IEC TS 62607-8-4:2024
(Main)Nanomanufacturing – Key control characteristics – Part 8-4: Metal-oxide interfacial devices – Activation energy of electronic trap states: Low-frequency-noise spectroscopy
Nanomanufacturing – Key control characteristics – Part 8-4: Metal-oxide interfacial devices – Activation energy of electronic trap states: Low-frequency-noise spectroscopy
IEC 62607-8-4:2024 specifies a measurement protocol to determine the key control characteristic
- activation energy of electronic trap states
for metal-oxide interfacial devices by
- low-frequency-noise spectroscopy
The noise spectra peak temperatures are obtained within a designated temperature range. Activation energies are then calculated based on the frequency dependence of the peak temperatures to analyse the energy levels associated with the electronic trap states. The activation energy is determined by the temperature dependence of the capture time at electron traps under the assumption that it is described by an Arrhenius function.
- In metal-oxide interfacial devices, electrical conductance is observed through an oxide nanolayer sandwiched between metal electrodes.
- The size of the conductive path in metal-oxide interfacial devices is dependent on the current value and is usually nanoscale in diameter, taking the form of a filamentary wire. This evaluation method is useful for analysing the electronic trap states in nanowires and other miniaturized devices that have nanolayers.
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IEC TS 62607-8-4 ®
Edition 1.0 2024-12
TECHNICAL
SPECIFICATION
Nanomanufacturing – Key control characteristics –
Part 8-4: Metal-oxide interfacial devices – Activation energy of electronic trap
states: Low-frequency-noise spectroscopy
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IEC TS 62607-8-4 ®
Edition 1.0 2024-12
TECHNICAL
SPECIFICATION
Nanomanufacturing – Key control characteristics –
Part 8-4: Metal-oxide interfacial devices – Activation energy of electronic trap
states: Low-frequency-noise spectroscopy
INTERNATIONAL
ELECTROTECHNICAL
COMMISSION
ICS 07.120 ISBN 978-2-8327-0080-8
– 2 – IEC TS 62607-8-4:2024 © IEC 2024
CONTENTS
FOREWORD . 4
INTRODUCTION . 6
1 Scope . 7
2 Normative references . 7
3 Terms, definitions, and abbreviated terms . 7
3.1 Terms and definitions . 7
3.1.1 General terms . 8
3.1.2 Terms specific to this document . 8
3.2 Abbreviated terms . 8
4 General . 9
4.1 Measurement principle . 9
4.2 Sample preparation of the DUT . 9
4.3 Experimental setup and apparatus . 9
5 Measurement procedure . 10
6 Data analysis and interpretation of results . 11
6.1 General . 11
6.2 Peak determination . 11
6.3 Interpretation of results . 11
7 Reporting data . 12
Annex A (informative) Case study: Low-frequency-noise spectroscopy measurement
of metal-oxide interfacial device . 13
A.1 General . 13
A.2 LFNS measurement . 13
A.3 Data analysis . 14
Annex B (informative) Case study: Low-frequency-noise spectroscopy measurement
of metal-oxide interfacial device . 18
B.1 General . 18
B.2 LFNS measurement . 18
B.3 Data analysis . 19
Annex C (informative) Case study: Low-frequency-noise spectroscopy measurement
of metal-oxide interfacial device (electrochemical-type [6]) . 21
C.1 General . 21
C.2 LFNS measurement . 21
C.3 Data analysis . 22
Bibliography . 24
Figure 1 – An example of sample placement and experimental system . 9
Figure A.1 – Transmission electron microscopy image of TiN/TaO /TiN . 13
x
Figure A.2 – Changes in noise spectra as a function of temperature at the given
frequencies . 14
Figure A.3 – Changes in noise spectra as a function of temperature at the given
frequencies with the fitting curves to determine the peak temperatures . 15
Figure A.4 – Arrhenius plot using the peak temperatures . 16
Figure A.5 – Arrhenius plot using the peak temperatures, ln( T ∕f ) . 17
Figure B.1 – Changes in noise spectra as a function of temperature at the given
frequencies with the fitting curves to determine the peak temperatures . 19
Figure B.2 – Arrhenius plot using the peak temperatures . 20
Figure B.3 – Arrhenius plot using the peak temperatures, ln(T ∕f) . 20
Figure C.1 – Transmission electron microscopy image of Cu/Ta O /Pt . 21
2 5
Figure C.2 – Changes in noise spectra as a function of temperature at the given
frequencies with the fitting curves to determine the peak temperatures . 22
Figure C.3 – Arrhenius plot using the peak temperatures . 23
Figure C.4 – Arrhenius plot using the peak temperatures, ln(T ∕f) . 23
Table 1 – LFNS measurement sequence and parameters . 10
Table A.1 – LFNS measurement sequence and parameters . 14
Table A.2 – Peak temperature at each frequency . 15
Table A.3 – Peak temperature at each frequency, ln(T ∕f) . 16
Table A.4 – R values and activation energies . 17
Table B.1 – LFNS measurement sequence and parameters . 19
Table B.2 – R values and activation energies . 20
Table C.1 – LFNS measurement sequence and parameters . 22
Table C.2 – R values and activation energies . 23
– 4 – IEC TS 62607-8-4:2024 © IEC 2024
INTERNATIONAL ELECTROTECHNICAL COMMISSION
____________
NANOMANUFACTURING –
KEY CONTROL CHARACTERISTICS –
Part 8-4: Metal-oxide interfacial devices – Activation energy of electronic
trap states: Low-frequency-noise spectroscopy
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IEC TS 62607-8-4 has been prepared by IEC technical committee 113: Nanotechnology for
electrotechnical products and systems. It is a Technical Specification.
The text of this Technical Specification is based on the following documents:
Draft Report on vo
...
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