Plastics - Determination of thermal conductivity and thermal diffusivity - Part 4: Light flash method (ISO 22007-4:2024)

This document specifies a method for the determination of the thermal diffusivity of a thin solid disc of plastics in the thickness direction by the light flash method. This method is based upon the measurement of the temperature rise at the rear face of the thin-disc specimen produced by a short energy pulse on the front face.
The method is applicable to homogeneous solid plastics as well as composites having an isotropic or orthotropic structure. In general, it covers materials having a thermal diffusivity, α, in the range 1 × 10−7 m2⋅s−1 < α < 1 × 10−4 m2⋅s−1. Measurements can be carried out in gaseous and vacuum environments over a temperature range from −100 °C to +400 °C.
NOTE          For inhomogeneous specimens, the measured values can be specimen thickness dependent.

Kunststoffe - Bestimmung der Wärmeleitfähigkeit und der Temperaturleitfähigkeit - Teil 4: Lichtblitzverfahren (ISO 22007-4:2024)

Dieses Dokument legt ein Verfahren zur Bestimmung der Temperaturleitfähigkeit dünner fester Kunststoffscheiben in der Dickenrichtung mit dem Lichtblitzverfahren fest. Dieses Verfahren beruht auf der Messung des Temperaturanstiegs an der Rückseite des Probekörpers in Form einer dünnen Scheibe, der durch einen kurzen Energiepuls an der Vorderseite bewirkt wird.
Das Verfahren ist anwendbar für homogene Kunststoffe im festen Zustand und Verbundstoffe, die eine isotrope oder orthotrope Struktur aufweisen. Allgemein deckt es Werkstoffe ab, die eine Temperaturleitfähigkeit α im Bereich von 1 × 10−7 m2 · s−1 < α < 1 × 10−4 m2 · s−1 aufweisen. Die Messungen können in gasförmigen Umgebungen und unter Vakuum in einem Temperaturbereich von −100 °C bis +400 °C durchgeführt werden.
ANMERKUNG   Bei inhomogenen Probekörpern können die Messwerte von der Probekörperdicke abhängen.

Plastiques - Détermination de la conductivité thermique et de la diffusivité thermique - Partie 4: Méthode flash lumineux (ISO 22007-4:2024)

Le présent document spécifie une méthode de détermination de la diffusivité thermique d’un disque plein mince en plastique suivant la direction de l’épaisseur par la méthode flash lumineux. Cette méthode est fondée sur le mesurage de l’élévation de température sur la face arrière d’une éprouvette sous forme de disque mince due à une courte impulsion énergétique sur la face avant.
La méthode est applicable aux plastiques compacts homogènes ou composites présentant une structure isotrope ou orthotrope. En général, cela inclut les matériaux ayant une diffusivité thermique, α, comprise dans la plage 1 × 10−7 m2⋅s−1 < α < 1 × 10−4 m2⋅s−1. Les mesurages peuvent être effectués en environnements gazeux et sous vide sur une plage de températures comprises entre −100 °C et +400 °C.
NOTE          Pour des éprouvettes non homogènes, les valeurs mesurées peuvent dépendre de l’épaisseur de l’éprouvette.

Polimerni materiali - Ugotavljanje toplotne prevodnosti in toplotne razprševalnosti - 4. del: Metoda z laserskim bliskom (ISO 22007-4:2024)

Ta dokument določa metodo za ugotavljanje toplotne razprševalnosti tanke trdne ploščice
iz polimernih materialov v smeri debeline z uporabo metode z laserskim bliskom. Ta metoda temelji na merjenju dviga temperature na zadnji strani tankega diska, do katerega pride zaradi kratkega energetskega impulza na sprednji strani.
Metoda se uporablja za homogene polimerne materiale v trdnem stanju in kompozite z izotropno ali ortotropno strukturo. Splošno zajema materiale, ki imajo toplotno razprševalnost, α, v območju 1 × 10−7 m2⋅s−1 < α < 1 × 10−4 m2⋅s−1. Meritve je mogoče opravljati v plinskem in vakuumskem okolju
pri temperaturi v območju od −100 °C do +400 °C.
OPOMBA: Za nehomogene primerke so izmerjene vrednosti lahko odvisne od debeline primerka.

General Information

Status
Published
Publication Date
16-Jan-2024
Technical Committee
Drafting Committee
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
17-Jan-2024
Completion Date
17-Jan-2024

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SLOVENSKI STANDARD
01-marec-2024
Polimerni materiali - Ugotavljanje toplotne prevodnosti in toplotne razprševalnosti
- 4. del: Metoda z laserskim bliskom (ISO 22007-4:2024)
Plastics - Determination of thermal conductivity and thermal diffusivity - Part 4: Light flash
method (ISO 22007-4:2024)
Kunststoffe - Bestimmung der Wärmeleitfähigkeit und der Temperaturleitfähigkeit – Teil
4: Lichtblitzverfahren (ISO 22007-4:2024)
Plastiques - Détermination de la conductivité thermique et de la diffusivité thermique -
Partie 4: Méthode par flash lumineux (ISO 22007-4:2024)
Ta slovenski standard je istoveten z: EN ISO 22007-4:2024
ICS:
83.080.01 Polimerni materiali na Plastics in general
splošno
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 22007-4
EUROPEAN STANDARD
NORME EUROPÉENNE
January 2024
EUROPÄISCHE NORM
ICS 83.080.01 Supersedes EN ISO 22007-4:2017
English Version
Plastics - Determination of thermal conductivity and
thermal diffusivity - Part 4: Light flash method (ISO 22007-
4:2024)
Plastiques - Détermination de la conductivité Kunststoffe - Bestimmung der Wärmeleitfähigkeit und
thermique et de la diffusivité thermique - Partie 4: der Temperaturleitfähigkeit - Teil 4:
Méthode par flash lumineux (ISO 22007-4:2024) Lichtblitzverfahren (ISO 22007-4:2024)
This European Standard was approved by CEN on 12 June 2023.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2024 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 22007-4:2024 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
This document (EN ISO 22007-4:2024) has been prepared by Technical Committee ISO/TC 61 "Plastics"
in collaboration with Technical Committee CEN/TC 249 “Plastics” the secretariat of which is held by SIS.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by July 2024, and conflicting national standards shall be
withdrawn at the latest by July 2024.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 22007-4:2017.
Any feedback and questions on this document should be directed to the users’ national standards
body/national committee. A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the
United Kingdom.
Endorsement notice
The text of ISO 22007-4:2024 has been approved by CEN as EN ISO 22007-4:2024 without any
modification.
International
Standard
ISO 22007-4
Third edition
Plastics — Determination of
2024-01
thermal conductivity and thermal
diffusivity —
Part 4:
Light flash method
Plastiques — Détermination de la conductivité thermique et de la
diffusivité thermique —
Partie 4: Méthode flash lumineux
Reference number
ISO 22007-4:2024(en) © ISO 2024

ISO 22007-4:2024(en)
© ISO 2024
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
ISO 22007-4:2024(en)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 2
5 Apparatus . 2
5.1 General .2
5.2 Furnace or climatic chamber .2
5.3 Flash source .4
5.4 Transient detectors .4
5.5 Thickness measurement device .5
6 Test specimen . 5
6.1 Shape and dimension of the specimen .5
6.2 Preparation and conditioning of test specimen .5
6.3 Coating the specimen .5
7 Calibration and verification . . 6
7.1 Calibration of apparatus .6
7.2 Verification of apparatus .6
8 Procedure . 6
9 Data analysis . 7
10 Uncertainty . 9
11 Test report . 9
Annex A (informative) Correction for finite pulse duration . 10
Annex B (informative) Alternative methods of calculating thermal diffusivity .11
Annex C (normative) Samples and test specimen preparation for injection mouldable
thermoplastics and thermosets.12
Bibliography .16

iii
ISO 22007-4:2024(en)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out through
ISO technical committees. Each member body interested in a subject for which a technical committee
has been established has the right to be represented on that committee. International organizations,
governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely
with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are described
in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the different types
of ISO document should be noted. This document was drafted in accordance with the editorial rules of the
ISO/IEC Directives, Part 2 (see www.iso.org/directives).
ISO draws attention to the possibility that the implementation of this document may involve the use of (a)
patent(s). ISO takes no position concerning the evidence, validity or applicability of any claimed patent
rights in respect thereof. As of the date of publication of this document, ISO had not received notice of (a)
patent(s) which may be required to implement this document. However, implementers are cautioned that
this may not represent the latest information, which may be obtained from the patent database available at
www.iso.org/patents. ISO shall not be held responsible for identifying any or all such patent rights.
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and expressions
related to conformity assessment, as well as information about ISO's adherence to the World Trade
Organization (WTO) principles in the Technical Barriers to Trade (TBT), see www.iso.org/iso/foreword.html.
This document was prepared by Technical Committee ISO/TC 61, Plastics, Subcommittee SC 5, Physical-
chemical properties, in collaboration with the European Committee for Standardization (CEN) Technical
Committee CEN/TC 249, Plastics, in accordance with the Agreement on technical cooperation between ISO
and CEN (Vienna Agreement).
This third edition cancels and replaces the second edition (ISO 22007-4:2017), which has been technically
revised.
The main changes are as follows:
— the term laser flash has been replaced by the more general term light flash.
A list of all parts in the ISO 22007 series can be f
...

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