SIST EN ISO 14544:2016

SLOVENSKI STANDARD
01-junij-2016
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SIST EN 12290:2005
SIST EN 12291:2004
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Fine ceramics (advanced ceramics, advanced technical ceramics) - Mechanical
properties of ceramic composites at high temperature - Determination of compression
properties (ISO 14544:2013)
Hochleistungskeramik - Mechanische Eigenschaften von keramischen
Verbundwerkstoffen bei hoher Temperatur - Bestimmung der Eigenschaften unter Druck
(ISO 14544:2013)
Céramiques techniques - Propriétés mécaniques des céramiques composites à haute
température - Détermination des caractéristiques en compression (ISO 14544:2013)
Ta slovenski standard je istoveten z: EN ISO 14544:2016
ICS:
81.060.30 Sodobna keramika Advanced ceramics
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 14544
EUROPEAN STANDARD
NORME EUROPÉENNE
April 2016
EUROPÄISCHE NORM
ICS 81.060.30 Supersedes EN 12290:2005, EN 12291:2003
English Version
Fine ceramics (advanced ceramics, advanced technical
ceramics) - Mechanical properties of ceramic composites
at high temperature - Determination of compression
properties (ISO 14544:2013)
Céramiques techniques - Propriétés mécaniques des Hochleistungskeramik - Mechanische Eigenschaften
céramiques composites à haute température - von keramischen Verbundwerkstoffen bei hoher
Détermination des caractéristiques en compression Temperatur - Bestimmung der Eigenschaften unter
(ISO 14544:2013) Druck (ISO 14544:2013)
This European Standard was approved by CEN on 18 March 2016.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2016 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 14544:2016 E
worldwide for CEN national Members.

Contents Page
European foreword . 3
European foreword
The text of ISO 14544:2013 has been prepared by Technical Committee ISO/TC 206 “Fine ceramics” of
the International Organization for Standardization (ISO) and has been taken over as EN ISO 14544:2016
by Technical Committee CEN/TC 184 “Advanced technical ceramics” the secretariat of which is held by
DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by October 2016, and conflicting national standards shall
be withdrawn at the latest by October 2016.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent
rights.
This document supersedes EN 12291:2003, EN 12290:2005.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 14544:2013 has been approved by CEN as EN ISO 14544:2016 without any modification.

INTERNATIONAL ISO
STANDARD 14544
First edition
2013-07-01
Fine ceramics (advanced ceramics,
advanced technical ceramics) —
Mechanical properties of ceramic
composites at high temperature —
Determination of compression
properties
Céramiques techniques — Propriétés mécaniques des céramiques
composites à haute température — Détermination des
caractéristiques en compression
Reference number
ISO 14544:2013(E)
©
ISO 2013
ISO 14544:2013(E)
© ISO 2013
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
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Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.org
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Published in Switzerland
ii © ISO 2013 – All rights reserved

ISO 14544:2013(E)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 3
5 Apparatus . 4
5.1 Test machine . 4
5.2 Load train. 4
5.3 Gastight test chamber . 4
5.4 Set-up for heating . 5
5.5 Extensometer . 5
5.6 Temperature measurement . 5
5.7 Data recording system . 5
5.8 Micrometers . 6
6 Test specimens. 6
6.1 General . 6
6.2 Compression between platens . 6
6.3 Test specimen used with grips . 7
7 Test specimen preparation .10
7.1 Machining and preparation .10
7.2 Number of test specimens .10
8 Test procedures .11
8.1 Test set-up: temperature considerations .11
8.2 Test set-up: other considerations .11
8.3 Testing technique .12
8.4 Test validity .13
9 Calculation of results .13
9.1 Test specimen origin .13
9.2 Compression strength .13
9.3 Strain at maximum compression force .14
9.4 Proportionality ratio or pseudo-elastic modulus, elastic modulus .14
10 Test report .16
Annex A (normative) Buckling: How to proceed when buckling is suspected .17
Bibliography .18
ISO 14544:2013(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2. www.iso.org/directives
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of any
patent rights identified during the development of the document will be in the Introduction and/or on
the ISO list of patent declarations received. www.iso.org/patents
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
The committee responsible for this document is ISO/TC 206, Fine ceramics.
iv © ISO 2013 – All rights reserved

INTERNATIONAL STANDARD ISO 14544:2013(E)
Fine ceramics (advanced ceramics, advanced technical
ceramics) — Mechanical properties of ceramic
composites at high temperature — Determination of
compression properties
1 Scope
This International Standard specifies the conditions for determination of compression properties of
ceramic matrix composite materials with continuous fibre reinforcement for temperatures up to 2 000 °C.
This International Standard applies to all ceramic matrix composites with a continuous fibre
reinforcement, unidirectional (1D), bidirectional (2D), and tridirectional (xD, with 2 < x ≤ 3), loaded
along one principal axis of reinforcement.
Two types of compression are distinguished:
a) compression between platens;
b) compression using grips.
2 Normative references
The following documents, in whole or in part, are normatively referenced in this document and are
indispensable for its application. For dated references, only the edition cited applies. For undated
references, the latest edition of the referenced document (including any amendments) applies.
ISO 3611, Geometrical product specifications (GPS) — Dimensional measuring equipment: Micrometers for
external measurements — Design and metrological characteristics
ISO 7500-1, Metallic materials — Verification of static uniaxial testing machines — Part 1: Tension/compression
testing machines — Verification and calibration of the force-measuring system
EN 10002-4, Metallic materials — Tensile test — Part 4: Verification of extensometers used in uniaxial testing
CEN/TS 15867:2009, Advanced technical ceramics — Ceramic composites — Guide to the determination of
the degree of misalignment in unixial mechanical tests
IEC 60584-1:1995, Thermocouples — Part 1: Reference tables
IEC 60584-2:1982, Thermocouples — Part 2: Tolerances
IEC 60584-2:1982,Amendment 1:1989
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.
3.1
test temperature
T
temperature of the test piece at the centre of the gauge length
ISO 14544:2013(E)
3.2
calibrated length
l
part of the test specimen that has uniform and minimum cross-section area
3.3
gauge length
L
o
initial distance between reference points on the test specimen in the calibrated length
3.4
controlled-temperature zone
part of the calibrated length, including the gauge length, where the temperature is within a range of
50 °C of the test temperature
3.5
initial cross-section area
A
o
initial cross-section area of the test specimen within the calibrated length, at test temperature
Note 1 to entry: Two initial cross-section areas of the test specimen can be defined as follows.
3.5.1
apparent cross-section area
total area of the cross section, A
o,a
3.5.2
effective cross-section area
total area corrected by a factor, to account for the presence of an antioxidant protection, A
o,e
3.6
longitudinal deformation
ΔL
decrease in the gauge length L between reference points under a compression force
3.7
compression strain
ε
relative change in the gauge length defined as the ratio ΔL/L
o
Note 1 to entry: Its value corresponding to the maximum force shall be denoted as ε .
c,m
3.8
compression stress
σ
compression force supported by the test specimen at any time in the test divided by the initial cross-
section area (A )
o
Note 1 to entry: Two compression stresses can be distinguished:
— apparent compression stress, σ , when the apparent cross-section area (or total cross-section area) is used;
a
— effective compression stress, σ , when the effective cross-section area is used
e
3.9
maximum compression force
F
m
highest recorded compression force in a compression test on the test specimen when tested to failure
2 © ISO 2013 – All rights reserved

ISO 14544:2013(E)
3.10
compression strength
σ
c,m
ratio of the maximum compression force (F ) to the initial cross-section area (A )
m o
Note 1 to entry: Two compression strengths can be distinguished:
— apparent compression strength, σ , when the apparent cross-section area (or total cross-section area) is used;
c,m,a
— effective compression strength, σ , when the effective cross-section area is used.
c,m,e
3.11
proportionality ratio or pseudo-elastic modulus, E
p
slope of the linear section of the stress-strain curve, if any
Note 1 to entry: Examination of the stress-strain curves for ceramic matrix composites allows definition of the
following cases:
a)  Material with a linear section in the stress-strain curve.
For ceramic matrix composites that have a mechanical behaviour characterized by a linear section, the
proportionality ratio is defined as:
σσ−
Ep(σσ,)= (1)
εε−
where (ε , σ ) and (ε , σ ) lie near the lower and upper limits of the linear section of the stress-strain curve.
1 1 2 2
The proportionality ratio or pseudo-elastic modulus is termed the elastic modulus, E, in the single case where the
material has a linear behaviour from the origin.
b)  Material with no-linear section in the stress-strain curve.
In this case only stress-strain couples can be fixed.
Two proportionality ratios or pseudo-elastic moduli can be distinguished:
— apparent proportionality ratio, Ep , when the apparent compression stress is used;
a
— effective proportionality ratio, Ep , when the effective compression stress is used.
e
4 Principle
A test specimen of specified dimensions is heated to the test temperature, and loaded in compression.
The test is performed at constant crosshead displacement rate, or constant deformation rate. Force and
longitudinal deformation are measured and recorded simultaneously.
NOTE 1 The test duration is limited to reduce creep effects.
NOTE 2 Constant loading rate is only allowed in the case of linear stress-strain behaviour up to failure.
NOTE 3 In order to protect fixtures, it is recommended to use constant crosshead displacement rate when the
test is carried out until rupture.
ISO 14544:2013(E)
5 Apparatus
5.1 Test machine
The machine shall be equipped with a system for measuring the force applied to the test specimen which
shall conform to grade 1 or better according to ISO 7500-1.
NOTE This should prevail during actual test conditions of, e.g. gas pressure and temperature.
5.2 Load train
The load train configuration shall ensure that the load indicated by the load cell and the load experienced
by the test specimen are the same.
The load train performance including the alignment system and the force transmitting system shall not
change because of heating.
The load train shall align the specimen axis with the direction of load application without introducing
bending or torsion in the specimen. The misalignment of the specimen shall be verified and documented
according to the procedure described in CEN/TS 15867:2009 The maximum percent bending shall not
−6
exceed 5 at an average strain of 500×10 .
NOTE 1 The alignment should be verified and documented in accordance with, for example, the procedure
described in CEN/TS 15867:2009.
There are two alternative means of load application.
a) Compression platens are connected to the load cell and on the moving crosshead. The parallelism of
these platens shall be better than 0,01 mm, in the loading area, at room temperature and they shall
be perpendicular to the load direction.
NOTE 1 The use of platens is not recommended for compression testing of 1D and 2D materials with low
thickness due to buckling.
NOTE 2 A compliant interlayer material between the test specimen and platens may be used for testing
macroscopically inhomogeneous materials to ensure even contact pressure. This material should be
chemically compatible with both test specimen and platen materials.
b) Grips are used to clamp and load the test specimen.
The grip design shall prevent the test specimen from slipping. The grips shall align the test specimen
axis with that of the applied force.
NOTE 3 Conformity with this requirement should be verified and documented according to, for example, the
[1]
procedure described in Reference.
NOTE 4 The grips or the platens may either be in the hot zone of the furnace or ou
...