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M/388 - PCBs from stationary

Standardisation Mandate to CEN for Standard Measuring methods for the determination of dioxin-like PCBs from stationary sources

General Information

Organization
CEN - CEN European Committee for Standardization
Status
Confirmed
Resolution Reference
CEN/BT C022/2006
Resolution Date
05-Jun-2006
Type Of Decision
(Dis-)Approval of mandate

Frequently Asked Questions

A European Standardization Mandate is a formal request from the European Commission to the European Standardization Organizations (CEN, CENELEC, and ETSI) to develop European standards (ENs) in support of EU legislation and policies. Mandates are issued under Regulation (EU) No 1025/2012 and help ensure that products and services meet the essential requirements set out in EU directives and regulations.

M/388 is a European Standardization Mandate titled "Standardisation Mandate to CEN for Standard Measuring methods for the determination of dioxin-like PCBs from stationary sources". Standardisation Mandate to CEN for Standard Measuring methods for the determination of dioxin-like PCBs from stationary sources There are 4 standards developed under this mandate.

Standards developed in response to a mandate and cited in the Official Journal of the European Union become "harmonized standards". Products manufactured in compliance with harmonized standards benefit from a presumption of conformity with the essential requirements of the corresponding EU directive or regulation, facilitating CE marking and market access across the European Economic Area.

Standardization Organization
ICS
Technical Committee
Directive
50
SIST
SIST EN 1948-4:2011(Main)
Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 4: Sampling and analysis of dioxin-like PCBs
EN 1948-4:2010

This European Standard specifies sampling from stationary sources, extraction, clean-up, identification and quantification procedures of the dioxin-like PCBs. The procedure described lays down requirements to measure the PCB congeners given in Annex A (see Table A.1). It is applicable to the 12 non- and mono-ortho PCB designated by the WHO. It is optimised to measure PCB concentrations of about 0,01 ng WHO-TEQPCB/m3.
In addition to the 12 non- and mono-ortho-PCB the present document is also applicable to measure further PCB-congeners like the "marker PCB" 28, 52, 101, 138, 153, 180 (see Annex F).
This document specifies a framework of quality control requirements which should be fulfilled by any PCB sampling, extraction, clean-up, identification and quantification methods to be applied.
As a result of their similar chemical behaviour PCBs, as shown in the validation campaign, can be sampled from stationary sources together with the PCDDs/PCDFs. Therefore, it is possible to measure PCBs together with PCDDs/PCDFs by applying EN 1948-1, -2, -3 and -4. The complete sampling procedure is described in EN 1948-1. Each of the three sampling methods of EN 1948-1 can be combined with the methods described in this document to complete the measurement procedure. EN 1948-1 is an integral part of the complete measurement procedure and is necessary for the determination of PCBs.
The analyses of the following PCB congeners is described in this European Standard and is validated in the validation campaign:
a)   Non-ortho substituted PCBs
1)   3,3’,4,4’-TeCB(77)
2)   3,4,4’,5-TeCB (81)
3)   3,3’,4,4’,5-PeCB (126)
4)   3,3’,4,4’,5,5’-HxCB (169)
b)   Mono-ortho substituted PCBs
1)   2,3,3’,4,4’-PeCB (105)
2)   2,3,4,4’,5-PeCB (114)
3)   2,3’,4,4’,5-PeCB (118)
4)   2’,3,4,4’,5-PeCB (123)
5)   2,3,3’,4,4’,5-HxCB (156)
6)   2,3,3’,4,4’,5’-HxCB (157)
7)   2,3’,4,4’,5,5’-HxCB (167)
8)   2,3,3’,4,4’,5,5’-HpCB (189)
c)   Marker PCBs
1)   2,4,4'- TriCB (28)
2)   2,2',5,5'-TeCB (52)
3)   2,2',4,5,5'- PeCB

  • Standard
    59 pages
    English language
    e-Library read for
    1 day
CEN
EN 1948-4:2010(Main)
Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 4: Sampling and analysis of dioxin-like PCBs
SIST EN 1948-4:2011

This European Standard specifies sampling from stationary sources, extraction, clean-up, identification and quantification procedures of the dioxin-like PCBs. The procedure described lays down requirements to measure the PCB congeners given in Annex A (see Table A.1). It is applicable to the 12 non- and mono-ortho PCB designated by the WHO. It is optimised to measure PCB concentrations of about 0,01 ng WHO-TEQPCB/m3.
In addition to the 12 non- and mono-ortho-PCB the present document is also applicable to measure further PCB-congeners like the "marker PCB" 28, 52, 101, 138, 153, 180 (see Annex F).
This document specifies a framework of quality control requirements which should be fulfilled by any PCB sampling, extraction, clean-up, identification and quantification methods to be applied.
As a result of their similar chemical behaviour PCBs, as shown in the validation campaign, can be sampled from stationary sources together with the PCDDs/PCDFs. Therefore, it is possible to measure PCBs together with PCDDs/PCDFs by applying EN 1948-1, -2, -3 and -4. The complete sampling procedure is described in EN 1948-1. Each of the three sampling methods of EN 1948-1 can be combined with the methods described in this document to complete the measurement procedure. EN 1948-1 is an integral part of the complete measurement procedure and is necessary for the determination of PCBs.
The analyses of the following PCB congeners is described in this European Standard and is validated in the validation campaign:
a)   Non-ortho substituted PCBs
1)   3,3’,4,4’-TeCB(77)
2)   3,4,4’,5-TeCB (81)
3)   3,3’,4,4’,5-PeCB (126)
4)   3,3’,4,4’,5,5’-HxCB (169)
b)   Mono-ortho substituted PCBs
1)   2,3,3’,4,4’-PeCB (105)
2)   2,3,4,4’,5-PeCB (114)
3)   2,3’,4,4’,5-PeCB (118)
4)   2’,3,4,4’,5-PeCB (123)
5)   2,3,3’,4,4’,5-HxCB (156)
6)   2,3,3’,4,4’,5’-HxCB (157)
7)   2,3’,4,4’,5,5’-HxCB (167)
8)   2,3,3’,4,4’,5,5’-HpCB (189)
c)   Marker PCBs
1)   2,4,4'- TriCB (28)
2)   2,2',5,5'-TeCB (52)
3)   2,2',4,5,5'- PeCB

  • Standard
    59 pages
    English language
    e-Library read for
    1 day
SIST
SIST-TS CEN/TS 1948-4:2008(Main)
Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 4: Sampling and analysis of dioxin-like PCBs
CEN/TS 1948-4:2007

This document specifies sampling from stationary sources, extraction, clean-up, identification and quantification procedures of the dioxin-like PCBs. The procedure described lays down requirements to measure the PCB congeners given in Annex A (see Table A.1). It is applicable to the twelve non- and mono-ortho PCB designated by the WHO. It is optimised to measure PCB concentrations in the range of 0,01 ng WHO-TEQPCB/m3.
In addition to the 12 non- and mono-ortho-PCB the present document is also applicable to measure further PCB-congeners like the so-called “marker PCB” 28, 52, 101, 138, 153, 180 (see Annex D).
This document specifies a framework of quality control requirements which have to be fulfilled by any PCB sampling, extraction, clean-up, identification and quantification methods to be applied.
It is assumed that due to their similar chemical behaviour PCBs may be sampled from stationary sources together with the PCDDs/PCDFs by the same methods. The complete sampling procedure is described in the EN 1948-1. Each of the three sampling methods of EN 1948-1 can be combined with the methods described in this document to complete the measurement procedure. EN 1948-1 is an integral part of the complete measurement procedure and is necessary for the determination of PCBs.
In addition it is possible to measure PCBs together with PCDDs/PCDFs by applying EN 1948 Part 1, Part 2, Part 3 and CEN/TS 1948 Part 4.

  • Technical specification
    41 pages
    English language
    e-Library read for
    1 day
CEN
CEN/TS 1948-4:2007(Main)
Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 4: Sampling and analysis of dioxin-like PCBs
SIST-TS CEN/TS 1948-4:2008

This document specifies sampling from stationary sources, extraction, clean-up, identification and quantification procedures of the dioxin-like PCBs. The procedure described lays down requirements to measure the PCB congeners given in Annex A (see Table A.1). It is applicable to the twelve non- and mono-ortho PCB designated by the WHO. It is optimised to measure PCB concentrations in the range of 0,01 ng WHO-TEQPCB/m3.
In addition to the 12 non- and mono-ortho-PCB the present document is also applicable to measure further PCB-congeners like the so-called “marker PCB” 28, 52, 101, 138, 153, 180 (see Annex D).
This document specifies a framework of quality control requirements which have to be fulfilled by any PCB sampling, extraction, clean-up, identification and quantification methods to be applied.
It is assumed that due to their similar chemical behaviour PCBs may be sampled from stationary sources together with the PCDDs/PCDFs by the same methods. The complete sampling procedure is described in the EN 1948-1. Each of the three sampling methods of EN 1948-1 can be combined with the methods described in this document to complete the measurement procedure. EN 1948-1 is an integral part of the complete measurement procedure and is necessary for the determination of PCBs.
In addition it is possible to measure PCBs together with PCDDs/PCDFs by applying EN 1948 Part 1, Part 2, Part 3 and CEN/TS 1948 Part 4.

  • Technical specification
    41 pages
    English language
    e-Library read for
    1 day
50