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ASTM C1210-21

(Guide)

Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within Nuclear Industry

Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within Nuclear Industry

SIGNIFICANCE AND USE
4.1 A laboratory quality assurance program is an essential program for laboratories within the nuclear industry. Guide C1009 provides guidance for establishing a quality assurance program for an analytical laboratory within the nuclear industry. This guide deals with the control of measurements aspect of the laboratory quality assurance program. Fig. 1 shows the relationship of measurement control with other essential aspects of a laboratory quality assurance program.
FIG. 1 Quality Assurance of Analytical Laboratory Data  
4.2 The fundamental purposes of a measurement control program are to provide the with-use  assurance (real-time control) that a measurement system is performing satisfactorily and to provide the data necessary to quantify measurement system performance. The with-use  assurance is usually provided through the satisfactory analysis of quality control samples (reference value either known or unknown to the analyst). The data necessary to quantify measurement system performance is usually provided through the analysis of quality control samples or the duplicate analysis of process samples, or both. In addition to the analyses of quality control samples, the laboratory quality control program should address (1) the preparation and verification of standards and reagents, (2) data analysis procedures and documentation, (3) calibration and calibration procedures, (4) measurement method qualification, (5) analyst qualification, and (6) other general program considerations. Other elements of laboratory quality assurance also impact the laboratory quality control program. These elements or requirements include (1) chemical analysis procedures and procedure control, (2) records storage and retrieval requirements, (3) internal audit requirements, (4) organizational considerations, and (5) training/qualification requirements. To the extent possible, this standard will deal primarily with quality control requirements rather than overall quality assurance re...
SCOPE
1.1 This guide provides guidance for establishing and maintaining a measurement system quality control program. Guidance is provided for general program considerations, preparation of quality control samples, analysis of quality control samples, quality control data analysis, analyst qualification, measurement system calibration, measurement method qualification, and measurement system maintenance.  
1.2 This guidance is provided in the following sections:    
Section  
General Quality Control Program Considerations  
5  
Quality Control Samples  
6  
Analysis of Quality Control Samples  
7  
Quality Control Data Analysis  
8  
Analyst Qualification  
9  
Measurement System Calibration  
10  
Qualification of Measurement Methods and Systems  
11  
Measurement System Maintenance  
12  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Jan-2021
ICS
03.120.10 - Quality management and quality assurance
27.120.01 - Nuclear energy in general
Technical Committee
C26 - Nuclear Fuel Cycle
Drafting Committee
C26.08 - Quality Assurance, Statistical Applications, and Reference Materials
Current Stage
Ref Project

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ASTM C1210-21 - Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within Nuclear IndustryASTM C1210-21 - Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within Nuclear Industry
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REDLINE ASTM C1210-21 - Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within Nuclear IndustryREDLINE ASTM C1210-21 - Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within Nuclear Industry
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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: C1210 − 21
Standard Guide for
Establishing a Measurement System Quality Control
Program for Analytical Chemistry Laboratories Within
1
Nuclear Industry
This standard is issued under the fixed designation C1210; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope C1108 Test Method for Plutonium by Controlled-Potential
Coulometry
1.1 This guide provides guidance for establishing and main-
C1128 Guide for Preparation of Working Reference Materi-
taining a measurement system quality control program. Guid-
als for Use in Analysis of Nuclear Fuel Cycle Materials
ance is provided for general program considerations, prepara-
C1156 Guide for Establishing Calibration for a Measure-
tion of quality control samples, analysis of quality control
ment Method Used to Analyze Nuclear Fuel Cycle Mate-
samples, quality control data analysis, analyst qualification,
rials
measurement system calibration, measurement method
C1297 Guide for Qualification of Laboratory Analysts for
qualification, and measurement system maintenance.
the Analysis of Nuclear Fuel Cycle Materials
1.2 This guidance is provided in the following sections:
E2554 Practice for Estimating and Monitoring the Uncer-
Section
tainty of Test Results of a Test Method Using Control
General Quality Control Program Considerations 5
Chart Techniques
Quality Control Samples 6
3
Analysis of Quality Control Samples 7 2.2 ANSI Standards:
Quality Control DataAnalysis 8
ANSI/ASQ B1 Guide for Quality Control Charts
Analyst Qualification 9
ANSI/ASQ B2 Control Chart Method of Analyzing Data
Measurement System Calibration 10
Qualification of Measurement Methods and Systems 11 ANSI/ASQB3 ControlChartMethodofControllingQuality
Measurement System Maintenance 12
During Production
4
1.3 This international standard was developed in accor-
2.3 ISO Standard:
dance with internationally recognized principles on standard-
ISO/IEC 17025 General requirements for the competence of
ization established in the Decision on Principles for the
testing and calibration laboratories
Development of International Standards, Guides and Recom-
ISO/IEC 17043 Conformity assessment — General require-
mendations issued by the World Trade Organization Technical
ments for proficiency testing
Barriers to Trade (TBT) Committee.
ISO Guide 80 Guidance for the in-house preparation of
quality control materials (QCMs)
2. Referenced Documents
2
2.1 ASTM Standards: 3. Terminology
C859 Terminology Relating to Nuclear Materials
3.1 For definitions of terms used in this guide but not
C1009 Guide for Establishing and Maintaining a Quality
defined herein, see Terminology C859.
Assurance Program forAnalytical LaboratoriesWithin the
3.2 Definitions:
Nuclear Industry
3.2.1 calibration, n—the set of operations that establishes,
C1068 Guide for Qualification of Measurement Methods by
under specified conditions, a metrologically traceable relation-
a Laboratory Within the Nuclear Industry
shipbetweenavaluemeasuredorindicatedbyaninstrumentor
system to a corresponding known value, typically derived from
1
This guide is under the jurisdiction ofASTM Committee C26 on Nuclear Fuel
appropriate reference standards or established physical con-
Cycle and is the direct responsibility of Subcommittee C26.08 on Quality
stants
Assurance, Statistical Applications, and Reference Materials.
Current edition approved Feb. 1, 2021. Published March 2021. Originally
approved in 1991. Last previous edition approved in 2018 as C1210 – 18. DOI:
3
10.1520/C1210-21. Available from American National Standards Institute (ANSI), 25 W. 43rd St.,
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 4th Floor, New York, NY 10036, http://www.ansi.org.
4
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Available from International Organization for Standardization (ISO), ISO
Standards volume information, refer to the standard’s Document Summary page on Central Secretariat, Chemin de Blandonnet 8, CP 401, 1214 Vernier, Geneva,
the ASTM website. Switzerland, https://www.iso.org.
Copyright ©ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1210 − 21
3.2.1.1 Discussion—The calibration relationship can be ex- try. This guide deals with the control of measurements aspect
pressed by a statement, function, diagram or table. of the laboratory qua
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: C1210 − 18 C1210 − 21
Standard Guide for
Establishing a Measurement System Quality Control
Program for Analytical Chemistry Laboratories Within the
1
Nuclear Industry
This standard is issued under the fixed designation C1210; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This standardguide provides guidance for establishing and maintaining a measurement system quality control program.
Guidance is provided for general program considerations, preparation of quality control samples, analysis of quality control
samples, quality control data analysis, analyst qualification, measurement system calibration, measurement method qualification,
and measurement system maintenance.
1.2 This guidance is provided in the following sections:
Section
General Quality Control Program Considerations 5
Quality Control Samples 6
Analysis of Quality Control Samples 7
Quality Control Data Analysis 8
Analyst Qualification 9
Measurement System Calibration 10
Measurement Method Qualification 11
Qualification of Measurement Methods and Systems 11
Measurement System Maintenance 12
1.3 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
C859 Terminology Relating to Nuclear Materials
C1009 Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear
Industry
C1068 Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry
C1108 Test Method for Plutonium by Controlled-Potential Coulometry
C1128 Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials
1
This guide is under the jurisdiction of ASTM Committee C26 on Nuclear Fuel Cycle and is the direct responsibility of Subcommittee C26.08 on Quality Assurance,
Statistical Applications, and Reference Materials.
Current edition approved Nov. 1, 2018Feb. 1, 2021. Published December 2018March 2021. Originally approved in 1991. Last previous edition approved in 20122018 as
C1210 – 12.C1210 – 18. DOI: 10.1520/C1210-18.10.1520/C1210-21.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1210 − 21
C1156 Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials
C1297 Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials
E2554 Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques
3
2.2 ANSI Standards:
ANSI/ASQ B1 Guide for Quality Control Charts
ANSI/ASQ B2 Control Chart Method of Analyzing Data
ANSI/ASQ B3 Control Chart Method of Controlling Quality During Production
4
2.3 ISO Standard:
ISO/IEC 17025 General requirements for the competence of testing and calibration laboratories
ISO/IEC 17043 Conformity assessment — General requirements for proficiency testing
ISO Guide 80 Guidance for the in-house preparation of quality control materials (QCMs)
3. Terminology
3.1 For definitions of terms used in this guide but not defined herein, see Terminology C859.
3.2 Definitions:
3.2.1 calibration, n—the set of operations that establishes, under specified conditions, a metrologically traceable relationship
between a value measured or indicated by an instrument or system to a corresponding known value, typically derived from
appropriate reference standards or established physical constants
3.2.1.1 Discussion—
The calibration relationship can be expressed by a statement, function, diagram or table.
3.2.1.2 Discussion—
Test Method C1108 is an example of calibration using established physical constants.
3.2.1.3 Discussion—
Additional details on calibration require
...

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Test Method for Shrinkage Temperature of Wet Blue and Wet White

SIGNIFICANCE AND USE
5.1 This test method is designed to determine the temperature at which the Wet Blue or Wet White specimen experiences shrinkage. In this test method, shrinkage occurs as a result of hydrothermal denaturation of the collagen protein molecules which make up the fiber structure of the Wet Blue or Wet White. The shrinkage temperature of Wet Blue or Wet White is influenced by many different factors, most of which appear to affect the number and nature of crosslinking interactions between adjacent polypeptide chains of the collagen protein molecules. The value of the shrinkage temperature of Wet Blue or Wet White is commonly used as an indicator of the type of tannage or the degree of tannage, or both, of that particular Wet Blue or Wet White (especially for the more hydrothermally stable tannages such as chrome tannage).
SCOPE
1.1 This test method covers the determination of the shrinkage temperature of all types of Wet Blue and Wet White. The heating medium is water when the shrinkage temperature is at or below 98 °C. The heating medium is a glycerine-water solution when the shrinkage temperature is above 98 °C.  
1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D8530/D8530M-23(Guide)
Standard Guide for the Selection and Use of Waterstops

SIGNIFICANCE AND USE
4.1 This guide is intended to be used in the selection and installation of waterstops in cast-in-place concrete construction. This guide is intended to assist the building owner, owner’s representative, architect, engineer, contractor, and/or authorized inspector during the specification and installation of waterstops.  
4.2 This guide is applicable to cast-in-place concrete construction. The use of this guide may not be appropriate for installation of waterstops in other types of concrete construction, including but not limited to, pneumatically applied (that is, shotcrete) and precast concrete construction.
SCOPE
1.1 This guide covers the use of waterstops within cast-in-place concrete construction. Waterstops are generally placed within static, non-moving construction joints in concrete to close off the joint to water, which may be under significant hydrostatic pressure. They are used as part of the overall waterproofing strategy for a building or other structure. Expansion and other types of moving joints may require the use of waterstops, which can accommodate the anticipated movement of the structure and are beyond the scope of this guide.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents: therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM E2956-23(Guide)
Standard Guide for Monitoring the Neutron Exposure of LWR Reactor Pressure Vessels

SIGNIFICANCE AND USE
4.1 Regulatory Requirements—The USA Code of Federal Regulations (10CFR Part 50, Appendix H) requires the implementation of a reactor vessel materials surveillance program for all operating LWRs. Other countries have similar regulations. The purpose of the program is to (1) monitor changes in the fracture toughness properties of ferritic materials in the reactor vessel beltline6 resulting from exposure to neutron irradiation and the thermal environment, and (2) make use of the data obtained from surveillance programs to determine the conditions under which the vessel can be operated with adequate margins of safety throughout its service life. Practice E185, derived mechanical property data, and (r, θ, z) physics-dosimetry data (derived from the calculations and reactor cavity and surveillance capsule measurements (1) using physics-dosimetry standards) can be used together with information in Guide E900 and Refs. 4, 11-18 to provide a relation between property degradation and neutron exposure, commonly called a “trend curve.” To obtain this trend curve at all points in the pressure vessel wall requires that the selected trend curve be used together with the appropriate (r, θ, z) neutron field information derived by use of this guide to accomplish the necessary interpolations and extrapolations in space and time.  
4.2 Neutron Field Characterization—The tasks required to satisfy the second part of the objective of 4.1 are complex and are summarized in Practice E853. In doing this, it is necessary to describe the neutron field at selected (r, θ, z) points within the pressure vessel wall. The description can be either time dependent or time averaged over the reactor service period of interest. This description can best be obtained by combining neutron transport calculations with plant measurements such as reactor cavity (ex-vessel) and surveillance capsule or RPV cladding (in-vessel) measurements, benchmark irradiations of dosimeter sensor materials, and knowledge of th...
SCOPE
1.1 This guide establishes the means and frequency of monitoring the neutron exposure of the LWR reactor pressure vessel throughout its operating life.  
1.2 The physics-dosimetry relationships determined from this guide may be used to estimate reactor pressure vessel damage through the application of Practice E693 and Guide E900, using fast neutron fluence (E > 1.0 MeV and E > 0.1 MeV), displacements per atom (dpa), or damage-function-correlated exposure parameters as independent exposure variables. Supporting the application of these standards are the E853, E944, E1005, and E1018 standards, identified in 2.1.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Guide
    12 pages
    English language
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  • Guide
    12 pages
    English language
    sale 15% off