Institute (BSI), 389 Chiswick High Rd.,
Current edition approved May 10, 2003. Published July 2003. Originally London W4 4AL, U.K.
4
approved in 2000. Last previous edition approved in 2002 as D 6514–02. Available from Institute of Petroleum (IP), 61 New Cavendish St., London,
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or WIG 7AR, U.K.
5
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Available from ASTM International Headquarters. Order Adjunct No.
Standards volume information, refer to the standard’s Document Summary page on ADJD6514. Names of suppliers in the United Kingdom can be obtained from the
the ASTM website. Institute of Petroleum. Two master standards are held by the IP for reference.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D6514–03
4.3 The glass cell in which the test specimen was stressed is 5.3 ThistestmethodisdesignedtocomplimentTestMethod
rinsed with heptane and dried. Residual deposits are compared D 5846 and is intended for evaluation of fluids which do not
with ASTM A
...

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