Bitumen and bituminous binders - Determination of dynamic viscosity of bitumen and bituminous binders by the cone and plate method

This document specifies a method for determining the dynamic viscosity of a bituminous binder over a range of temperatures by means of a cone and plate viscometer. The test method is intended for all bituminous binders (e.g. paving grade bitumen and polymer modified), unaged or aged. It is also suitable for recovered bituminous binders according to EN 12697 3 [1] and EN 12697 4 [2] with no or limited amount of filler.
WARNING - The use of this document may involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this document to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

Bitumen und bitumenhaltige Bindemittel - Bestimmung der dynamischen Viskosität von Bitumen und bitumenhaltigen Bindemitteln mit dem Platte-Kegel-Verfahren

Dieses Dokument legt ein Verfahren zur Bestimmung der dynamischen Viskosität eines bitumenhaltigen Bindemittels über einen bestimmten Temperaturbereich mit einem Platte-Kegel-Viskosimeter fest. Das Prüfverfahren ist für alle ungealterten oder gealterten bitumenhaltigen Bindemittel (z. B. Straßenbaubitumen und polymermodifizierte Bitumen) vorgesehen. Es eignet sich auch für rückgewonnene bitumenhaltige Bindemittel nach EN 12697 3 [1] und EN 12697 4 [2] mit geringem Fülleranteil oder ganz ohne Füller.
WARNUNG - Die Anwendung dieses Dokuments kann die Anwendung gefährlicher Stoffe, Arbeits-gänge und Geräte mit sich bringen. Dieses Dokument beansprucht nicht, alle damit verbundenen Sicherheitsprobleme zu behandeln. Es liegt in der Verantwortung des Anwenders dieses Dokuments, geeignete Maßnahmen für die Sicherheit und den Gesundheitsschutz zu ergreifen und dafür Sorge zu tragen, dass behördliche und gesetzliche Maßnahmen eingehalten werden.

BItume et liants bitumineux - Détermination de la viscosité dynamique des bitumes modifiés par la méthode cône et plateau

Le présent document prescrit une méthode permettant de déterminer la viscosité dynamique d‘un liant bitumineux sur une plage de températures, au moyen d'un viscosimètre à cône et plateau. La méthode d’essai est applicable à tous les liants bitumineux (bitume routier et bitume modifié par des polymères par exemple), avant ou après vieillissement. Elle est également applicable pour les liants bitumineux récupérés, conformément aux normes EN 12697-3 [1] et EN 12697-4 [2], avec peu ou pas de filler (fines).
AVERTISSEMEN - L'utilisation de ce document implique l'intervention de produits, d'opérations et d'équipements à caractère dangereux. Le présent document n'est pas censé aborder tous les problèmes de sécurité concernés par son usage. Il est de la responsabilité de l'utilisateur de ce document de consulter et d'établir des règles de sécurité et d'hygiène appropriées et de déterminer l'applicabilité des restrictions réglementaires avant utilisation.

Bitumen in bitumenska veziva - Določevanje dinamične viskoznosti bitumna in bitumenskih veziv z metodo s konusom in ploščo

Ta evropski standard določa metodo za določanje dinamične viskoznosti bitumenskih veziv pri različnih temperaturah s konusnim in ploščatim viskozimetrom. Preskusna metoda se uporablja za vsa bitumenska veziva (cestogradbeni bitumen in s polimeri modificiran bitumen). Uporablja se tudi za ponovno pridobljena bitumenska veziva v skladu s standardoma EN 12697 3 in EN 12697 4 z omejeno količino polnila ali brez njega.
OPOZORILO: Pri uporabi tega evropskega standarda so lahko prisotni nevarni materiali, postopki in oprema. Ta evropski standard ne obravnava vseh varnostnih težav, ki se nanašajo na njegovo uporabo. Za vzpostavitev ustreznih varnostnih in zdravstvenih praks ter za določitev uporabnosti regulativnih omejitev pred uporabo je odgovoren uporabnik tega evropskega standarda.

General Information

Status
Published
Public Enquiry End Date
29-Mar-2016
Publication Date
07-Nov-2018
Technical Committee
VLA - Water proofing
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
05-Nov-2018
Due Date
10-Jan-2019
Completion Date
08-Nov-2018

Relations

Effective Date
01-Dec-2018

Overview

EN 13702:2018 - "Bitumen and bituminous binders - Determination of dynamic viscosity of bitumen and bituminous binders by the cone and plate method" (CEN) specifies a laboratory method to measure dynamic viscosity of bituminous binders using a cone-and-plate viscometer. The method applies to paving-grade and polymer-modified binders (PMBs), aged or unaged, and is suitable for recovered binders (with no or limited filler) extracted from asphalt mixtures.

Key topics and technical requirements

  • Principle: A sample is placed between a cone and plate; torque at specified shear rates is measured and converted to dynamic viscosity (η = τ / γ̇).
  • Apparatus ranges:
    • Shear rate: 5 × 10−2 s−1 to 5 × 102 s−1
    • Viscosity: 5 × 10−2 Pa·s to 105 Pa·s
    • Temperature control: typically 60 °C to 180 °C with accuracy ±0.5 °C up to 100 °C and ±1.0 °C above 100 °C
  • Procedure highlights:
    • Sampling per EN 58 and sample preparation per EN 12594
    • Select cone geometry to match desired shear rate; maintain temperature stability
    • Set shear rate within ±10 %, allow stabilization (60 ± 5 s) and read viscosity; average two tests
    • If two results differ by >5 % repeat on a new sample
    • Example test points: 60 °C at 5 × 10−2 s−1; 100 °C at 5 × 101 s−1; 150 °C at 5 × 102 s−1
  • Precision:
    • Repeatability: differences >5 % expected in only 1 case in 20
    • Reproducibility: differences >15 % expected in only 1 case in 20
  • Notes: Cone factor, non-Newtonian behaviour (e.g., thixotropy in PMBs), and rheological effects (Weissenberg) are addressed; software in modern viscometers typically performs calculations.

Applications

  • Quality control and acceptance testing of bitumen and polymer-modified binders
  • Characterisation of viscosity across temperature and shear-rate ranges for mix design, production control and performance assessment
  • Evaluation of recovered binders from asphalt for recycling research and specification compliance
  • R&D and comparative testing of binder formulations

Who uses this standard

  • Pavement material testing laboratories
  • Bitumen and asphalt manufacturers
  • Road authorities and specification bodies
  • Academic and industrial researchers working on binder rheology and recycling

Related standards

  • EN 58 - Sampling bituminous binders
  • EN 12594 - Preparation of test samples
  • EN 12697-3 / EN 12697-4 - Bitumen recovery methods (rotary evaporator, fractionating column)

Safety note

EN 13702:2018 includes a safety warning: testing may involve hazardous materials and equipment. Users must follow appropriate laboratory safety procedures and regulatory limits before conducting tests.

Frequently Asked Questions

SIST EN 13702:2018 is a standard published by the Slovenian Institute for Standardization (SIST). Its full title is "Bitumen and bituminous binders - Determination of dynamic viscosity of bitumen and bituminous binders by the cone and plate method". This standard covers: This document specifies a method for determining the dynamic viscosity of a bituminous binder over a range of temperatures by means of a cone and plate viscometer. The test method is intended for all bituminous binders (e.g. paving grade bitumen and polymer modified), unaged or aged. It is also suitable for recovered bituminous binders according to EN 12697 3 [1] and EN 12697 4 [2] with no or limited amount of filler. WARNING - The use of this document may involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this document to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

This document specifies a method for determining the dynamic viscosity of a bituminous binder over a range of temperatures by means of a cone and plate viscometer. The test method is intended for all bituminous binders (e.g. paving grade bitumen and polymer modified), unaged or aged. It is also suitable for recovered bituminous binders according to EN 12697 3 [1] and EN 12697 4 [2] with no or limited amount of filler. WARNING - The use of this document may involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this document to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

SIST EN 13702:2018 is classified under the following ICS (International Classification for Standards) categories: 75.140 - Waxes, bituminous materials and other petroleum products; 91.100.50 - Binders. Sealing materials. The ICS classification helps identify the subject area and facilitates finding related standards.

SIST EN 13702:2018 has the following relationships with other standards: It is inter standard links to SIST EN 13702:2010. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

SIST EN 13702:2018 is associated with the following European legislation: EU Directives/Regulations: 305/2011; Standardization Mandates: M/124. When a standard is cited in the Official Journal of the European Union, products manufactured in conformity with it benefit from a presumption of conformity with the essential requirements of the corresponding EU directive or regulation.

You can purchase SIST EN 13702:2018 directly from iTeh Standards. The document is available in PDF format and is delivered instantly after payment. Add the standard to your cart and complete the secure checkout process. iTeh Standards is an authorized distributor of SIST standards.

Standards Content (Sample)


2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Bitumen und bitumenhaltige Bindemittel - Bestimmung der dynamischen Viskosität von Bitumen und bitumenhaltigen Bindemitteln mit dem Platte-Kegel-VerfahrenBItume et liants bitumineux - Détermination de la viscosité dynamique des bitumes modifiés par la méthode cône et plateauBitumen and bituminous binders - Determination of dynamic viscosity of bitumen and bituminous binders by the cone and plate method91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:Ta slovenski standard je istoveten z:EN 13702:2018SIST EN 13702:2018en,fr,de01-december-2018SIST EN 13702:2018SLOVENSKI
STANDARDSIST EN 13702:20101DGRPHãþD

EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 13702
October
t r s z ICS
y wä s v râ
{ sä s r rä w r Supersedes EN
s u y r tã t r s rEnglish Version
Bitumen and bituminous binders æ Determination of dynamic viscosity of bitumen and bituminous binders by the cone and plate method Bitumes et liants bitumineux æ Détermination de la viscosité dynamique des bitumes et liants bitumineux par la méthode du cône et plateau
Bitumen und bitumenhaltige Bindemittel æ Bestimmung der dynamischen Viskosität von Bitumen und bitumenhaltigen Bindemitteln mit dem PlatteæKegelæVerfahren This European Standard was approved by CEN on
t y August
t r s zä
egulations which stipulate the conditions for giving this European Standard the status of a national standard without any alterationä Upætoædate lists and bibliographical references concerning such national standards may be obtained on application to the CENæCENELEC Management Centre or to any CEN memberä
translation under the responsibility of a CEN member into its own language and notified to the CENæCENELEC Management Centre has the same status as the official versionsä
CEN members are the national standards bodies of Austriaá Belgiumá Bulgariaá Croatiaá Cyprusá Czech Republicá Denmarká Estoniaá Finlandá Former Yugoslav Republic of Macedoniaá Franceá Germanyá Greeceá Hungaryá Icelandá Irelandá Italyá Latviaá Lithuaniaá Luxembourgá Maltaá Netherlandsá Norwayá Polandá Portugalá Romaniaá Serbiaá Slovakiaá Sloveniaá Spainá Swedená Switzerlandá Turkey and United Kingdomä
EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre:
Rue de la Science 23,
B-1040 Brussels
t r s z CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Membersä Refä Noä EN
s u y r tã t r s z ESIST EN 13702:2018
...

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