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ASTM

ASTM D7861-14

(Test Method)

Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy

Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy

General Information

Status
Historical
Publication Date
14-Dec-2014
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.04.0F - Absorption Spectroscopic Methods
Current Stage
Ref Project

Relations

Replaced By
ASTM D7861-14e1 - Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy
Effective Date
15-Dec-2014
Referred By
ASTM D7467-20a - Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
Effective Date
15-Dec-2014
Referred By
ASTM D396-21 - Standard Specification for Fuel Oils
Effective Date
15-Dec-2014
Referred By
ASTM D975-23 - Standard Specification for Diesel Fuel
Effective Date
15-Dec-2014

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ASTM D7861-14 - Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared SpectroscopyASTM D7861-14 - Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy
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ASTM D7861-14 - Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D7861 − 14
StandardTest Method for
Determination of Fatty Acid Methyl Esters (FAME) in Diesel
Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared
1
Spectroscopy
This standard is issued under the fixed designation D7861; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D4177 Practice for Automatic Sampling of Petroleum and
Petroleum Products
1.1 This test method determines fatty acid methyl esters
D4307 Practice for Preparation of Liquid Blends for Use as
(FAME or biodiesel) in diesel fuel oils. FAME can be
Analytical Standards
quantitatively determined from 1.0 % to 30.0 % by volume.
D5854 Practice for Mixing and Handling of Liquid Samples
This test method uses linear variable filter (LVF) array based
of Petroleum and Petroleum Products
mid-infrared spectroscopy for monitoring FAME concentra-
D6299 Practice for Applying Statistical Quality Assurance
tion.
and Control Charting Techniques to Evaluate Analytical
NOTE 1—See Section 6 for a list of interferences that could affect the
Measurement System Performance
results produced from this method.
D6300 Practice for Determination of Precision and Bias
1.2 This test method uses a horizontal attenuated total
Data for Use in Test Methods for Petroleum Products and
reflectance (HATR) crystal and a univariate calibration.
Lubricants
D6751 Specification for Biodiesel Fuel Blend Stock (B100)
1.3 The values stated in SI units are to be regarded as
for Middle Distillate Fuels
standard. No other units of measurement are included in this
D7371 Test Method for Determination of Biodiesel (Fatty
standard.
AcidMethylEsters)ContentinDieselFuelOilUsingMid
1.4 This standard does not purport to address all of the
Infrared Spectroscopy (FTIR-ATR-PLS Method)
safety concerns, if any, associated with its use. It is the
D7467 Specification for Diesel Fuel Oil, Biodiesel Blend
responsibility of the user of this standard to establish appro-
(B6 to B20)
priate safety and health practices and determine the applica-
E168 Practices for General Techniques of Infrared Quanti-
bility of regulatory limitations prior to use.
3
tative Analysis (Withdrawn 2015)
E1655 Practices for Infrared Multivariate Quantitative
2. Referenced Documents
Analysis
2
2.1 ASTM Standards:
D975 Specification for Diesel Fuel Oils
3. Terminology
D1298 Test Method for Density, Relative Density, or API
3.1 Definitions:
Gravity of Crude Petroleum and Liquid Petroleum Prod-
3.1.1 biodiesel, n—fuel comprised of mono-alkyl esters of
ucts by Hydrometer Method
long chain fatty acids derived from vegetable oils or animal
D4052 Test Method for Density, Relative Density, and API
fats, designated B100.
Gravity of Liquids by Digital Density Meter
3.1.2 biodiesel blend (BXX), n—blend of biodiesel fuel with
D4057 Practice for Manual Sampling of Petroleum and
diesel fuel oils.
Petroleum Products
3.1.2.1 Discussion—In the abbreviation, BXX, the XX rep-
resents the volume percentage of biodiesel fuel in the blend.
1 3.1.3 diesel fuel, n—petroleum-based middle distillate fuel.
This test method is under the jurisdiction of ASTM Committee D02 on
Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of
3.1.4 univariate calibration, n—aprocess for creating a
Subcommittee D02.04.0F on Absorption Spectroscopic Methods.
calibration model in which a single measured variable, for
Current edition approved Dec. 15, 2014. Published February 2015. DOI:
10.1520/D7861-14.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on The last approved version of this historical standard is referenced on
the ASTM website. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D7861 − 14
example, the absorbance at a particular wavelength, is corre- 6.5 This test method is not appropriate for fatty acid ethyl
lated with the concentration or property values for a set of esters (FAEE). FAEEs will cause a negative bias.
calibration samples.
7. Apparatus
3.2 Acronyms:
3.2.1 ATR, n—attenuated total reflectance 7.1 Mid-Infrared Spectrometer:
7.1.1 LVF Array Based Mid-Infrared Spectrometer—The
3.2.2 BXX, n—see 3.1.2
type of apparatus suitable for use in this test method employs
3.2.3 FAEE, n—fatty acid ethyl esters
an IR source, a HATR crystal, a LVF paired to a detector array,
3.2.4 FAME, n—fatty acid meth
...

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