ASTM D3806-98(2011)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D3806 − 98 (Reapproved 2011)
Standard Test Method of
Small-Scale Evaluation of Fire-Retardant Paints (2-Foot
Tunnel Method)
This standard is issued under the fixed designation D3806; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
1.1 This test method determines the protection a coating 2.1 ASTM Standards:
affords its substrate, and the comparative burning characteris- C220Specification for Flat Asbestos-Cement Sheets
ticsofcoatingsbyevaluatingtheflamespreadoverthesurface D344Test Method for Relative Hiding Power of Paints by
when ignited under controlled conditions in a small tunnel. the Visual Evaluation of Brushouts
This establishes a basis for comparing surface-burning charac- D1475Test Method For Density of Liquid Coatings, Inks,
teristics of different coatings without specific consideration of and Related Products
all the end-use parameters that might affect surface-burning D2196Test Methods for Rheological Properties of Non-
characteristics under actual fire conditions. Newtonian Materials by Rotational (Brookfield type)
Viscometer
1.2 In addition to the experimental flamespread rate, the
E84Test Method for Surface Burning Characteristics of
weight of panel consumed, time of afterflaming and afterglow,
Building Materials
chardimensionsandindex,andheightofintumescencemaybe
2.2 Federal Standard:
measured in this test. However, a relationship should not be
Fed. Spec. TT-V-119Varnish, Spar, Phenolic Resin
presumed among these measurements.
3. Significance and Use
1.3 This standard should be used to measure and describe
the properties of materials, products, or assemblies in response
3.1 Anumber of laboratory procedures are used to evaluate
to heat and flame under controlled laboratory conditions, and
the effectiveness of fire-retardant and fire-resistant treatments
shouldnotbeusedtodescribeorappraisethefirehazardorfire
and coatings. In general, these methods measure the three
risk of materials, products, or assemblies under actual fire
stages of fire development: (1) ignition; (2) flame spread (rate
conditions. However, results of this test may be used as
of growth of the fire); and (3) conflagration extent. While all
elements of a fire risk assessment which takes into account all
three are of extreme importance, flame spread has been
of the factors which are pertinent to an assessment of the fire
recognized as the main factor associated with testing fire-
hazard of a particular end use.
retardant coatings.
1.4 The values stated in SI units are to be regarded as the
3.2 Flame spread ratings based uponTest Method E84 have
standard. The values given in parentheses are for information
acquired common acceptance by regulatory agencies, but such
only.
large-scale tests are seldom practical during the development
1.5 This standard does not purport to address all of the
or modification of a fire-retardant coating.
safety concerns, if any, associated with its use. It is the
3.3 This test method provides the relative flame spread of
responsibility of the user of this standard to establish appro-
experimental coatings using small test specimens. By calibrat-
priate safety and health practices and determine the applica-
ingthe2-foottunnelwithTestMethodE84-ratedfire-retardant
bility of regulatory limitations prior to use.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
This test method is under the jurisdiction of ASTM Committee D01 on Paint contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
and Related Coatings, Materials, andApplications and is the direct responsibility of Standards volume information, refer to the standard’s Document Summary page on
Subcommittee D01.21 on Chemical Analysis of Paints and Paint Materials. the ASTM website.
Current edition approved June 1, 2011. Published June 2011. Originally Available from Standardization Documents Order Desk, DODSSP, Bldg. 4,
approved in 1979. Last previous edition approved in 2004 as D3806–98(2004). Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http://
DOI: 10.1520/D3806-98R11. dodssp.daps.dla.mil.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D3806 − 98 (2011)
paint, results obtained by this test method should be indicative 4.2 Burner, 215 mm (8.5 in.) high with 40-mm diameter,
ofthoseobtainedwithalargespecimenintheTestMethodE84 10-mmthickgridforusewithnaturalgas.Theburnerisplaced
tunnel. 57 mm (2 ⁄4 in.) in from the fire end of the tunnel and 25 mm
(1 in.) below the bottom side of the sample holder, that is, 30
4. Apparatus
mm (1 ⁄8 in.) from the bottom of the specimen. See Fig. 1.
4.1 Flame Tunnel (seeFig.1A)—610-mm(two-foot)flame
NOTE 2—Artificial gas or liquid petroleum (LP) gas may be used, but
tunnelconsistingofasbestos-cementboardmountedonaniron
burners designed for these types of gases must be used.
framework and supplied with natural gas fuel of uniform
4.3 Ignition Transformer, or other suitable ignition source,
quality.
to generate a spark through a 2-mm ( ⁄16-in.) Nichrome wire to
4.1.1 The framework is constructed of 3 by 25 by 25-mm
theburnerbarrel.Thetransformerisactivatedbyapush-button
( ⁄8 by 1 by 1-in.) angle iron, the top of which provides a 610
type spark switch.
by100-mm(24by4-in.)specimenholderinclinedat28°tothe
horizontal. The framework is mounted on a 250 by 610 by
4.4 Gas Supply, of uniform quality controlled by a positive-
13-mm (10 by 24 by ⁄2-in.) steel base.The specimen holder is flowpressureregulatoryvalve(0to152mm(0to6in.)water)
elevated185mm(7 ⁄8in.)abovethebaseatthelower(fire)end and a gas flowmeter (0.6 to 5.0 SCFH).
and 480 mm (18 ⁄8 in.) at the upper (flue) end.
4.5 Insulating and Fire Resistant Backing for Test Panels,
4.1.2 The fire end and sides of the tunnel are covered to the
7 7
consisting of 100 by 605-mm (3 ⁄8 by 23 ⁄8-in.) pieces of
extent shown in Fig. 1, with 6-mm ( ⁄4-in.) asbestos-cement
13-mm ( ⁄2-in.) asbestos-cement board or inorganic reinforced
5 6
board or 6-mm ( ⁄4-in.) inorganic reinforced-cement board
cementboardand ⁄2-in.steelplateappliedoneabovetheother
attached to the inside of the angle iron framework. The open
with asbestos cement or the inorganic reinforced cement board
flue end and the cut-out sides allow a natural draft through the
placed directly on top of the test panel.
tunnel. Additional air access is provided by a 25-mm (1-in.)
4.6 Thermocouple totally shielded (see Note 3), installed
hole drilled in the cover at the fire end, centered and 115 mm
through the hole in the side of the specimen holder so that its
(4 ⁄2 in.) above the base.
tip rests on the back, cool side, of the test panel.
4.1.3 Anobservationwindowmadeofa50-mm(2-in.)wide
strip of 3-mm ( ⁄8-in.) polished heat-resistant sheet glass is
NOTE 3—Some commercial tunnels are supplied with more than one
located just below the specimen holder, extending the full thermocouple.
length of the tunnel, 610 mm (24 in.). This glass is marked by
4.7 Recording Potentiometer, 0 to 300°C range.
anyappropriatemethodat1-in.intervalsfrom4to22in.A560
4.8 Audible Timer, set to sound at 15-s intervals to indicate
1 1
by 55 by 2-mm (22 by 2 ⁄4 by ⁄16-in.) sheet metal shield is
the time for flame-front measurements.
attached above the window, slanting downwards at an angle of
60° to shield the observation window. The angle iron panel 4.9 Constant Temperature and Humidity Room or Cabinet,
maintained at 50 6 5% relative humidity and 23 6 2°C (73.5
holder is notched along the bottom or supporting lip of the
angle at 25-mm (1-in.) intervals to assist in the measurements 6 3.5°F).
of the flame advance.
5. Test Panels
NOTE 1—Arule may also be mounted outside the observation window
5.1 Test Panels—SeeTable1foralistofvariouswoodsand
to help measure the flame advancement.
1 7
their densities. Wood, 6 by 100 by 605-mm ( ⁄4 by 3 ⁄8 by
4.1.4 A 2.5-mm ( ⁄32-in.) hole is drilled in the side of the
23 ⁄8-in.) close grained, as nearly edge grain as possible and
specimen holder immediately above the center of the burner to
free from knots and imperfections. The panels should be solid
allow insertion of a thermocouple.
wood with surfaces planed and sanded (see Note 4). Kiln-dry
4.1.5 The tunnel should be placed in an area as free from
test panels to contain not more than 10 weight% of moisture
drafts as possible with facilities for removal or escape of
on an oven dry basis.
combustion products. (Standard laboratory hood with forced
NOTE 4—Douglas fir, 6.3-mm ( ⁄4-in.) 3-ply, marine–grade plywood
draft off during test.)
may be used upon agreement between manufacturer and user. Asbestos-
cement board, steel, or concrete may be used upon agreement between
The sole source of supply of a suitable cabinet and assembly known to the
manufacturer and user.
committeeatthistimeisDek-TronScientific,244East3rdSt.,Plainfield,NJ07060.
If you are aware of alternative suppliers, please provide this information toASTM 5.1.1 Prior to coating, condition test panels for 14 days in
International Headquarters. Your comments will receive careful consideration at a
the controlled atmosphere of 50 6 5% relative humidity and
meeting of the responsible technical committee, which you may attend.
The sole source of supply of an asbestos-cement board, transite, known to the
committee at this time is Manville Corp., Denver CO 80217 If you are aware of The sole source of supply of a burner, Catalog No. 3–902 for artificial gas, or
alternative suppliers, please provide this information to ASTM International CatalogNo.3–900and3–902fornaturalgasandLPgas,respectively,knowntothe
Headquarters.Your comments will receive careful consideration at a meeting of the committee at this time is Fisher Scientific Co. If you are aware of alternative
responsible technical committee, which you may attend. suppliers, please provide this information to ASTM International Headquarters.
The sole source of supply of inorganic reinforced-cement board, #100S and Your comments will receive careful consideration at a meeting of the responsible
3 3 1
100H, nominal 1600 to 1760 kg/m (100 to 110 lb/ft ), known to the committee at technical committee, which you may attend.
this time is Shameful Corp., 100 Spence Lane, Nashville, TN 37210. If you are The sole source of supply of a thermocouple, Megopak Type J, known to the
aware of alternative suppliers, please provide this information to ASTM Interna- committee at this time is Megopak Co. If you are aware of alternative suppliers,
tional Headquarters.Your comments will receive careful consideration at a meeting please provide this information to ASTM International Headquarters. Your com-
of the responsible technical committee, which you may attend. ments will receive careful consideration at a meeting of the responsible technical
7 1
Quartz or high-silica glass has been found satisfactory for this purpose. committee, which you may attend.
D3806 − 98 (2011)
FIG. 1 Flame Tunnel
D3806 − 98 (2011)
TABLE 1 Densities and Panel Weights of Various Woods (Conditioned at Relative Humidity 50 ± 5 % and 23± 2°C
(73.5 ± 3.5°F) for 14 days)
7 7 1
Density (9 to 10 % Moisture), Weight of 3 ⁄8 by 23 ⁄8 by ⁄4 in.
Type of Wood
3 3
kg/m (lb/ft ) Panel, g
Red cedar 345 to 360 (21.4 to 22.4) 130 to 140
Douglas fir 465 to 560 (29 to 35) 180 to 215
White pine-Ponderosa pine 360 to 420 (22.4 to 26.4) 140 to 160
Southern yellow pine 495 to 590 (31 to 37) 190 to 225
Redwood 435 to 450 (27.2 to 28.2) 165 to 175
23 6 2°C (73.5 6 3.5°F) toa9to10% moisture content. 60.5 D
W 5 (2)
Refer to Table 1 for the density and weight per panel of each S
R
listed wood.
where:
5.1.2 Seal the ends of the panels with two coats of varnish
W = weight of applied wet coating, g,
conforming to Fed. Spec. TT-V-119 after conditioning. Allow
D = coating density, g/mL, and
each coat of varnish to air-dry 18 to 24 h.
S = spreading rate in m /L.
R
6. Calibration Standards
7.5 Dry the coated panels under standard conditions (4.9)
until equilibrium weight is obtained, allowing sufficient time
6.1 Zero-Flame Spread—Asbestos-cement board, Type F
forthecompleteevaporationofsolvents,anycuringthatmight
conforming to Specification C220, 13 by 100 by 605 mm ( ⁄2
be required by the material, and for the attainment of equilib-
7 7
by 3 ⁄8 by 23 ⁄8 in.), conditioned as in 5.1.1.
rium moisture content. Forty-eight hours are normally suffi-
NOTE5—Inorganicreinforcedcementboard,6.3-mm( ⁄4-in.)thickmay
cient except for certain coatings that may require longer
be substituted for asbestos cement.
periods because they trap solvent or contain solvents that
6.2 Fire-Rated Standard—A test panel, similar to that used
evaporate very slowly.
with test coatings, coated with Test Method E84 rated paint at
7.6 Apply and cure non-air–drying coatings as recom-
the manufacturer’s recommended spreading rate and condi-
mended by the supplier and condition as specified in 7.5.
tioned as in Section 7.
NOTE 6—Do not use paint beyond manufacturer’s stated shelf life.
8. Calibration of the Tunnel
8.1 Calibrate the tunnel prior to each day’s operation with
7. Preparation of Test Panels
the calibration standards described in Section 6.
7.1 Thoroughly mix the coating under test by a suitable
8.1.1 Place the zero flame-spread standard in the holder,
means until it is uniform in composition and consistency. Test
smooth side down, and back it with the backing plate (4.5).
Methods D2196 describes a suitable preparation procedure.
8.1.2 Open the gas valve and adjust to a pressure of 1.3 kPa
7.2 Determine the density of the coating in accordance with
2 3
(3 oz/in. ) and a constant flow of 38 mL/s (4.8 ft /h), and
Test Method D1475 in grams per millilitre (or pounds per
actuate the interval timer.
gallon) for calculating the weight of the coating to be applied
to the panel to comply with the specified spreading rate.
NOTE 7—These conditions are specified for a natural gas supply
3 3
providing40MJ/m (1055BTU/ft ).Foranyothergassupply,adjustflow
7.3 Brush apply the coating to conditioned test panels in as
to provide 1490 J/s (5085 BTU/h).
uniform a manner as possible to obtain the specified spreading
8.1.2.1 When the timer sounds, ignite the burner using the
rate. A suitable procedure appears in Test Method D344.
ignition transformer. Observe the flame front, measure in
Application may be by other conventional means and i
...