SIST EN ISO 9455-2:2001

SLOVENSKI STANDARD
01-februar-2001
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Soft soldering fluxes - Test methods - Part 2: Determination of non-volatile matter,
ebulliometric method (ISO 9455-2:1993)
Flußmittel zum Weichlöten - Prüfverfahren - Teil 2: Bestimmung nichtflüchtiger Stoffe,
ebulliometrische Methode (ISO 9455-2:1993)
Flux de brasage tendre - Méthodes d'essai - Partie 2: Dosage des matieres non volatiles
par ébulliométrie (ISO 9455-2:1993)
Ta slovenski standard je istoveten z: EN ISO 9455-2:1995
ICS:
25.160.50 Trdo in mehko lotanje Brazing and soldering
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

INTERNATIONAL Is0
STANDARD 9455-2
First edition
1993-04-I 5
Soft soldering fluxes - Test methods -
Part 2:
Determination of non-volatile matter,
ebulliometric method
Flux de brasage tendre - M&hodes d’essai -
Partie 2: Dosage des mat&es non volatiles par 6bulliom6 trie
Reference number
IS0 9455-Z: 1993(E)
IS0 9455-Z: 1993(E)
Foreword
IS0 (the International Organization for Standardizat ion) is a worldw ‘ide
federation of national standards bodies (IS0 member bodies). The work
of preparing International Standards is normally carried out through IS0
technical committees. Each member body interested in a subject for
which a technical committee has been established has the right to be
represented on that committee. International organizations, governmental
and non-governmental, in liaison with ISO, also take part in the work. IS0
collaborates closely with the International Electrotechnical Commission
(I EC) on all matters of electrotechnical standardization.
Draft International Standards adopted by the technical committees are
circulated to the member bodies for voting. Publication as an International
Standard requires approval by at least 75 % of the member bodies casting
a vote.
International Standard IS0 9455-2 was prepared by Technical Committee
ISO/TC 44, Welding and allied processes, Sub-Committee SC 12,
Soldering and brazing materials.
IS0 9455 consists of the following parts, under the general title Soft
soldering fluxes - Test methods:
- Part 7: Determination of non-volatile matter, gravimetric method
- Part 2: Determination of non-volatile matter, ebulliometric method
- Part 3: Determination of acid value, po ten tiome tric and visual
titration methods
- Part 5: Copper mirror test
- Part 6: De termination of halide content
- Part 8: Determination of zinc content
- Part 9: Determination of ammonia content
- Part ? 0: Flux efficacy tests, solder spread method
- Part 7 7: Solubility of flux residues
0 IS0 1993
All rights reserved. No part of this publication may be reproduced or utilized in any form or
by any means, electronic or mechanical, including photocopying and microfilm, without per-
mission in writing from the publisher.
International Organization for Standardization
Case Postale 56 l CH-1211 Geneve 20 l Switzerland
Printed in Switzerland
IS0 9455-2: 1993(E)
- Part 12: Steel tube corrosion test
- Part 13: Determination of flux spattering
- Part 14: Assessment of tackiness of flux residues
- Part 15: Copper corrosion test
- Part 16: Flux efficacy tests, wetting balance method
[Technical Report]
- Part 17: Determination of surface insulation resistance of flux resi-
dues (Comb test)
- Part 18: Electrochemical migration test for flux residues
Annex A of this part of IS0 9455 is for information only.

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INTERNATIONAL STANDARD IS0 9455-2: 1993(E)
- Test methods -
Soft soldering fluxes
Part 2:
Determination of non-volatile matter, ebulliometric method
1 Scope 3 Principle
This part of ISQ 9455 specifies an ebulliometric A weighed amount of the flux sample is evaporated
method for the determination of the content of non- in an ebulliometer until the entire volatile part is driven
volatile matter in soft soldering fluxes. It is applicable off, which is determined by following the graph of
to liquid fluxes of classes 1 .I .I, 1 .I .2 and 1 .I .3, as distillation temperature against time. The flux residue
is considered as the non-volatile content of flux.
defined in IS0 9454-1, and only those fluxes contain-
ing solvents of relatively high volatility, such as
propan-2-01. The method is applicable only to fluxes
with a non-volatile content of 10 % or more.
NOTE 1 For the determination of the content of non-
4 Apparatus
volatile matter of liquid fluxes of these classes, where the
solvent has a lower volatility than propan-2-01, the method
Usual laboratory apparatus and, in particular, the fol-
given in IS0 9455-l should be used.
lowing.
4.1 Martin ebulliometer (IS0 4791-1:1985,
2 Normative references
5.04.10), but with a spherical distillation flask, as
shown in figure 1.
The following standards contain provisions which,
through reference in this text, constitute provisions
NOTE 2 It has been found that better heat exchange
of this part of IS0 9455. At the time of publication, the
characteristics are obtained between the heater and the
editions indicated were valid. All standards are subject
distillation flask if a spherical flask is used rather than the
to revision, and parties to agreements based on this
pear-shaped flask normally supplied with the Martin
part of IS0 9455 are encouraged to investigate the
ebulliometer.
possibility of applying the most recent editions of the
standards indicated below. Members of IEC and IS0
maintain registers of currently valid International
4.2 Thermostatically controlled heater, suitable
Standards.
for heating the distillation flask of the ebulliometer.
IS0 4791-I : 1985, Laboratory apparatus - Vocabulary
relating to apparatus made essentially from glass,
4.3 Laboratory thermometer, covering the range
porcelain or vitreous silica - Part 1: Names for items
50 “C to 150 O
...