ISO 9932:2021
(Main)Paper and board - Determination of water vapour transmission rate of sheet materials - Dynamic sweep and static gas methods
Paper and board - Determination of water vapour transmission rate of sheet materials - Dynamic sweep and static gas methods
This document describes general test methods for determining the water vapour transmission rate of sheet materials by means of a dynamic gas method or a static gas method. Depending on the method and specific apparatus employed, materials up to 38 mm thick and with water vapour transmission rates in the range from 0,05 g/(m2·d) to 65 g/(m2·d) can be tested. The basis of the function of the instrumental techniques is briefly described. Advice on calibration is given in Annex B.
Papier et carton — Détermination du coefficient de transmission de la vapeur d'eau des matériaux en feuille — Méthode dynamique par balayage de gaz et méthode statique
General Information
- Status
- Published
- Publication Date
- 28-Feb-2021
- Technical Committee
- ISO/TC 6/SC 2 - Test methods and quality specifications for paper and board
- Current Stage
- 6060 - International Standard published
- Start Date
- 01-Mar-2021
- Due Date
- 21-May-2021
- Completion Date
- 01-Mar-2021
Relations
- Effective Date
- 23-Apr-2020
Overview
ISO 9932:2021 specifies laboratory test methods for determining the water vapour transmission rate (WVTR) of sheet materials such as paper and board using two instrumental techniques: the dynamic sweep gas method (Method A) and the static gas (electrolytic) method (Method B). Depending on equipment, the standard covers materials up to 38 mm thickness and WVTRs from 0.05 to 65 g/(m2·d). Annexes provide guidance on saturated saline solutions (Annex A) and calibration (Annex B). ISO 9932:2021 is a minor revision of the 1990 edition and complements gravimetric dish methods (see ISO 2528).
Key topics and technical requirements
- Scope and applicability: Instrumental methods for sheet materials, suitable for very low transmission rates and thicker specimens compared to gravimetric methods.
- Method A - Dynamic sweep gas:
- Principle: One side held at high relative humidity, the other swept by a dry inert gas; moisture in the sweep gas is detected by a sensor (electrical resistance, electrolytic cell or infrared).
- Requirements: sealed test cell, controlled temperature (normally 23 °C ±1 °C or 38 °C ±1 °C), desiccated sweep gas (air or nitrogen), sensitive sensor (detect ~0.05 % RH or better), and calibration specimen.
- Method B - Static gas (electrolytic):
- Principle: Test piece seals a cell containing an electrolytic element; water vapour entering the cell is electrolysed and measured as current (microammeter) per Faraday’s law.
- Requirements: humidity cabinet, stainless steel test cells, electrolytic element construction, control box with microammeter calibrated to g/(m2·d).
- Sampling and specimen preparation: Follow ISO 186 for sampling; prepare multiple test pieces (ten), account for face orientation, edge sealing for composites or thick specimens (aluminium foil tape guidance).
- Calibration and precision: Annex B covers instrument standardization; the document includes a general statement of precision and comparison notes with gravimetric (ISO 2528).
Practical applications and users
ISO 9932:2021 is used where accurate WVTR data are critical:
- Packaging engineers assessing barrier performance of paper, board and laminates.
- Quality control and testing laboratories needing faster results and higher sensitivity than gravimetric dish methods.
- R&D teams developing barrier coatings, composite sheets and multilayer materials.
- Building-materials testing where moisture transmission through panels and sheets affects performance.
- Instrument manufacturers and calibration labs for validating and standardizing WVTR test cells.
Related standards
- ISO 2528 - Gravimetric (dish) method for WVTR.
- ISO 186 - Sampling to determine average quality of paper and board.
Keywords: ISO 9932:2021, water vapour transmission rate, WVTR, dynamic sweep gas method, static gas method, paper and board, test methods, packaging, barrier materials.
Frequently Asked Questions
ISO 9932:2021 is a standard published by the International Organization for Standardization (ISO). Its full title is "Paper and board - Determination of water vapour transmission rate of sheet materials - Dynamic sweep and static gas methods". This standard covers: This document describes general test methods for determining the water vapour transmission rate of sheet materials by means of a dynamic gas method or a static gas method. Depending on the method and specific apparatus employed, materials up to 38 mm thick and with water vapour transmission rates in the range from 0,05 g/(m2·d) to 65 g/(m2·d) can be tested. The basis of the function of the instrumental techniques is briefly described. Advice on calibration is given in Annex B.
This document describes general test methods for determining the water vapour transmission rate of sheet materials by means of a dynamic gas method or a static gas method. Depending on the method and specific apparatus employed, materials up to 38 mm thick and with water vapour transmission rates in the range from 0,05 g/(m2·d) to 65 g/(m2·d) can be tested. The basis of the function of the instrumental techniques is briefly described. Advice on calibration is given in Annex B.
ISO 9932:2021 is classified under the following ICS (International Classification for Standards) categories: 85.060 - Paper and board. The ICS classification helps identify the subject area and facilitates finding related standards.
ISO 9932:2021 has the following relationships with other standards: It is inter standard links to ISO 9932:1990. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
ISO 9932:2021 is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.
Standards Content (Sample)
INTERNATIONAL ISO
STANDARD 9932
Second edition
2021-03
Paper and board — Determination
of water vapour transmission rate of
sheet materials — Dynamic sweep and
static gas methods
Papier et carton — Détermination du coefficient de transmission de
la vapeur d'eau des matériaux en feuille — Méthode dynamique par
balayage de gaz et méthode statique
Reference number
©
ISO 2021
© ISO 2021
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting
on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address
below or ISO’s member body in the country of the requester.
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Published in Switzerland
ii © ISO 2021 – All rights reserved
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Method A: Dynamic sweep gas method . 1
4.1 Principle . 1
4.2 Apparatus . 2
5 Method B: Static gas method . 3
5.1 Principle . 3
5.2 Apparatus . 3
6 Sampling . 4
7 Preparation of test pieces . 5
8 Procedure. 5
8.1 Method A . 5
8.2 Method B . 5
8.3 Barrier material having one face of uncoated paper . 5
8.4 Creased material . 6
9 Expression of results . 6
10 Precision . 6
10.1 General statement of the precision . 6
10.2 Method A . 6
10.3 Method B . 6
11 Test report . 6
Annex A (normative) Saturated saline solutions . 7
Annex B (normative) Calibration . 8
Annex C (informative) Comparison of dynamic method with gravimetric method .9
Bibliography .10
Foreword
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www .iso .org/ iso/ foreword .html.
This document was prepared by Technical Committee ISO/TC 6, Paper, board and pulps, Subcommittee
SC 2, Test methods and quality specifications for paper and board.
This second edition cancels and replaces the first edition (ISO 9932:1990), of which it constitutes a
minor revision. The changes compared to the previous edition are as follows:
— update of the normative references;
— removal of footnotes listing instruments in Clauses 4 and 5;
— addition of a general statement of the precision.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www .iso .org/ members .html.
iv © ISO 2021 – All rights reserved
Introduction
The rate of water vapour penetration through a barrier is an important property in many applications,
for example, in building and in packaging. ISO 2528 describes a dish method for the determination of
the transmission rate and this method has wide acceptance. It does, however, have three disadvantages.
Results take several days to obtain, it is not suitable for transmission rates less than 1 g/(m ·d) and it is
not recommended for materials thicker than 3 mm.
The methods described in this document can, depending on the material being tested, produce results
in a matter of hours and are suitable for materials with transmission rates considerably less than 1 g/
(m ·d). Depending on the specific apparatus, they are also suitable for materials up to 38 mm thick.
INTERNATIONAL STANDARD ISO 9932:2021(E)
Paper and board — Determination of water vapour
transmission rate of sheet materials — Dynamic sweep and
static gas methods
1 Scope
This document describes general test methods for determining the water vapour transmission rate of
sheet materials by means of a dynamic gas method or a static gas method. Depending on the method
and specific apparatus employed, materials up to 38 mm thick and with water vapour transmission
2 2
rates in the range from 0,05 g/(m ·d) to 65 g/(m ·d) can be tested. The basis of the function of the
instrumental techniques is briefly described. Advice on calibration is given in Annex B.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 186:2002, Paper and board — Sampling to determine average quality
ISO 2528:2017, Sheet materials — Determination of water vapour transmission rate (WVTR) —
Gravimetric (dish) method
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
— ISO Online browsing platform: available at https:// www .iso .org/ obp
— IEC Electropedia: available at http:// www .electropedia .org/
3.1
water vapour transmission rate
mass of water vapour transmitted through unit area in unit time under specified conditions of
temperature and humidity. It is expressed in grams per square metre per 24 h [g/(m ·d)]
3.2
dry side
side of the test cell which is exposed to low humidity
3.3
wet side
side of the test cell which is exposed to high humidity
4 Method A: Dynamic sweep gas method
4.1 Principle
The test piece is mounted between two chambers. One at a known relative humidity and the other
swept by a dry gas. The amount of water vapour picked up by the dry gas stream is detected by an
electrical sensor and converted to a reading which directly, or after calculation, is a measure of the rate
of water vapour transmission through the test piece.
4.2 Apparatus
4.2.1 Test cell, designed to clamp a test piece having a defined area, between two chambers, one swept
by a dry gas (the dry side) and the other containing an atmosphere of high relative humidity (the wet
side) (see Figure 1).
Key
1 flowmeter 8 by-pass
2 desiccant column or electrolytic cell 9 recorder or display
3 test piece 10 sensor (infra-red, electrolytic cell or electrical
4 dry side resistance element)
5 test cell A gas recirculation in some systems
6 enclosure maintained at required temperature B dry gas in
7 water or saline solution
Figure 1 — Schematic diagram of dynamic system
4.2.2 Clamping arrangements, to allow rapid insertion and removal of the test piece, equipped with
s
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