SIST EN 16317:2013/kFprA1:2016
(Amendment)Fertilizers and liming materials - Determination of arsenic by inductively coupled plasma-atomic emission spectrometry (ICP-AES) after aqua regia dissolution
Fertilizers and liming materials - Determination of arsenic by inductively coupled plasma-atomic emission spectrometry (ICP-AES) after aqua regia dissolution
EN 16317:2013 will be amended taking into account liming materials in the scope of the method. Clause 10 Precision and Annex A Results of the inter-laboratory test will be amended by addition of the precision data received from the inter-laboratory test performed in 2013 analysing samples of liming materials. The main title of the document will be extended to liming materials to read: Fertilizers and liming materials.
Düngemittel und Kalkdünger - Bestimmung von Arsen mit Atomemissionsspektrometrie mit induktiv gekoppeltem Plasma (ICP-AES) nach Königswasseraufschluss
Engrais et amendements minéraux basiques - Détermination de l'arsenic par spectrométrie d'émission atomique avec plasma induit par haute fréquence (ICP-AES) après digestion á l'eau régale
Gnojila in sredstva za apnjenje - Določevanje arzena z atomsko emisijsko spektrometrijo z induktivno sklopljeno plazmo (ICP/AES) po raztapljanju v zlatotopki - Dopolnilo A1
General Information
- Status
- Not Published
- Public Enquiry End Date
- 29-Sep-2015
- Technical Committee
- KAT - Soil quality
- Current Stage
- 98 - Abandoned project (Adopted Project)
- Start Date
- 16-Oct-2017
- Due Date
- 21-Oct-2017
- Completion Date
- 16-Oct-2017
Relations
- Effective Date
- 01-Dec-2017
- Effective Date
- 01-Sep-2015
Overview
SIST EN 16317:2013/kFprA1:2016 is a European standard developed by CEN/TC 260 that defines a precise analytical method for determining arsenic content in fertilizers and liming materials. The method employs inductively coupled plasma-atomic emission spectrometry (ICP-AES) following sample dissolution with aqua regia. This amendment updates the scope of the original EN 16317:2013 standard to explicitly include liming materials alongside fertilizers, reflecting their growing importance in agricultural soil treatment.
The standard ensures accurate and reproducible quantification of arsenic, a potentially toxic element, which is critical for regulatory compliance and safe agricultural practices. It incorporates results from extensive inter-laboratory tests, providing validated precision data specific to liming materials - such as dolomitic limestone, burnt lime, and converter lime.
Key Topics
Scope Expansion
The method applies to both fertilizers and liming materials, allowing labs to use a unified procedure for arsenic determination in these soil amendments.Analytical Technique
Utilizes inductively coupled plasma-atomic emission spectrometry (ICP-AES), known for high sensitivity and multi-element detection capabilities.Sample Preparation
Samples are dissolved using aqua regia, a mixture of nitric and hydrochloric acids, ensuring efficient extraction of arsenic for analysis.Precision and Reproducibility
Includes enhanced precision data derived from inter-laboratory trials conducted in 2013, addressing repeatability and reproducibility for different liming materials.Inter-Laboratory Validation
Statistical evaluation based on tests across multiple labs enhances confidence in results, critical for standardized compliance testing.Terminology Updates
Harmonizes terms by referencing EN 12944 series standards related to fertilizers and liming materials vocabulary.
Applications
Agricultural Quality Control
Enables fertilizer and liming material producers to verify arsenic levels, ensuring products meet safety standards and environmental regulations.Soil Amendment Testing
Authorities and laboratories assessing soil treatment products use this method to monitor arsenic contamination risks.Regulatory Compliance
Supports compliance with European Union and national regulations governing trace element content in agricultural inputs.Research and Development
Provides a standardized analytical approach for R&D efforts aimed at improving fertilizer and liming material formulations.Environmental Monitoring
Helps assess potential soil contamination from agricultural sources by quantifying arsenic residues accurately.
Related Standards
EN 12944-1, EN 12944-2, EN 12944-3
Define vocabulary and terms applicable to fertilizers and liming materials, referenced for consistent terminology in EN 16317.EN 16317:2013 (Original Standard)
The foundation document for arsenic determination in fertilizers, now extended by this amendment to include liming materials.Other ICP-AES Method Standards
Complementary standards exist for determining trace elements in different matrices, offering additional protocols for laboratories.
Keywords: EN 16317:2013, fertilizer standards, liming materials standard, arsenic determination, ICP-AES, aqua regia dissolution, CEN standards, agricultural quality control, soil amendment analysis, trace element testing
Frequently Asked Questions
SIST EN 16317:2013/kFprA1:2016 is a draft published by the Slovenian Institute for Standardization (SIST). Its full title is "Fertilizers and liming materials - Determination of arsenic by inductively coupled plasma-atomic emission spectrometry (ICP-AES) after aqua regia dissolution". This standard covers: EN 16317:2013 will be amended taking into account liming materials in the scope of the method. Clause 10 Precision and Annex A Results of the inter-laboratory test will be amended by addition of the precision data received from the inter-laboratory test performed in 2013 analysing samples of liming materials. The main title of the document will be extended to liming materials to read: Fertilizers and liming materials.
EN 16317:2013 will be amended taking into account liming materials in the scope of the method. Clause 10 Precision and Annex A Results of the inter-laboratory test will be amended by addition of the precision data received from the inter-laboratory test performed in 2013 analysing samples of liming materials. The main title of the document will be extended to liming materials to read: Fertilizers and liming materials.
SIST EN 16317:2013/kFprA1:2016 is classified under the following ICS (International Classification for Standards) categories: 65.080 - Fertilizers. The ICS classification helps identify the subject area and facilitates finding related standards.
SIST EN 16317:2013/kFprA1:2016 has the following relationships with other standards: It is inter standard links to SIST EN 16317:2013+A1:2017, SIST EN 16317:2013. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
SIST EN 16317:2013/kFprA1:2016 is associated with the following European legislation: Standardization Mandates: M/418. When a standard is cited in the Official Journal of the European Union, products manufactured in conformity with it benefit from a presumption of conformity with the essential requirements of the corresponding EU directive or regulation.
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Standards Content (Sample)
SLOVENSKI STANDARD
SIST EN 16317:2013/oprA1:2015
01-september-2015
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Fertilizers and liming materials - Determination of arsenic by inductively coupled plasma-
atomic emission spectrometry (ICP-AES) after aqua regia dissolution
Düngemittel und Kalkdünger - Bestimmung von Arsen mit Atomemissionsspektrometrie
mit induktiv gekoppeltem Plasma (ICP-AES) nach Königswasseraufschluss
Engrais et amendements minéraux basiques - Détermination de l'arsenic par
spectrométrie d'émission atomique avec plasma induit par haute fréquence (ICP-AES)
après digestion á l'eau régale
Ta slovenski standard je istoveten z: EN 16317:2013/prA1
ICS:
65.080 Gnojila Fertilizers
SIST EN 16317:2013/oprA1:2015 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
SIST EN 16317:2013/oprA1:2015
SIST EN 16317:2013/oprA1:2015
EUROPEAN STANDARD
DRAFT
EN 16317:2013
NORME EUROPÉENNE
EUROPÄISCHE NORM
prA1
June 2015
ICS 65.080
English Version
Fertilizers and liming materials - Determination of arsenic by
inductively coupled plasma-atomic emission spectrometry (ICP-
AES) after aqua regia dissolution
Engrais et amendements minéraux basiques - Düngemittel und Kalkdünger - Bestimmung von Arsen mit
Détermination de l'arsenic par spectrométrie d'émission Atomemissionsspektrometrie mit induktiv gekoppeltem
atomique avec plasma induit par haute fréquence (ICP- Plasma (ICP-AES) nach Königswasseraufschluss
AES) après digestion á l'eau régale
This draft amendment is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee CEN/TC 260.
This draft amendment A1, if approved, will modify the European Standard EN 16317:2013. If this draft becomes an amendment, CEN
members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for inclusion of this amendment
into the relevant national standard without any alteration.
This draft amendment was established by CEN in three official versions (English, French, German). A version in any other language made
by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has
the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United
Kingdom.
Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are aware and to
provide supporting documentation.
Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without notice and
shall not be referred to as a European Standard.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2015 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 16317:2013/prA1:2015 E
worldwide for CEN national Members.
SIST EN 16317:2013/oprA1:2015
EN 16317:2013/prA1:2015 (E)
Contents
Page
Foreword .3
1 Modification to the Title .4
2 Modifications to Clause 1, Scope .4
3 Modification to Clause 2, Normative references .
...
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