SIST EN 14214:2003

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Kraftstoffe für Kraftfahrzeuge - Fettsäure-Methylester (FAME) für Dieselmotoren - Anforderungen und PrüfverfahrenCarburants pour automobiles - Esters méthyliques d'acide gras (EMAG) pour moteurs diesel - Exigences et méthodes d'essaisAutomotive fuels - Fatty acid methyl esters (FAME) for diesel engines - Requirements and test methods75.160.20Liquid fuelsICS:Ta slovenski standard je istoveten z:EN 14214:2003SIST EN 14214:2003en01-november-2003SIST EN 14214:2003SLOVENSKI
STANDARD



SIST EN 14214:2003



EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 14214July 2003ICS 75.160.20English versionAutomotive fuels - Fatty acid methyl esters (FAME) for dieselengines - Requirements and test methodsCarburants pour automobiles - Esters méthyliques d'acidegras (EMAG) pour moteurs diesel - Exigences et méthodesd'essaisKraftstoffe für Kraftfahrzeuge - Fettsäure-Methylester(FAME) für Dieselmotoren - Anforderungen undPrüfverfahrenThis European Standard was approved by CEN on 14 February 2003.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and UnitedKingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2003 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 14214:2003 ESIST EN 14214:2003



EN 14214:2003 (E)2ContentsForeword.31Scope.42Normative references.43Sampling.54Pump marking.65Requirements and test methods.65.1Dyes and markers.65.2Additives.65.3Generally applicable requirements and related test methods.65.4Climate dependent requirements and related test methods.85.5Precision and dispute.8Annex A (Normative) Details of interlaboratory test programme.9Annex B (Normative) Calculation of Iodine Value.10B.1Scope.10B.2Definition.10B.3Procedure.10B.4Expression of the result.11Annex C (Normative) Correction factor for calculation of density of FAME.12SIST EN 14214:2003



EN 14214:2003 (E)3ForewordThis document EN 14214:2003 has been prepared by Technical Committee CEN/TC 19 “Petroleumproducts, lubricants and related products”, the secretariat of which is held by NEN.This European Standard shall be given the status of a national standard, either by publication of anidentical text or by endorsement, at the latest by January 2004, and conflicting national standardsshall be withdrawn at the latest by January 2004.This document has been prepared under a mandate given to CEN by the European Commission andthe European Free Trade Association.This document has been prepared by CEN /TC 19, "Petroleum products, lubricants and relatedproducts".This European standard exists in parallel with: EN 590 "Automotive fuels - Diesel - Requirements andtest methods".This standard gives all relevant characteristics, requirements and test methods for FAME, which areknown at this time to be necessary to define the product to be used as automotive diesel fuel,including iodine value. The stability characteristics of FAME are under investigation in an EU-fundedresearch programme ‘BIOSTAB’, and suitable limits and test methods may be incorporated into anamended version of this standard upon successful conclusion of this programme, including a possiblereplacement for iodine value.Many of the test methods included in this standard were the subject of interlaboratory testing todetermine the applicability of the method and its precision in relation to different sources of fatty acidmethyl esters. These fatty acid methyl esters were produced from rapeseed and sunflower oil.Annex A is normative and contains the precision data generated on the test methods which are theresult of the interlaboratory testing as mentioned above, carried out by working groups of CEN/TC 19.Annex B and C, also normative, contain details on calculations.According to the CEN/CENELEC Internal Regulations, the national standards organizations of thefollowing countries are bound to implement this European Standard: Austria, Belgium, CzechRepublic, Denmark, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Luxembourg,Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and the UnitedKingdom.SIST EN 14214:2003



EN 14214:2003 (E)41 ScopeThis European Standard specifies requirements and test methods for marketed and delivered fatty acidmethyl esters (FAME) to be used either as automotive fuel for diesel engines at 100% concentration, oras an extender for automotive fuel for diesel engines in accordance with the requirements of EN 590. At100% concentration it is applicable to fuel for use in diesel engine vehicles designed or subsequentlyadapted to run on 100% FAME.NOTEFor the purposes of this European Standard, the term “% (m/m)” is used to represent the massfraction.2 Normative referencesThis European Standard incorporates by dated or undated reference, provisions from other publications.These normative references are cited at the appropriate places in the text and the publications are listedhereafter. For dated references, subsequent amendments to or revisions of any of these publicationsapply to this European Standard only when incorporated in it by amendment or revision. For undatedreferences the latest edition of the publication referred to applies.EN 116:1997, Diesel and domestic heating fuels – Determination of cold filter plugging pointEN 590:1999, Automotive fuels - Diesel - Requirements and test methodsEN 12662:1998, Liquid petroleum products - Determination of contamination in middle distillatesEN 14103:20031) , Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) – Determination of esterand linolenic acid methyl ester contentsEN 14104:20031), Fat and oil derivatives – Fatty Acid Methyl Esters (FAME) - Determination of acidvalueEN 14105:20031), Fat and oil derivatives – Fatty Acid Methyl Esters (FAME) – Determination offree and total glycerol and mono-, di- and triglyceride content –(Reference method)EN 14106:20031), Fat and oil derivatives – Fatty Acid Methyl Esters (FAME)– Determination of freeglycerol contentEN 14107:20031), Fat and oil derivatives – Fatty Acid Methyl Esters (FAME) – Determination ofphosphorus content by inductively coupled plasma (ICP) emission spectrometryEN 14108:20031), Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) – Determination ofsodium content by atomic absorption spectrometryEN 14109:20031), Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) – Determination ofpotassium content by atomic absorption spectrometryEN 14110:20031), Fat and oil derivatives – Fatty Acid Methyl Esters (FAME) - Determination ofmethanol contentEN 14111:20031), Fat and oil derivatives – Fatty Acid Methyl Esters (FAME) – Determination of iodinevalueEN 14112:20031), Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) - Determination ofoxidation stability (accelerated oxidation test).
1)To be publishedSIST EN 14214:2003



EN 14214:2003 (E)5prEN 14538:2002 Fat and oil derivatives – Fatty acid methyl esters (FAME) – Determination of Ca andMg content by optical emission spectral analysis with inductively coupled plasma (ICP OES).EN ISO 2160:1998, Petroleum products - Corrosiveness to copper - Copper strip test(ISO 2160:1998).EN ISO 3104:1996, Petroleum products - Transparent and opaque liquids - Determination ofkinematic viscosity and calculation of dynamic viscosity (ISO 3104:1994).EN ISO 3104:1998/C2:1999, Petroleum products - Transparent and opaque liquids - Determination ofkinematic viscosity and calculation of dynamic viscosity (ISO 3104:1997, including Cor. 2:1999)EN ISO 31702) Petroleum liquids – Manual sampling.EN ISO 3171:1999, Petroleum liquids – Automatic pipeline sampling (ISO 3171:1988).EN ISO 3675:1998, Crude petroleum and liquid petroleum products - Laboratory determination ofdensity - Hydrometer method (ISO 3675:1998).prEN ISO 3679:20023), Determination of flash point - Rapid equilibrium closed cup method (ISO/DIS3679:2002).EN ISO 4259:1995, Petroleum products - Determination and application of precision data in relation tomethods of test (ISO 4259:1992, including Cor. 1:1993).EN ISO 5165:1998, Petroleum products - Diesel fuels - Determination of the ignition quality of dieselfuels - Cetane engine method (ISO 5165:1998).EN ISO 10370:1995, Petroleum products - Determination of carbon residue - Micro method(ISO 10370:1993).EN ISO 12185:1996/C1:2001, Crude petroleum and petroleum products - Determination of density -Oscillating U-tube method (ISO 12185:1996, including Cor. 1:2001).EN ISO 12937:2000, Petroleum products - Determination of water - Coulometric Karl Fisher titrationmethod (ISO 12937:2000).EN ISO 13759:1996, Petroleum products – Determination of alkyl nitrate in diesel fuels –Spectrometric method (ISO 13759:1996).prEN ISO 20846:2002, Petroleum products – Determination of the sulfur content of automative fuels –Energy-dispersive X-ray fluorescence spectrometry (ISO/DIS 20846:2002).prEN ISO 20884:2002, Petroleum products – Determination of low sulfur content of automotive fuels –Wavelength-dispersive X-ray fluorescence spectrometry (ISO/DIS 20884:2002).ISO 3987:1994, Petroleum products - Lubricating oils and additives - Determination of sulfated ash.ASTM D 1160:1999, Distillation of Petroleum Products at Reduced Pressure.3 SamplingSamples shall be taken as described in EN ISO 3170 or EN ISO 3171 and/or in accordance with therequirements of national standards or regulations for the sampling of automotive diesel fuel. The national
2)To be published (revision of EN ISO 3170:1995)3)Revision of ISO 3679:1983SIST EN 14214:2003



EN 14214:2003 (E)6requirements shall be set out in a national annex to this European Standard, either in detail or byreference only.In view of the sensitivity of some of the test methods referred to in this European Standard, particularattention shall be paid to compliance with any guidance on sampling containers, which is included inthe test method standard.4 Pump markingInformation to be marked
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