Standard Test Method for Bulk Specific Gravity and Density of Non-Absorptive Compacted Asphalt Mixtures

SIGNIFICANCE AND USE
5.1 The results obtained from this test method can be used to determine the unit weight of compacted dense asphalt mixtures and in conjunction with Test Method D3203/D3203M, to obtain percent air voids. These values in turn may be used in determining the relative degree of compaction.  
5.2 Since specific gravity has no units, it must be converted to density in order to do calculations that require units. This conversion is made by multiplying the specific gravity at a given temperature by the density of water at the same temperature.
Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers the determination of bulk specific gravity and density of specimens of compacted asphalt mixtures.  
1.2 This test method should not be used with samples that contain open or interconnecting voids or absorb more than 2.0 % of water by volume, or both, as determined in 11.3.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
30-Apr-2021

Relations

Effective Date
01-Feb-2024
Effective Date
01-Nov-2023
Effective Date
01-Nov-2019
Effective Date
15-Aug-2018
Effective Date
01-Jun-2017
Effective Date
01-Oct-2016
Effective Date
01-May-2015
Effective Date
01-May-2014
Effective Date
07-Mar-2014
Effective Date
01-Dec-2013
Effective Date
01-May-2013
Effective Date
01-Feb-2012
Effective Date
01-Dec-2011
Effective Date
01-Dec-2011
Effective Date
15-Jun-2011

Overview

ASTM D2726/D2726M-21 is the internationally recognized standard test method for determining the bulk specific gravity and density of non-absorptive compacted asphalt mixtures. Developed by ASTM Committee D04 on Road and Paving Materials, this standard is fundamental for evaluating the physical properties of dense asphalt pavements and mixtures. By establishing standardized procedures, the method supports quality assurance and performance assessments in paving projects and laboratory research worldwide.

This test method is specifically designed for asphalt specimens that do not contain open or interconnected voids and do not absorb more than 2.0% water by volume. It can be applied to both laboratory-molded and field-extracted pavement samples, provided they meet these criteria, making it valuable for a wide range of construction and research applications in the asphalt industry.

Key Topics

  • Bulk Specific Gravity (Gmb): The ratio of the mass of a compacted asphalt sample to the mass of an equal volume of water at 25°C. This is a dimensionless value used as a parameter for further calculations.
  • Density Determination: Density is calculated by multiplying the measured specific gravity of the asphalt specimen by the density of water at test temperature, giving results in kg/m³ or lb/ft³.
  • Quality of Compaction: The results guide the determination of unit weight and the relative degree of compaction, essential for ensuring pavement durability and longevity.
  • Sample Suitability: Samples must be free from foreign materials and meet water absorption criteria (<2.0% by volume).
  • Test Precision: The method addresses both single-operator and multilaboratory precision, which is crucial to ensure consistent and reliable measurements.
  • Application of SI and Inch-Pound Units: Both measurement systems are permitted, but mixing units is not allowed to maintain standardization.

Applications

  • Pavement Construction Quality Control: Determining the density and specific gravity of compacted asphalt pavements, ensuring compliance with project specifications.
  • Research and Laboratory Testing: Supporting mix design, evaluation of material behavior, and comparison of asphalt mixtures.
  • Degree of Compaction Measurement: When used in conjunction with related standards (e.g., ASTM D3203/D3203M for air voids), it helps assess compaction efficiency of asphalt concrete, directly impacting pavement lifespan.
  • Performance Evaluation: Provides key metrics that enable engineers to monitor the long-term behavior of pavements under actual service conditions.
  • Regulatory Compliance: Used by governmental agencies, contractors, and consulting engineers to verify acceptance properties of asphalt paving materials.

Related Standards

  • ASTM D3203/D3203M: Test Method for Percent Air Voids in Compacted Asphalt Mixtures
  • ASTM D1188: Test Method for Bulk Specific Gravity and Density of Compacted Bituminous Mixtures Using Coated Samples
  • ASTM D3666: Specification for Minimum Requirements for Agencies Testing and Inspecting Road and Paving Materials
  • ASTM D975/D979M: Practice for Sampling Bituminous Paving Mixtures
  • ASTM D5361/D5361M: Practice for Sampling Compacted Asphalt Mixtures for Laboratory Testing
  • ASTM D6752/D6752M: Test Method for Bulk Specific Gravity and Density Using Automatic Vacuum Sealing
  • ASTM D7227/D7227M: Practice for Rapid Drying of Compacted Asphalt Mixtures
  • ASTM Standards for Thermometers and Equipment: E1, E77, E563, E644, E1137/E1137M, and E2251

Keywords: bulk specific gravity, density, asphalt mixtures, compacted asphalt, ASTM D2726, unit weight, compaction, air voids, pavement quality, density test.

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Frequently Asked Questions

ASTM D2726/D2726M-21 is a standard published by ASTM International. Its full title is "Standard Test Method for Bulk Specific Gravity and Density of Non-Absorptive Compacted Asphalt Mixtures". This standard covers: SIGNIFICANCE AND USE 5.1 The results obtained from this test method can be used to determine the unit weight of compacted dense asphalt mixtures and in conjunction with Test Method D3203/D3203M, to obtain percent air voids. These values in turn may be used in determining the relative degree of compaction. 5.2 Since specific gravity has no units, it must be converted to density in order to do calculations that require units. This conversion is made by multiplying the specific gravity at a given temperature by the density of water at the same temperature. Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors. SCOPE 1.1 This test method covers the determination of bulk specific gravity and density of specimens of compacted asphalt mixtures. 1.2 This test method should not be used with samples that contain open or interconnecting voids or absorb more than 2.0 % of water by volume, or both, as determined in 11.3. 1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE 5.1 The results obtained from this test method can be used to determine the unit weight of compacted dense asphalt mixtures and in conjunction with Test Method D3203/D3203M, to obtain percent air voids. These values in turn may be used in determining the relative degree of compaction. 5.2 Since specific gravity has no units, it must be converted to density in order to do calculations that require units. This conversion is made by multiplying the specific gravity at a given temperature by the density of water at the same temperature. Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors. SCOPE 1.1 This test method covers the determination of bulk specific gravity and density of specimens of compacted asphalt mixtures. 1.2 This test method should not be used with samples that contain open or interconnecting voids or absorb more than 2.0 % of water by volume, or both, as determined in 11.3. 1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D2726/D2726M-21 is classified under the following ICS (International Classification for Standards) categories: 91.100.50 - Binders. Sealing materials; 93.080.20 - Road construction materials. The ICS classification helps identify the subject area and facilitates finding related standards.

ASTM D2726/D2726M-21 has the following relationships with other standards: It is inter standard links to ASTM D4753-24, ASTM D6752/D6752M-23, ASTM E644-11(2019), ASTM D6752/D6752M-18, ASTM D6752/D6752M-17, ASTM D3666-16, ASTM D4753-15, ASTM E77-14, ASTM D5361/D5361M-14, ASTM D3666-13, ASTM E1-13, ASTM D979/D979M-12, ASTM D3203/D3203M-11, ASTM D3666-11, ASTM D979/D979M-11. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

ASTM D2726/D2726M-21 is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.

Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation:D2726/D2726M −21
Standard Test Method for
Bulk Specific Gravity and Density of Non-Absorptive
Compacted Asphalt Mixtures
This standard is issued under the fixed designation D2726/D2726M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope* Compacted Bituminous Mixtures Using Coated Samples
D3203/D3203M Test Method for PercentAir Voids in Com-
1.1 This test method covers the determination of bulk
pacted Asphalt Mixtures
specific gravity and density of specimens of compacted asphalt
D3666 Specification for Minimum Requirements for Agen-
mixtures.
cies Testing and Inspecting Road and Paving Materials
1.2 This test method should not be used with samples that
D4753 Guide for Evaluating, Selecting, and Specifying Bal-
contain open or interconnecting voids or absorb more than
ances and Standard Masses for Use in Soil, Rock, and
2.0 % of water by volume, or both, as determined in 11.3.
Construction Materials Testing
1.3 The values stated in either SI units or inch-pound units D5361/D5361M Practice for Sampling Compacted Asphalt
Mixtures for Laboratory Testing
are to be regarded separately as standard. The values stated in
each system are not necessarily exact equivalents; therefore, to D6752/D6752M Test Method for Bulk Specific Gravity and
Density of CompactedAsphalt Mixtures UsingAutomatic
ensure conformance with the standard, each system shall be
used independently of the other, and values from the two Vacuum Sealing Method
D7227/D7227M Practice for Rapid Drying of Compacted
systems shall not be combined.
Asphalt Mixture Specimens Using Vacuum DryingAppa-
1.4 This standard does not purport to address all of the
ratus
safety concerns, if any, associated with its use. It is the
E1 Specification for ASTM Liquid-in-Glass Thermometers
responsibility of the user of this standard to establish appro-
E77 Test Method for Inspection and Verification of Ther-
priate safety, health, and environmental practices and deter-
mometers
mine the applicability of regulatory limitations prior to use.
E563 Practice for Preparation and Use of an Ice-Point Bath
1.5 This international standard was developed in accor-
as a Reference Temperature
dance with internationally recognized principles on standard-
E644 Test Methods for Testing Industrial Resistance Ther-
ization established in the Decision on Principles for the
mometers
Development of International Standards, Guides and Recom-
E1137/E1137M Specification for Industrial Platinum Resis-
mendations issued by the World Trade Organization Technical
tance Thermometers
Barriers to Trade (TBT) Committee.
E2251 Specification for Liquid-in-Glass ASTM Thermom-
eters with Low-Hazard Precision Liquids
2. Referenced Documents
2.1 ASTM Standards:
3. Terminology
D979/D979M Practice for Sampling Bituminous Paving
3.1 Definitions of Terms Specific to This Standard:
Mixtures
3.1.1 bulk density—as determined by this test method, the
D1188 TestMethodforBulkSpecificGravityandDensityof
mass of a metre cubed (or foot cubed) of the material at 25 °C
[77 °F].
3.1.2 bulk specific gravity—as determined by this test
This test method is under the jurisdiction of ASTM Committee D04 on Road
and Paving Materials and is the direct responsibility of Subcommittee D04.21 on
method, the ratio of the mass of a given volume of material at
Specific Gravity and Density of Asphalt Mixtures.
25 °C [77 °F] to the mass of an equal volume of water at the
Current edition approved May 1, 2021. Published May 2021. Originally
same temperature.
approved in 1968. Last previous edition approved in 2019 as D2726/D2726M – 19.
DOI: 10.1520/D2726_D2726M-21.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 4. Summary of Test Method
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
4.1 The specimen is immersed in a water bath at 25 °C
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. [77 °F].The mass under water is recorded, and the specimen is
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D2726/D2726M−21
takenoutofthewater,blottedquicklywithadampclothtowel, 6.3 Drying Oven, capable of maintaining a temperature of
and weighed in air. The difference between the two masses is 110 6 5 °C [230 6 9 °F].
used to measure the mass of an equal volume of water at 25 °C
6.4 Thermometer—The thermometer shall be one of the
[77 °F].
following:
4.2 This test method provides guidance for determination of
6.4.1 A liquid-in-glass partial or total immersion thermom-
the oven-dry or thoroughly dry mass of the specimen.The bulk
eter of suitable range with subdivisions and maximum scale
specific gravity is calculated from these masses. Then the
error of 0.5 °C [1.0 °F] which conforms to the requirements of
density is obtained by multiplying the specific gravity of the
SpecificationE1.Calibratethethermometerinaccordancewith
specimen by the density of the water.
one of the methods in Test Method E77 or verify its original
calibration at the ice point (Notes 4 and 5).
5. Significance and Use
NOTE4—PracticeE563providesinstructionsonthepreparationanduse
5.1 The results obtained from this test method can be used
of an ice-point bath as a reference temperature.
to determine the unit weight of compacted dense asphalt
NOTE5—Ifthethermometerdoesnotread0.0 60.5 °C[32.0 61.0 °F]
mixtures and in conjunction with Test Method D3203/
at the ice point, then the thermometer should be recalibrated.
D3203M, to obtain percent air voids. These values in turn may
6.4.2 A liquid-in-glass partial or total immersion thermom-
be used in determining the relative degree of compaction.
eter of suitable range with subdivisions and maximum scale
5.2 Since specific gravity has no units, it must be converted
error of 0.5 °C [1.0 °F] which conforms to the requirements of
to density in order to do calculations that require units. This
Specification E2251. Calibrate the thermometer in accordance
conversion is made by multiplying the specific gravity at a
with one the methods in Test Method E77 or verify its original
given temperature by the density of water at the same tempera-
calibration at the ice point (Notes 4 and 5).
ture.
6.4.3 Aplatinumresistancethermometer(PRT)withaprobe
NOTE 1—The quality of the results produced by this standard are
which conforms to the requirements of Specification E1137/
dependent on the competence of the personnel performing the procedure
E1137M. The PRT shall have a three- or four-wire connection
and the capability, calibration, and maintenance of the equipment used.
configuration and the overall sheath length shall be at least
Agencies that meet the criteria of Specification D3666 are generally
50 mm [2 in.] greater than the immersion depth. Calibrate the
considered capable of competent and objective testing, sampling,
inspection, etc. Users of this standard are cautioned that compliance with
PRT system (probe and readout) in accordance with Test
Specification D3666 alone does not completely ensure reliable results.
Methods E644 or verify its original calibration at the ice point
Reliable results depend on many factors; following the suggestions of
(Notes4and5).Correctionsshallbeappliedtoensureaccurate
Specification D3666 or some similar acceptable guideline provides a
measurements within 0.5 °C [1.0 °F].
means of evaluating and controlling some of those factors.
6.4.4 A metal-sheathed thermistor with a sensor substan-
6. Apparatus
tially similar in construction to the PRT probe described in
6.1 Balance, with ample capacity, and with sufficient sensi- 6.4.3. Calibrate the thermistor system (sensor and readout) in
tivity to enable bulk specific gravities of the specimens to be
accordance with Test Methods E644 or verify its original
calculated to at least four significant figures, that is, to at least calibrationattheicepoint(Notes4and5).Correctionsshallbe
three decimal places. It shall be equipped with a suitable
applied to ensure accurate measurements within 0.5 °C
apparatus to permit weighing the specimen while suspended in [1.0 °F].
water. To avoid erroneous readings by undue displacement of
water, use wire or fish line of the smallest practical size to 7. Standardization
suspend the specimen and holder. Do not use chains, strings, or
7.1 Balance—Standardize at least once each twelve months.
sash cords. The balance shall conform to Guide D4753 as a
Class GP2 balance.
7.2 Temperature-Measuring Devices—Standardize at least
once every twelve months.
NOTE 2—Since there are no more significant figures in the quotient
(bulk specific gravity) than appear in either the dividend (the mass of the
7.3 Drying Oven—Standardize thermometric devices at
specimen in air) or in the divisor (the mass of the volume of water equal
least once every twelve months.
to the volume of the specimen, obtained from the difference in weight of
the saturated surface-dry specimen in air and in water), this means that the
NOTE 6—The terms of standardization, verification, calibration, and
balance must have a sensitivity
...


This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D2726/D2726M − 19 D2726/D2726M − 21
Standard Test Method for
Bulk Specific Gravity and Density of Non-Absorptive
Compacted Asphalt Mixtures
This standard is issued under the fixed designation D2726/D2726M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope*
1.1 This test method covers the determination of bulk specific gravity and density of specimens of compacted asphalt mixtures.
1.2 This test method should not be used with samples that contain open or interconnecting voids or absorb more than 2.0 % of
water by volume, or both, as determined in 11.3.
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each
system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used
independently of the other, and values from the two systems shall not be combined.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of
regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2.1 ASTM Standards:
D979/D979M Practice for Sampling Bituminous Paving Mixtures
D1188 Test Method for Bulk Specific Gravity and Density of Compacted Bituminous Mixtures Using Coated Samples
D3203/D3203M Test Method for Percent Air Voids in Compacted Asphalt Mixtures
D3666 Specification for Minimum Requirements for Agencies Testing and Inspecting Road and Paving Materials
D4753 Guide for Evaluating, Selecting, and Specifying Balances and Standard Masses for Use in Soil, Rock, and Construction
Materials Testing
D5361/D5361M Practice for Sampling Compacted Asphalt Mixtures for Laboratory Testing
D6752/D6752M Test Method for Bulk Specific Gravity and Density of Compacted Asphalt Mixtures Using Automatic Vacuum
Sealing Method
D7227/D7227M Practice for Rapid Drying of Compacted Asphalt Mixture Specimens Using Vacuum Drying Apparatus
This test method is under the jurisdiction of ASTM Committee D04 on Road and Paving Materials and is the direct responsibility of Subcommittee D04.21 on Specific
Gravity and Density of Asphalt Mixtures.
Current edition approved March 1, 2019May 1, 2021. Published March 2019May 2021. Originally approved in 1968. Last previous edition approved in 20172019 as
D2726/D2726M – 17.D2726/D2726M – 19. DOI: 10.1520/D2726_D2726M-19.10.1520/D2726_D2726M-21.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D2726/D2726M − 21
E1 Specification for ASTM Liquid-in-Glass Thermometers
E77 Test Method for Inspection and Verification of Thermometers
E563 Practice for Preparation and Use of an Ice-Point Bath as a Reference Temperature
E644 Test Methods for Testing Industrial Resistance Thermometers
E1137/E1137M Specification for Industrial Platinum Resistance Thermometers
E2251 Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
3. Terminology
3.1 Definitions of Terms Specific to This Standard:
3.1.1 bulk density—as determined by this test method, the mass of a metre cubed (or foot cubed) of the material at 25 °C [77 °F].
3.1.2 bulk specific gravity—as determined by this test method, the ratio of the mass of a given volume of material at 25 °C [77 °F]
to the mass of an equal volume of water at the same temperature.
4. Summary of Test Method
4.1 The specimen is immersed in a water bath at 25 °C [77 °F]. The mass under water is recorded, and the specimen is taken out
of the water, blotted quickly with a damp cloth towel, and weighed in air. The difference between the two masses is used to measure
the mass of an equal volume of water at 25 °C [77 °F].
4.2 This test method provides guidance for determination of the oven dry oven-dry or thoroughly dry mass of the specimen. The
bulk specific gravity is calculated from these masses. Then the density is obtained by multiplying the specific gravity of the
specimen by the density of the water.
5. Significance and Use
5.1 The results obtained from this test method can be used to determine the unit weight of compacted dense asphalt mixtures and
in conjunction with Test Method D3203/D3203M, to obtain percent air voids. These values in turn may be used in determining
the relative degree of compaction.
5.2 Since specific gravity has no units, it must be converted to density in order to do calculations that require units. This conversion
is made by multiplying the specific gravity at a given temperature by the density of water at the same temperature.
NOTE 1—The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the
capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable
of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does
not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar
acceptable guideline provides a means of evaluating and controlling some of those factors.
6. Apparatus
6.1 Balance, with ample capacity, and with sufficient sensitivity to enable bulk specific gravities of the specimens to be calculated
to at least four significant figures, that is, to at least three decimal places. It shall be equipped with a suitable apparatus to permit
weighing the specimen while suspended in water. To avoid erroneous readings by undue displacement of water, use wire or fish
line of the smallest practical size to suspend the specimen and holder. Do not use chains, strings, or sash cords. The balance shall
conform to Guide D4753 as a Class GP2 balance.
NOTE 2—Since there are no more significant figures in the quotient (bulk specific gravity) than appear in either the dividend (the mass of the specimen
in air) or in the divisor (the mass of the volume of water equal to the volume of the specimen, obtained from the difference in weight of the saturated
surface-dry specimen in air and in water), this means that the balance must have a sensitivity capable of providing both mass values to at least four figures.
For example, a sensitivity of 0.1 g [0.0002 lb] would provide four significant figures for mass in the range from 100.1 to 999.9 g [0.221 to 2.204 lb].
6.2 Water Bath, capable of maintaining a temperature of 25 6 1 °C [77 6 1.8 °F] for immersing the specimen in water while
suspended, equipped with an overflow outlet for maintaining a constant water level. The use of an overflow outlet is mandatory.
NOTE 3—The water bath does not need to be a sophisticated device. Any method that maintains 25 6 1 °C [77 6 1.8 °F] can be used including tempering,
aquarium heaters, stirrers, or other devices.
D2726/D2726M − 21
6.3 Drying Oven, capable of maintaining a temperature of 110 6 5 °C [230 6 9 °F].
6.4 Thermometer—The thermometer shall be one of the following:
6.4.1 A liquid-in-glass partial or total immersion thermometer of suitable range with subdivisions and maximum scale error of
0.5 °C [1.0 °F] which conforms to the requirements of Specification E1. Calibrate the thermometer in accordance with one of the
methods in Test Method E77 or verify its original calibration at the ice point (Notes 4 and 5).
NOTE 4—Practice E563 provides instructions on the preparation and use of an ice-point bath as a reference temperature.
NOTE 5—If the thermometer does not read 0.0 6 0.5 °C [32.0 6 1.0 °F] at the ice point, then the thermometer should be recalibrated.
6.4.2 A liquid-in-glass partial or total immersion thermometer of suitable range with subdivisions and maximum scale error of
0.5 °C [1.0 °F] which conforms to the requirements of Specification E2251. Calibrate the thermometer in accordance with one the
methods in Test Method E77 or verify its original calibration at the ice point (Notes 4 and 5).
6.4.3 A platinum resistance thermometer (PRT) with a probe which conforms to the requirements of Specification E1137/E1137M.
The PRT shall have a three- or four-wire connection configuration and the overall sheath length shall be at least 50 mm [2 in.]
greater than the immersion depth. Calibrate the PRT system (probe and readout) in accordance with Test Methods E644 or verify
its original calibration at the ice point (Notes 4 and 5). Corrections shall be applied to ensure accurate measurements within 0.5 °C
[1.0 °F
...

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