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CEN

EN ISO 10301:1997

(Main)

Water quality - Determination of highly volatile halogenated hydrocarbons - Gas-chromatographic methods (ISO 10301:1997)

Water quality - Determination of highly volatile halogenated hydrocarbons - Gas-chromatographic methods (ISO 10301:1997)

Standard confirmed by resolution 281/2002

Wasserbeschaffenheit - Bestimmung leichtflüchtiger halogenierter Kohlenwasserstoffe - Gaschromatographische Verfahren (ISO 10301:1997)

Qualité de l'eau - Dosage des hydrocarbures halogénés hautement volatils - Méthodes par chromatographie en phase gazeuse (ISO 10301:1997)

Kakovost vode - Določevanje lahko hlapnih halogeniranih ogljikovodikov - Metoda plinske kromatografije (ISO 10301:1997)

General Information

Status
Published
Publication Date
14-Apr-1997
ICS
13.060.30 - Sewage water
Technical Committee
CEN/TC 230 - Water analysis
Drafting Committee
CEN/TC 230 - Water analysis
Current Stage
9093 - Decision to confirm - Review Enquiry
Start Date
21-May-2008
Completion Date
21-May-2008
Directive
76/464/EEC - Pollution caused by certain dangerous substances discharged into the aquatic environment of the Community
Mandate
M/BC/CEN/92/45 - Water analysis
Ref Project
SIST EN ISO 10301:1998 - Water quality - Determination of highly volatile halogenated hydrocarbons - Gas-chromatographic methods (ISO 10301:1997)

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EN ISO 10301:1998
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SLOVENSKI STANDARD
SIST EN ISO 10301:1998
01-januar-1998
.DNRYRVWYRGH'RORþHYDQMHODKNRKODSQLKKDORJHQLUDQLKRJOMLNRYRGLNRY0HWRGD
SOLQVNHNURPDWRJUDILMH ,62
Water quality - Determination of highly volatile halogenated hydrocarbons - Gas-
chromatographic methods (ISO 10301:1997)
Wasserbeschaffenheit - Bestimmung leichtflüchtiger halogenierter Kohlenwasserstoffe -
Gaschromatographische Verfahren (ISO 10301:1997)
Qualité de l'eau - Dosage des hydrocarbures halogénés hautement volatils - Méthodes
par chromatographie en phase gazeuse (ISO 10301:1997)
Ta slovenski standard je istoveten z: EN ISO 10301:1997
ICS:
13.060.50 3UHLVNDYDYRGHQDNHPLþQH Examination of water for
VQRYL chemical substances
SIST EN ISO 10301:1998 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 10301:1998

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SIST EN ISO 10301:1998

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SIST EN ISO 10301:1998

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SIST EN ISO 10301:1998

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SIST EN ISO 10301:1998

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SIST EN ISO 10301:1998
INTERNATIONAL IS0
STANDARD 10301
First edition
1997-04-I 5
Water quality -
Determination of highly
volatile halogenated hydrocarbons -
Gas-chromatographic methods
Qualit de I’eau - Dosage des hydrocarbures halog&& hautemen t vola tils -
Mkthodes par chromatographie en phase gazeuse
Reference number
IS0 10301:1997(E)

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SIST EN ISO 10301:1998
IS0 10301:1997(E)
Contents
1
SECTION 1: General
1
1 .I Scope
2
1.2 Normative references
3
1.3 Definition
4
SECTION 2: Liquid/liquid extraction and analysis by gas chromatography
4
2.1 Principle
4
2.2 Interferences
4
2.3 Reagents
6
2.4 Apparatus
8
2.5 Sampling and sample preparation
8
2.6 Procedure
11
2.7 Calibration
16
2.8 Identification and evaluation
18
2.9 Expression of results
19
2.10 Precision data
21
2.11 Test report
0 IS0 1997
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced
or utilized in any form or by any means, electronic or mechanical, including photocopying and
microfilm, without permission in writing from the publisher.
International Organization for Standardization
Case postale 56 l CH-1211 Genbve 20 l Switzerland
Internet central @I iso.ch
c=ch; a=4OOnet; p=iso; o=isocs; s=central
x.400
Printed in Switzerland
ii

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SIST EN ISO 10301:1998
IS0 10301:1997(E)
@ IS0
SECT ‘ION 3: Static headspace method and ana lysis by gas chromatography 22
22
3.1 Principle
3.2 Interferences 22
3.3 Reagents 22
22
3.4 Apparatus
23
3.5 Sampling
24
3.6 Procedure
26
3.7 Calibration
3.8 Identification and evaluation 29
3.9 Expression of results 31
31
3.10 Precision data
33
3.11 Test report
Annex A (informative) Characteristics of highly volatile halogenated
34
hydrocarbons
Annex B (informative) Examples of gas chromatograms for highly volatile
41
halogenated hydrocarbons
Annex C (informative) Example of a microseparator 45
Annex D (informative) Sensitivity of electron-capture detector 46
47
Annex E (informative) Extraction recovery with pentane
Annex F (informative) Qualitative method for testing the quality of
“penicillin type” stoppers 48
49
Annex G (informative) Collection of samples
. . .
III

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SIST EN ISO 10301:1998
IS0 10301:1997(E)
Foreword
IS0 (the International Organization for Standardization) is a worldwide federation of
national standards bodies (IS0 member bodies). The work of preparing International
Standards is normally carried out through IS0 technical committees. Each member
body interested in a subject for which a technical committee has been established has
the right to be represented on that committee. International organizations,
governmental and non-governmental, in liaison with ISO, also take part in the work.
IS0 collaborates closely with the International Electrotechnical Commission (IEC) on
all matters of electrotechnical standardization.
Draft International Standards adopted by the technical committees are circulated to
the member bodies for voting. Publication as an International Standard requires
approval by at least 75 % of the member bodies casting a vote.
International Standard IS0 10301 was prepared by Technical Committee lSO/TC 147,
Water quality, Subcommittee SC 2, Physical, chemical and biochemical methods.
Annexes A to G of this International Standard are for information only.
IV

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SIST EN ISO 10301:1998
@ IS0 IS0 10301:1997(E)
Introduct
...

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