EN ISO 20049-1:2020
(Main)Solid biofuels - Determination of self-heating of pelletized biofuels - Part 1: Isothermal calorimetry (ISO 20049-1:2020)
Solid biofuels - Determination of self-heating of pelletized biofuels - Part 1: Isothermal calorimetry (ISO 20049-1:2020)
This document:
a) specifies a general test procedure for quantification of the spontaneous heat generation from solid biofuel pellets using isothermal calorimetry;
b) specifies a screening test procedure for wood pellets using an instrument temperature of 60 °C;
c) establishes procedures for sampling and sample handling of solid biofuel pellets prior to the analysis of spontaneous heat generation; and
d) gives guidance on the applicability and use of isothermal calorimetry for calculation of the net reaction rate of the heat producing reactions of solid biofuel pellets.
The test procedure given in this document quantifies the thermal power (heat flow) of the sample during the test, it does not identify the source of self-heating in the test portion analysed.
Data on spontaneous heat generation determined using this document is only associated with the specific quality and age of the sample material. The results are product specific.
This document is applicable to solid biofuel pellets only.
The information derived using this document is for use in quality control and in hazard and risk assessments related to the procedures given in ISO 20024:2020.
Biogene Festbrennstoffe - Bestimmung der Selbsterhitzung von Pellets aus biogenen Brennstoffen - Teil 1: Isotherme Kalorimetrie (ISO 20049-1:2020)
Dieses Dokument
a) legt ein allgemeines Prüfverfahren zur quantitativen Bestimmung der spontanen Wärmeerzeugung von Pellets aus biogenen Festbrennstoffen unter Anwendung der isothermen Kalorimetrie fest;
b) legt ein Screening Prüfverfahren für Holzpellets unter Anwendung einer Gerätetemperatur von 60 °C fest;
c) legt Verfahren für die Probenahme und Handhabung von Proben von Pellets aus biogenen Fest-brennstoffen vor der Analyse der spontanen Wärmeerzeugung fest; und
d) liefert Hinweise zur Anwendbarkeit und Anwendung der isothermen Kalorimetrie für die Berechnung der Nettoreaktionsgeschwindigkeit der wärmeerzeugenden Reaktionen von Pellets aus biogenen Fest¬brennstoffen.
Mit dem in diesem Dokument angeführten Prüfverfahren wird die thermische Leistung (der Wärmestrom) der Probe während der Prüfung quantitativ bestimmt. Die Quelle der Selbsterhitzung in der analysierten Prüfmenge wird nicht ermittelt.
Die unter Anwendung dieses Dokuments ermittelten Daten zur spontanen Wärmeerzeugung sind nur mit der spezifischen Qualität und dem Alter des Probenmaterials verbunden. Die Ergebnisse sind produkt¬spezifisch.
Dieses Dokument ist anzuwenden für Pellets aus biogenen Festbrennstoffen.
Die Informationen, die unter Anwendung dieses Dokuments abgeleitet werden, sind für die Verwendung bei der Qualitätssteuerung und Beurteilungen von Gefährdungen und Risiken im Zusammenhang mit den in ISO 20024:2020 angegebenen Verfahren bestimmt.
Biocombustibles solides - Détermination de l'auto-échauffement des granulés de biocombustibles - Partie 1: Détermination calorimétrique isotherme (ISO 20049-1:2020)
Le présent document:
a) spécifie un mode opératoire d'essai général pour la quantification, à l'aide de la détermination calorimétrique isotherme, de la production spontanée de chaleur par les granulés de biocombustibles solides;
b) spécifie un mode opératoire d'essai de présélection pour les granulés de bois utilisant une température d'appareil de 60 °C;
c) établit des procédures d'échantillonnage et de manipulation des échantillons de granulés de biocombustibles solides avant l'analyse de la production spontanée de chaleur; et
d) fournit des recommandations relatives à l'applicabilité et à l'utilisation de la détermination calorimétrique isotherme pour le calcul de la vitesse de réaction nette des réactions productrices de chaleur des granulés de biocombustibles solides.
Le mode opératoire d'essai fourni dans le présent document quantifie la puissance thermique (flux thermique) de l'échantillon pendant l'essai; il n'identifie pas la source de l'auto-échauffement dans la prise d'essai analysée.
Les données relatives à la production spontanée de chaleur déterminées à l'aide du présent document sont uniquement associées à la qualité et à l'âge spécifiques de l'échantillon de matériau. Les résultats sont propres au produit.
Le présent document s'applique exclusivement aux granulés de biocombustibles solides.
Les informations déduites à l'aide du présent document sont destinées à être utilisées dans le contrôle qualité et dans l'identification des dangers et l'évaluation des risques associés aux procédures fournies dans l'ISO 20024:2020.
Trdna biogoriva - Določanje samosegrevanja peletiziranih biogoriv - 1. del: Izotermalna kalorimetrija (ISO 20049-1:2020)
General Information
Standards Content (Sample)
SLOVENSKI STANDARD
01-julij-2020
Trdna biogoriva - Določanje samosegrevanja peletiziranih biogoriv - 1. del:
Izotermalna kalorimetrija (ISO 20049-1:2020)
Solid biofuels - Determination of self-heating of pelletized biofuels - Part 1: Isothermal
calorimetry (ISO 20049-1:2020)
Biogene Festbrennstoffe - Bestimmung der Selbsterhitzung von Pellets aus biogenen
Brennstoffen - Teil 1: Isotherme Kalorimetrie (ISO 20049-1:2020)
Biocombustibles solides - Détermination de l'auto-échauffement des granulés de
biocombustibles - Partie 1: Détermination calorimétrique isotherme (ISO 20049-1:2020)
Ta slovenski standard je istoveten z: EN ISO 20049-1:2020
ICS:
75.160.40 Biogoriva Biofuels
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
EN ISO 20049-1
EUROPEAN STANDARD
NORME EUROPÉENNE
May 2020
EUROPÄISCHE NORM
ICS 27.190; 75.160.40
English Version
Solid biofuels - Determination of self-heating of pelletized
biofuels - Part 1: Isothermal calorimetry (ISO 20049-
1:2020)
Biocombustibles solides - Détermination de l'auto- Biogene Festbrennstoffe - Bestimmung der
échauffement des granulés de biocombustibles - Partie Selbsterhitzung von Pellets aus biogenen Brennstoffen
1: Détermination calorimétrique isotherme (ISO - Teil 1: Isotherme Kalorimetrie (ISO 20049-1:2020)
20049-1:2020)
This European Standard was approved by CEN on 1 May 2020.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
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United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2020 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 20049-1:2020 E
worldwide for CEN national Members.
Contents Page
European foreword . 3
European foreword
This document (EN ISO 20049-1:2020) has been prepared by Technical Committee ISO/TC 238 "Solid
biofuels" in collaboration with Technical Committee CEN/TC 335 “Solid biofuels” the secretariat of
which is held by SIS.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by November 2020, and conflicting national standards
shall be withdrawn at the latest by November 2020.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the
United Kingdom.
Endorsement notice
The text of ISO 20049-1:2020 has been approved by CEN as EN ISO 20049-1:2020 without any
modification.
INTERNATIONAL ISO
STANDARD 20049-1
First edition
2020-05
Solid biofuels — Determination of
self-heating of pelletized biofuels —
Part 1:
Isothermal calorimetry
Biocombustibles solides — Détermination de l'auto-échauffement des
granulés de biocombustibles —
Partie 1: Détermination calorimétrique isotherme
Reference number
ISO 20049-1:2020(E)
©
ISO 2020
ISO 20049-1:2020(E)
© ISO 2020
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ISO 20049-1:2020(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 2
5 Apparatus . 3
6 Sample handling . 4
6.1 General . 4
6.2 Sampling . 4
6.3 Sample transport and storage . 4
6.4 Sample preparation . 4
7 Test procedure . 5
7.1 Temperature stabilisation . 5
7.2 Sample vial preparation . 5
7.2.1 Preparation procedure . 5
7.2.2 Procedure to find proper test portion mass in case of influence from
oxygen deficiency . 5
7.3 Reference vial preparation . 5
7.4 Measurement . 6
7.4.1 First baseline measurement . 6
7.4.2 Sample measurement . 6
7.4.3 Second baseline measurement . 6
7.4.4 Measurement data file . 6
8 Results . 7
8.1 Test data . 7
8.2 Reported data . 7
9 Test report . 7
10 Repeatability and reproducibility . 8
Annex A (normative) Calibration of the calorimeter. 9
Annex B (informative) Examples of screening data .11
Annex C (informative) Determination of reaction kinetics .13
Annex D (informative) Information on the Interlaboratory study (ILS) .21
Bibliography .27
ISO 20049-1:2020(E)
Foreword
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